FI93868C - Framställning av tallolje - Google Patents
Framställning av tallolje Download PDFInfo
- Publication number
- FI93868C FI93868C FI906451A FI906451A FI93868C FI 93868 C FI93868 C FI 93868C FI 906451 A FI906451 A FI 906451A FI 906451 A FI906451 A FI 906451A FI 93868 C FI93868 C FI 93868C
- Authority
- FI
- Finland
- Prior art keywords
- acid
- tall oil
- acidification
- oil
- pine
- Prior art date
Links
- 239000003784 tall oil Substances 0.000 title claims description 34
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 40
- 239000002253 acid Substances 0.000 claims description 23
- 230000020477 pH reduction Effects 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 239000003760 tallow Substances 0.000 claims 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 27
- 235000011613 Pinus brutia Nutrition 0.000 description 27
- 241000018646 Pinus brutia Species 0.000 description 27
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 23
- 239000000344 soap Substances 0.000 description 22
- 239000000203 mixture Substances 0.000 description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 239000011347 resin Substances 0.000 description 9
- 229920005989 resin Polymers 0.000 description 9
- 150000007513 acids Chemical class 0.000 description 8
- 235000014113 dietary fatty acids Nutrition 0.000 description 8
- 239000000194 fatty acid Substances 0.000 description 8
- 229930195729 fatty acid Natural products 0.000 description 8
- 150000004665 fatty acids Chemical class 0.000 description 8
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 7
- BTXXTMOWISPQSJ-UHFFFAOYSA-N 4,4,4-trifluorobutan-2-one Chemical compound CC(=O)CC(F)(F)F BTXXTMOWISPQSJ-UHFFFAOYSA-N 0.000 description 6
- BQACOLQNOUYJCE-FYZZASKESA-N Abietic acid Natural products CC(C)C1=CC2=CC[C@]3(C)[C@](C)(CCC[C@@]3(C)C(=O)O)[C@H]2CC1 BQACOLQNOUYJCE-FYZZASKESA-N 0.000 description 6
- 239000001913 cellulose Substances 0.000 description 6
- 229920002678 cellulose Polymers 0.000 description 6
- 238000004587 chromatography analysis Methods 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- QUUCYKKMFLJLFS-UHFFFAOYSA-N Dehydroabietan Natural products CC1(C)CCCC2(C)C3=CC=C(C(C)C)C=C3CCC21 QUUCYKKMFLJLFS-UHFFFAOYSA-N 0.000 description 5
- NFWKVWVWBFBAOV-UHFFFAOYSA-N Dehydroabietic acid Natural products OC(=O)C1(C)CCCC2(C)C3=CC=C(C(C)C)C=C3CCC21 NFWKVWVWBFBAOV-UHFFFAOYSA-N 0.000 description 5
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 5
- NFWKVWVWBFBAOV-MISYRCLQSA-N dehydroabietic acid Chemical compound OC(=O)[C@]1(C)CCC[C@]2(C)C3=CC=C(C(C)C)C=C3CC[C@H]21 NFWKVWVWBFBAOV-MISYRCLQSA-N 0.000 description 5
- 229940118781 dehydroabietic acid Drugs 0.000 description 5
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 5
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 4
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 4
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 4
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 4
- 239000005642 Oleic acid Substances 0.000 description 4
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 4
- 235000020778 linoleic acid Nutrition 0.000 description 4
- 239000012452 mother liquor Substances 0.000 description 4
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 229920005610 lignin Polymers 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- 229910052717 sulfur Inorganic materials 0.000 description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 description 2
- OPZZWWFHZYZBRU-UHFFFAOYSA-N butanedioic acid;butane-1,1-diol Chemical compound CCCC(O)O.OC(=O)CCC(O)=O OPZZWWFHZYZBRU-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000010433 feldspar Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 159000000000 sodium salts Chemical class 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- 235000018185 Betula X alpestris Nutrition 0.000 description 1
- 235000018212 Betula X uliginosa Nutrition 0.000 description 1
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000006114 decarboxylation reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000006317 isomerization reaction Methods 0.000 description 1
- 239000010665 pine oil Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B13/00—Recovery of fats, fatty oils or fatty acids from waste materials
- C11B13/005—Recovery of fats, fatty oils or fatty acids from waste materials of residues of the fabrication of wood-cellulose (in particular tall-oil)
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Detergent Compositions (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Claims (4)
1. Förfarande för framställning av tallolja frän mjuk talloijetväl genom surgöring av mjuk talloijetväl och genom 20 avskiljning av den sälunda erhällna tailoijän, kännetecknat av att surgöringen genomföres med saltsyra.
1. Menetelmä mäntyöljyn valmistamiseksi mäntysuovasta ha-pottamalla mäntysuopa ja erottamalla näin saatu mäntyöljy, tunnettu siitä, että hapotus suoritetaan suolahapolla. 5
2. Förfarande enligt patentkrav 1, kännetecknat av att surgöringen genomföres vid 60 tili 220°C, företrädesvis vid 25 85 tili 100°C.
