ES2119172T5 - Procedimiento para la produccion de esteres plastificantes y esteres de poliol. - Google Patents

Procedimiento para la produccion de esteres plastificantes y esteres de poliol.

Info

Publication number
ES2119172T5
ES2119172T5 ES94906704T ES94906704T ES2119172T5 ES 2119172 T5 ES2119172 T5 ES 2119172T5 ES 94906704 T ES94906704 T ES 94906704T ES 94906704 T ES94906704 T ES 94906704T ES 2119172 T5 ES2119172 T5 ES 2119172T5
Authority
ES
Spain
Prior art keywords
esters
plastifying
procedure
production
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES94906704T
Other languages
English (en)
Other versions
ES2119172T3 (es
Inventor
Larry Oliver Jones
Glen Wilson Davis
John Lyford Iv
Sun Tsun Fong
Ramesh Relumal Hemrajani
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ExxonMobil Chemical Patents Inc
Original Assignee
ExxonMobil Chemical Patents Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=21719891&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2119172(T5) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by ExxonMobil Chemical Patents Inc filed Critical ExxonMobil Chemical Patents Inc
Application granted granted Critical
Publication of ES2119172T3 publication Critical patent/ES2119172T3/es
Publication of ES2119172T5 publication Critical patent/ES2119172T5/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1868Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1875Stationary reactors having moving elements inside resulting in a loop-type movement internally, i.e. the mixture circulating inside the vessel such that the upwards stream is separated physically from the downwards stream(s)
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

UN PROCESO PARA LA ESTERIFICACION CATALITICA O NO CATALITICA DE ACIDOS O ANHIDRIDOS CON UN MONO-ALCOHOL O UN COMPUESTO POLIHIDROXI QUE COMNPRENDE LOS PASOS DE AÑADIR LOS REAGENTES AL VASO DE REACCION PARA FORMAR UNA MEZCLA DE REACCION, Y DE CALENTAR LA MEZCLA DE REACCION Y MANTENER UNA PRESION SUFICIENTE PARA OBTENER LA EBULLICION DE LA MEZCLA DE REACCION DE MANERA QUE SE PRODUZCA LA ESTERIFICACION Y SE ELIMINE AGUA COMO VAPOR MIENTRAS QUE LA MEZCLA DE REACCION SE SIGUE CONTINUAMENTE MEZCLANDO EN EL VASO REACTOR DE MODO QUE AL MENOS ALREDEDOR DE 2.5 A 20 VOLUMENES DE LA MEZCLA DE REACCION SEAN INTERNAMENTE RECIRCULADOS POR MINUTO, POR LO CUAL SE INTENSIFICA EL INDICE DE CONVERSION.
ES94906704T 1993-01-19 1994-01-19 Procedimiento para la produccion de esteres plastificantes y esteres de poliol. Expired - Lifetime ES2119172T5 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US08/006,228 US5324853A (en) 1993-01-19 1993-01-19 Process for the production of plasticizer and polyolesters

Publications (2)

Publication Number Publication Date
ES2119172T3 ES2119172T3 (es) 1998-10-01
ES2119172T5 true ES2119172T5 (es) 2002-07-01

Family

ID=21719891

Family Applications (1)

Application Number Title Priority Date Filing Date
ES94906704T Expired - Lifetime ES2119172T5 (es) 1993-01-19 1994-01-19 Procedimiento para la produccion de esteres plastificantes y esteres de poliol.

Country Status (14)

Country Link
US (1) US5324853A (es)
EP (1) EP0680463B2 (es)
JP (1) JPH08505879A (es)
KR (1) KR100284475B1 (es)
CN (1) CN1046265C (es)
AU (1) AU675294B2 (es)
BR (1) BR9405659A (es)
CA (1) CA2154153C (es)
DE (1) DE69410988T3 (es)
ES (1) ES2119172T5 (es)
MY (1) MY110495A (es)
SG (1) SG48306A1 (es)
TW (1) TW268940B (es)
WO (1) WO1994017028A1 (es)

