ES2079967T3 - Procedimiento para la cristalizacion en un cristalizador de deflector y tubo de aspiracion. - Google Patents

Procedimiento para la cristalizacion en un cristalizador de deflector y tubo de aspiracion.

Info

Publication number
ES2079967T3
ES2079967T3 ES93905825T ES93905825T ES2079967T3 ES 2079967 T3 ES2079967 T3 ES 2079967T3 ES 93905825 T ES93905825 T ES 93905825T ES 93905825 T ES93905825 T ES 93905825T ES 2079967 T3 ES2079967 T3 ES 2079967T3
Authority
ES
Spain
Prior art keywords
crystals
crystallizer
deflector
crystallization
procedure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES93905825T
Other languages
English (en)
Inventor
Mo Kan Choi
Roger Hornberger
Roy Jeffrey Lilley Jr
Jeffrey E Neiman
Willie Woodrow Rhodes Jr
Charles Elmo Kline
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Honeywell International Inc
Original Assignee
AlliedSignal Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by AlliedSignal Inc filed Critical AlliedSignal Inc
Application granted granted Critical
Publication of ES2079967T3 publication Critical patent/ES2079967T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/24—Sulfates of ammonium
    • C01C1/248—Preventing coalescing or controlling form or size of the crystals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0018—Evaporation of components of the mixture to be separated
    • B01D9/0022—Evaporation of components of the mixture to be separated by reducing pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0018—Evaporation of components of the mixture to be separated
    • B01D9/0031—Evaporation of components of the mixture to be separated by heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0036—Crystallisation on to a bed of product crystals; Seeding

Landscapes

  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Glass Compositions (AREA)
  • Glanulating (AREA)
  • Fertilizers (AREA)
  • Peptides Or Proteins (AREA)

Abstract

EN UN PROCESO DE CRISTALIZACION CONTINUO EN EL QUE SE UTILIZA UN APARATO CRISTALIZADOR DE PANTALLA CON TUBOS DE ASPIRACION (DTB) EVAPORADOR PARA PRODUCIR UN PRODUCTO DE CRISTAL, LA MEJORA CONSISTE EN ALIMENTAR A UNA VELOCIDAD CONSTANTE EN EL CUERPO DE UNA LECHADA UNA SUSPENSION DE CRISTALES EN UNA SOLUCION A UNA TEMPERATURA NO SUPERIOR A LA TEMPERATURA DE TRABAJO DEL RECIPIENTE CRISTALIZADOR DE DTB, EN DONDE DICHA SUSPENSION DE CRISTALES CONTIENE UN SOLUTO Y DE UN 6 A UN 24% EN VOLUMEN, EN BASE AL VOLUMEN TOTAL DE LA SUSPENSION, DE CRISTALES EN DONDE AL MENOS UN 35% DE LOS CRISTALES TIENE UN TAMAÑO SUPERIOR A 14 RETICULOS (1,2 MM), EN UNA CANTIDAD EN QUE EL PESO DE CRISTALES ES DE UN 4 A UN 25 POR CIENTO EL PESO DEL PRODUCTO RETIRADO, CON LO QUE LOS CICLOS DE DISTRIBUCION POR TAMAÑO DE LAS PARTICULAS DEL PRODUCTO RETIRADO SE REDUCE Y AUMENTA LA VELOCIDAD DE PRODUCCION DE CRISTALES DE TAMAÑO GRANULAR.
ES93905825T 1992-03-27 1993-02-09 Procedimiento para la cristalizacion en un cristalizador de deflector y tubo de aspiracion. Expired - Lifetime ES2079967T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US85957592A 1992-03-27 1992-03-27

Publications (1)

Publication Number Publication Date
ES2079967T3 true ES2079967T3 (es) 1996-01-16

Family

ID=25331247

Family Applications (1)

Application Number Title Priority Date Filing Date
ES93905825T Expired - Lifetime ES2079967T3 (es) 1992-03-27 1993-02-09 Procedimiento para la cristalizacion en un cristalizador de deflector y tubo de aspiracion.