2. Patenttivaatimuksen 1 mukainen menetelmä, tunnettu siitä, että hapotus suoritetaan lämpötilassa välillä 60° ja 220°C, edullisesti välillä 85° ja 100°C.
3. Förfarande enligt patentkrav 1 eller 2, kännetecknat av att surgöringsreaktionen genomföres under betingelser med förhöjt tryck vid en temperatur över 100°C. 30
3. Patenttivaatimuksen 1 tai 2 mukainen menetelmä, tunnet tu siitä, että hapotusreaktio suoritetaan yli 100°C:n lämpötilassa paineen alaisena.
4. Patenttivaatimuksen 1 mukainen menetelmä, tunnettu sii-15 tä, että saadun mäntyöljyn happoluku on 100-160 mg KOH/g.
4. Förfarande enligt patentkrav 1, kännetecknat av att sy-ratalet hos den sälunda erhällna talloijän är 100 tili 160 mg KOH/g.
Priority Applications (16)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI906451A FI93868C (sv) | 1990-12-28 | 1990-12-28 | Framställning av tallolje |
| CA 2056836 CA2056836C (en) | 1990-12-28 | 1991-12-03 | Production of tall oil |
| CH3613/91A CH682238A5 (sv) | 1990-12-28 | 1991-12-09 | |
| IT91MI3363 IT1252221B (it) | 1990-12-28 | 1991-12-16 | Produzione di tallolio |
| AT0251091A AT399172B (de) | 1990-12-28 | 1991-12-18 | Tallölherstellung |
| DE4141913A DE4141913C2 (de) | 1990-12-28 | 1991-12-18 | Tallölherstellung |
| GB9126949A GB2251248B (en) | 1990-12-28 | 1991-12-19 | Production of tall oil |
| SE9103811A SE505831C2 (sv) | 1990-12-28 | 1991-12-20 | Förfarande för framställning av tallolja från talloljetvål |
| ES9102851A ES2054541B1 (es) | 1990-12-28 | 1991-12-20 | Procedimiento para producir aceite de resina a partir de jabon blando de aceite de resina. |
| PL91292944A PL168096B1 (pl) | 1990-12-28 | 1991-12-23 | Sposób wytwarzania oleju talowego PL |
| SK4119-91A SK279772B6 (sk) | 1990-12-28 | 1991-12-27 | Spôsob výroby talového oleja |
| CS914119A CZ281616B6 (cs) | 1990-12-28 | 1991-12-27 | Způsob výroby talového oleje |
| SU5010424 RU2029782C1 (ru) | 1990-12-28 | 1991-12-27 | Способ получения таллового масла |
| NO915117A NO178897C (no) | 1990-12-28 | 1991-12-27 | Fremgangsmåte ved fremstilling av tallolje |
| FR9116224A FR2671096B1 (fr) | 1990-12-28 | 1991-12-27 | Production d'huile de tall. |
| JP1818792A JPH06340890A (ja) | 1990-12-28 | 1992-01-02 | トール油の製造方法 |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI906451 | 1990-12-28 | ||
| FI906451A FI93868C (sv) | 1990-12-28 | 1990-12-28 | Framställning av tallolje |
Publications (4)
| Publication Number | Publication Date |
|---|---|
| FI906451A0 FI906451A0 (sv) | 1990-12-28 |
| FI906451A FI906451A (sv) | 1992-06-29 |
| FI93868B FI93868B (sv) | 1995-02-28 |
| FI93868C true FI93868C (sv) | 1995-06-12 |
Family
ID=8531663
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FI906451A FI93868C (sv) | 1990-12-28 | 1990-12-28 | Framställning av tallolje |
Country Status (16)
| Country | Link |
|---|---|
| JP (1) | JPH06340890A (sv) |
| AT (1) | AT399172B (sv) |
| CA (1) | CA2056836C (sv) |
| CH (1) | CH682238A5 (sv) |
| CZ (1) | CZ281616B6 (sv) |
| DE (1) | DE4141913C2 (sv) |
| ES (1) | ES2054541B1 (sv) |
| FI (1) | FI93868C (sv) |
| FR (1) | FR2671096B1 (sv) |
| GB (1) | GB2251248B (sv) |
| IT (1) | IT1252221B (sv) |
| NO (1) | NO178897C (sv) |
| PL (1) | PL168096B1 (sv) |
| RU (1) | RU2029782C1 (sv) |
| SE (1) | SE505831C2 (sv) |
| SK (1) | SK279772B6 (sv) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI95723C (sv) * | 1992-11-10 | 1996-04-11 | Lt Dynamics Oy | Förfarande för surgöring av såpa med en stor överdosering av NaHSO3-lösning |