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JP3944251B2 (ja) * 1995-03-22 2007-07-11 松本油脂製薬株式会社 エステル精製方法
US6177387B1 (en) 1996-08-30 2001-01-23 Exxon Chemical Patents Inc Reduced odor and high stability aircraft turbine oil base stock
CN1249740A (zh) * 1997-02-28 2000-04-05 新日本理化株式会社 对羟基苯甲酸酯,包含其的增塑剂、聚酰胺树脂组合物和模塑制品
US5898077A (en) * 1997-10-07 1999-04-27 Matsumoto Yushi-Seiyaku Co., Ltd. Process for preparation of an ester
EE04110B1 (et) * 1997-11-24 2003-08-15 Energea-Umwelttechnologie Gmbh Rasvhappe metüülestri valmistamise meetod ja seadmestik meetodi realiseerimiseks
DE10056179A1 (de) * 2000-11-13 2002-05-29 Basf Ag Verfahren zur Herstellung von Estern mehrbasiger Säuren
US6906164B2 (en) * 2000-12-07 2005-06-14 Eastman Chemical Company Polyester process using a pipe reactor
KR100426229B1 (ko) * 2001-01-05 2004-04-08 주식회사 엘지화학 폴리염화비닐 수지용 트리메틸올프로판 에스테르 가소제조성물
AT504727A1 (de) * 2002-04-12 2008-07-15 Energea Umwelttechnologie Gmbh Verfahren und anlage zur veresterung von fettsäuren
GB0320206D0 (en) * 2003-08-29 2003-10-01 Exxonmobil Chem Patents Inc Improvements in or relating to plasticiser
JP2006154384A (ja) * 2004-11-30 2006-06-15 Konica Minolta Opto Inc 位相差フィルム、及びそれを用いた偏光板、表示装置
JP2006182606A (ja) * 2004-12-28 2006-07-13 Miyoshi Oil & Fat Co Ltd セメント混和剤及びセメント組成物
CN1300092C (zh) * 2005-03-09 2007-02-14 贵州宏福实业开发有限总公司 多元醇脂肪酸酯的生产方法
US7919649B2 (en) * 2005-05-27 2011-04-05 Exxonmobile Chemical Patents Inc. Plasticiser esters
KR20080018961A (ko) * 2005-06-24 2008-02-28 헥시온 스페셜티 케미컬스 리서치 벨기에 에스.에이. 3차 알킬이 치환된 산을 이용한 폴리올의 에스테르화 방법
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US20080139780A1 (en) * 2006-12-07 2008-06-12 Debruin Bruce Roger Polyester production system employing short residence time esterification
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KR100919930B1 (ko) 2007-01-10 2009-10-07 주식회사 엘지화학 내이행성이 우수한 고분자 가소제, 이의 제조방법 및 이를포함하는 고분자 수지 조성물
US7892498B2 (en) 2007-03-08 2011-02-22 Eastman Chemical Company Polyester production system employing an unagitated esterification reactor
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KR101506046B1 (ko) * 2007-03-13 2015-03-25 엑손모빌 케미칼 패턴츠 인코포레이티드 회분식 에스터화
ATE482921T1 (de) * 2007-03-13 2010-10-15 Exxonmobil Chem Patents Inc Verfahren zur herstellung von estern
US8729289B2 (en) * 2007-03-13 2014-05-20 Exxonmobil Chemical Patents Inc. Ester production
US7829653B2 (en) 2007-07-12 2010-11-09 Eastman Chemical Company Horizontal trayed reactor
US7842777B2 (en) 2007-07-12 2010-11-30 Eastman Chemical Company Sloped tubular reactor with divided flow
US7858730B2 (en) * 2007-07-12 2010-12-28 Eastman Chemical Company Multi-level tubular reactor with dual headers
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DE102009048774A1 (de) 2009-10-08 2011-04-28 Oxea Deutschland Gmbh Verfahren zur Farbaufhellung von Polyolestern
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WO2011054782A1 (de) 2009-11-05 2011-05-12 Basf Se Kleb- und dichtstoffe enthaltend ester auf basis von 2-propylheptanol
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CN102958898B (zh) 2010-08-25 2015-05-20 埃克森美孚化学专利公司 酯的制备方法
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CN103130640B (zh) * 2013-01-16 2015-06-10 宁波东来化工有限公司 一种制备1,2-环己烷二甲酸二癸酯的装置及其方法
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DE102013018456B4 (de) 2013-11-02 2019-01-24 Oxea Gmbh Verfahren zur Gewinnung von mit Polyolestern angereicherten Produktströmen aus den Nebenströmen der Polyolesterherstellung
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PL3092266T3 (pl) 2014-01-09 2018-12-31 Basf Se Kompozycja plastyfikatora zawierająca pochodną furanu i ester kwasu 1,2-cykloheksanodikarboksylowego