| WO2016040915A1 (en) * | 2014-09-12 | 2016-03-17 | Arizona Chemical Company, Llc | Process for recovering crude tall oil |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH275810A (de) * | 1948-04-16 | 1951-06-15 | Jihoceske Papirny Narodni Podn | Verfahren zur Herstellung von Tallöl. |
| GB695702A (en) * | 1949-06-29 | 1953-08-19 | Ernest Segessemann | Improved tall oil treatment |
| US2530809A (en) * | 1949-08-23 | 1950-11-21 | Pittsburgh Plate Glass Co | Fractionation of tall oil |
| US3109839A (en) * | 1962-02-26 | 1963-11-05 | Sharples Corp | Production of organic acids |
| US3575952A (en) * | 1969-10-02 | 1971-04-20 | Scm Corp | Tall oil recovery |
| US3804819A (en) * | 1972-05-03 | 1974-04-16 | Scm Corp | Recovery of fatty acids from tall oil heads |
| US4495095A (en) * | 1983-04-04 | 1985-01-22 | Union Camp Corporation | Acidulation and recovery of crude tall oil from tall oil soaps |
| US4483791A (en) * | 1983-06-22 | 1984-11-20 | Sylvachem Corporation | Recovery of fatty acids from tall oil heads |
| GB8915263D0 (en) * | 1989-07-03 | 1989-08-23 | Unilever Plc | Process for soap splitting using a high temperature treatment |
-
1990
- 1990-12-28 FI FI906451A patent/FI93868C/sv not_active IP Right Cessation
-
1991
- 1991-12-03 CA CA 2056836 patent/CA2056836C/en not_active Expired - Fee Related
- 1991-12-09 CH CH3613/91A patent/CH682238A5/de unknown
- 1991-12-16 IT IT91MI3363 patent/IT1252221B/it active IP Right Grant
- 1991-12-18 DE DE4141913A patent/DE4141913C2/de not_active Expired - Fee Related
- 1991-12-18 AT AT0251091A patent/AT399172B/de not_active IP Right Cessation
- 1991-12-19 GB GB9126949A patent/GB2251248B/en not_active Expired - Fee Related
- 1991-12-20 SE SE9103811A patent/SE505831C2/sv not_active IP Right Cessation
- 1991-12-20 ES ES9102851A patent/ES2054541B1/es not_active Expired - Lifetime
- 1991-12-23 PL PL91292944A patent/PL168096B1/pl unknown
- 1991-12-27 NO NO915117A patent/NO178897C/no unknown
- 1991-12-27 CZ CS914119A patent/CZ281616B6/cs not_active IP Right Cessation
- 1991-12-27 FR FR9116224A patent/FR2671096B1/fr not_active Expired - Fee Related
- 1991-12-27 SK SK4119-91A patent/SK279772B6/sk unknown
- 1991-12-27 RU SU5010424 patent/RU2029782C1/ru active
-
1992
- 1992-01-02 JP JP1818792A patent/JPH06340890A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| NO178897C (no) | 1996-06-26 |
| FI906451A0 (sv) | 1990-12-28 |
| ES2054541B1 (es) | 1995-02-01 |
| FI93868B (sv) | 1995-02-28 |
| ITMI913363A1 (it) | 1993-06-16 |
| GB2251248B (en) | 1994-03-30 |
| RU2029782C1 (ru) | 1995-02-27 |
| ES2054541A1 (es) | 1994-08-01 |
| PL292944A1 (en) | 1992-09-07 |
| GB9126949D0 (en) | 1992-02-19 |
| SE9103811D0 (sv) | 1991-12-20 |
| FI906451A (sv) | 1992-06-29 |
| AT399172B (de) | 1995-03-27 |
| CA2056836A1 (en) | 1992-06-29 |
| FR2671096A1 (fr) | 1992-07-03 |
| CS411991A3 (en) | 1992-07-15 |
| NO178897B (no) | 1996-03-18 |
| PL168096B1 (pl) | 1996-01-31 |
| CZ281616B6 (cs) | 1996-11-13 |
| CH682238A5 (sv) | 1993-08-13 |
| NO915117L (no) | 1992-06-29 |
| ITMI913363A0 (it) | 1991-12-16 |
| IT1252221B (it) | 1995-06-05 |
| SE505831C2 (sv) | 1997-10-13 |
| DE4141913C2 (de) | 1999-04-29 |
| SK279772B6 (sk) | 1999-03-12 |
| ATA251091A (de) | 1994-08-15 |
| FR2671096B1 (fr) | 1994-10-07 |
| CA2056836C (en) | 1999-05-04 |
| NO915117D0 (no) | 1991-12-27 |
| GB2251248A (en) | 1992-07-01 |
| SE9103811L (sv) | |
| JPH06340890A (ja) | 1994-12-13 |
| DE4141913A1 (de) | 1992-07-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| BB | Publication of examined application | ||
| MM | Patent lapsed |
Owner name: VEITSILUOTO OY |