DE102015207291A1 (de) 2014-04-24 2016-03-10 Basf Se Weichmacher-Zusammensetzung, die Furanderivate und 1,2-Cyclohexandicarbonsäureester enthält
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TWI706979B (zh) 2014-08-19 2020-10-11 德商巴斯夫歐洲公司 包含聚合二羧酸酯的塑化劑組成物
TWI686444B (zh) 2014-09-04 2020-03-01 德商巴斯夫歐洲公司 包含聚合二羧酸酯的塑化劑組成物
US10287417B2 (en) 2015-01-30 2019-05-14 Basf Se Plasticizer composition containing polymeric dicarboxylic acid esters and terephthalic acid dialkyl esters
CN106045857A (zh) * 2015-04-24 2016-10-26 中国科学院大连化学物理研究所 一种二环己基甲酸二元醇酯增塑剂的制备方法
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US20180282511A1 (en) 2015-09-30 2018-10-04 Basf Se Plasticizer composition containing polymeric dicarboxylic acid esters and terephthalic acid dialkyl esters
ES2743975T5 (es) 2015-09-30 2023-05-10 Basf Se Composición de plastificante que contiene ésteres de ácido dicarboxílico poliméricos y ésteres de ácido 1,2-diclohexandicarboxílico
US20180282510A1 (en) 2015-09-30 2018-10-04 Basf Se Plasticizer composition containing polymeric dicarboxylic acid esters and dicarboxylic acid diesters
CN105254501A (zh) * 2015-10-23 2016-01-20 淮阴师范学院 环己烷-1,2-二甲酸二异壬酯的制备方法
EP3178908A1 (en) 2015-12-11 2017-06-14 Basf Se The use of 2,5-furandicarboxylic acid esters as lubricants
PL3405518T3 (pl) 2016-01-20 2020-05-18 Basf Se Kompozycja plastyfikatora, która zawiera estry alifatycznych kwasów dikarboksylowych i diestry wybrane spośród estrów kwasu 1,2-cykloheksanodikarboksylowego i estrów kwasu tereftalowego
CA3018424A1 (en) 2016-03-23 2017-09-28 Basf Se Polymer composition containing a cycloalkyl alkyl dicarboxylic acid diester as a plasticizer
CN109563305A (zh) 2016-08-01 2019-04-02 巴斯夫欧洲公司 增塑剂组合物
WO2018024597A1 (de) 2016-08-01 2018-02-08 Basf Se Weichmacher-zusammensetzung
WO2018024591A1 (de) 2016-08-01 2018-02-08 Basf Se Weichmacher-zusammensetzung
EP3491054A1 (de) 2016-08-01 2019-06-05 Basf Se Weichmacher-zusammensetzung
KR102641380B1 (ko) * 2016-11-11 2024-02-28 오씨아이 주식회사 테레프탈산계 에스터 화합물을 정제하는 방법
WO2019185409A1 (de) 2018-03-29 2019-10-03 Basf Se Pvc-zusammensetzung, enthaltend wenigstens einen weichmacher der wenigstens eine carbonsäureestergruppe aufweist und wenigstens eine carbodiimidverbindung
EP3747860B1 (de) 2019-06-04 2023-07-26 Basf Se Neue weichmacher auf cyclohexanon-basis
KR102669652B1 (ko) 2019-09-19 2024-05-28 주식회사 엘지화학 에스터화 생성물의 중화/수분리 장치 및 에스터화 생성물의 중화/수분리 방법
KR102528326B1 (ko) * 2020-02-14 2023-05-02 한화솔루션 주식회사 에스테르계 화합물의 제조방법
KR20220067352A (ko) * 2020-11-17 2022-05-24 주식회사 엘지화학 디에스터계 물질의 제조방법
WO2024133359A1 (de) 2022-12-21 2024-06-27 Basf Se Weichmacher
WO2024133358A1 (de) 2022-12-21 2024-06-27 Basf Se Weichmacher-verbindung
WO2024153687A1 (de) 2023-01-19 2024-07-25 Basf Se Verfahren zur herstellung von 1,2-cyclohexandicarbonsäuredialkylestern

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Also Published As

Publication number Publication date
AU6032294A (en) 1994-08-15
AU675294B2 (en) 1997-01-30
EP0680463B1 (en) 1998-06-10
JPH08505879A (ja) 1996-06-25
BR9405659A (pt) 1995-11-14
SG48306A1 (en) 1998-04-17
CA2154153C (en) 2004-08-10
DE69410988D1 (de) 1998-07-16
DE69410988T3 (de) 2002-06-27
ES2119172T3 (es) 1998-10-01
US5324853A (en) 1994-06-28
CA2154153A1 (en) 1994-08-04
TW268940B (es) 1996-01-21
CN1118158A (zh) 1996-03-06
KR960700216A (ko) 1996-01-19
EP0680463B2 (en) 2001-12-19
DE69410988T2 (de) 1998-12-10
EP0680463A1 (en) 1995-11-08
CN1046265C (zh) 1999-11-10
WO1994017028A1 (en) 1994-08-04
MY110495A (en) 1998-06-30
KR100284475B1 (ko) 2001-04-02

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