Country Status (6)

Country Link
EP (1) EP0632738B1 (es)
JP (1) JPH07505087A (es)
KR (1) KR950700778A (es)
DE (1) DE69300767T2 (es)
ES (1) ES2079967T3 (es)
WO (1) WO1993019826A1 (es)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE69818981D1 (de) * 1997-02-27 2003-11-20 Ajinomoto Kk Vorrichtung und verfahren zur kristallisation
NL1007846C2 (nl) * 1997-12-18 1999-06-21 Niro Process Technology Bv Werkwijze en inrichting voor het vriesconcentreren van stoffen.
DE19912699A1 (de) * 1999-03-20 2000-09-28 Domo Caproleuna Gmbh Verfahren zur Steuerung der Kristallgröße bei der kontinuierlichen Massenkristallisation
GR1003453B (el) * 1999-07-07 2000-10-12 ���������� ���������� �.�. Μεθοδος παραγωγης κοκκωδους θειικου αμμωνιου
DE10026619A1 (de) 2000-05-29 2001-12-06 Basf Ag Vorrichtung zur Herstellung von Kristallen
WO2005002703A1 (en) * 2003-07-03 2005-01-13 Dsm Ip Assets B.V. Process for separating granular size fertilizer crystals
WO2005002702A1 (en) * 2003-07-03 2005-01-13 Dsm Ip Assets B.V. Process for separating granular size crystals
US7615663B2 (en) 2004-09-02 2009-11-10 Eastman Chemical Company Optimized production of aromatic dicarboxylic acids
JP2009544562A (ja) * 2006-07-28 2009-12-17 ディーエスエム アイピー アセッツ ビー．ブイ． 大型結晶生成物の連続製造方法
FR2918575B1 (fr) * 2007-07-09 2009-08-28 Crystal Evap Consult Sarl Appareil de cristallisation a circulation forcee.
WO2009077346A1 (de) * 2007-12-14 2009-06-25 Gea Messo Gmbh Verfahren und vorrichtung zur herstellung eines grobkörnigen ammoniumsulfat-produktkristallisats
DE102008007155B4 (de) * 2008-02-01 2014-04-30 Gea Messo Gmbh Verfahren und Vorrichtung zur kontinuierlichen Herstellung eines grobkörnigen kristallinen Ammoniumsulfat-Produkts
DE102008007154B4 (de) * 2008-02-01 2014-03-20 Gea Messo Gmbh Verfahren zur Herstellung eines grobkörnigen Ammoniumsulfat-Produkts durch Kristllisation
DE102008029050A1 (de) 2008-06-18 2009-12-24 Gea Messo Gmbh Verfahren und Vorrichtung zur kontinuierlichen Herstellung eines Kristallisats mit konstanter Korngrößenverteilung
DE102008059754A1 (de) 2008-12-01 2010-06-02 Gea Messo Gmbh Verfahren zur Erzeugung eines grobkörnigen Ammoniumsulfat-Produkts
DE102009017097B4 (de) * 2009-04-15 2016-06-16 Air Liquide Global E&C Solutions Germany Gmbh Verfahren zur kontinuierlichen Behandlung einer Salz enthaltenden Lösung
US20110024354A1 (en) * 2009-07-30 2011-02-03 General Electric Company Desalination system and method
GB2489684A (en) * 2011-03-31 2012-10-10 Haifa Chemicals Ltd Crystallisation Apparatus
EP2794042B1 (en) 2011-12-22 2017-05-10 Dow Global Technologies LLC Process and apparatus for forced circulation evaporative crystallization with large deposit inventory
DE102012101702B4 (de) 2012-03-01 2017-10-05 Gea Messo Gmbh Verfahren zur Herstellung eines grobkörnigen Ammoniumsulfat-Produkts durch Kristallisation und Anlage zur Durchführung des Verfahrens
CN102614679B (zh) * 2012-03-19 2014-10-22 通辽梅花生物科技有限公司 一种连续结晶罐以及连续蒸发结晶工艺
US9676633B2 (en) 2012-09-24 2017-06-13 Cap Iii B.V. Process for preparing crystalline ammonium sulfate product
CN103073030B (zh) * 2013-02-01 2014-05-07 青海盐湖工业股份有限公司 一种用于水解光卤石的结晶器
DE202014010477U1 (de) 2014-04-16 2015-09-15 Gea Messo Gmbh Anlage zur Herstellung eines grobkörnigen Produktkristallisats
DE102015013959B4 (de) 2014-10-30 2022-05-05 Henning Meldau Verfahren und Vorrichtung zur Herstellung von Kristallen
CN117753042B (zh) * 2024-02-22 2024-05-14 瀚能(苏州)节能科技有限公司 布膜分液结构、板式降膜结晶系统及提纯方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2346517A (en) * 1940-10-04 1944-04-11 J D & A B Spreckels Company Method of crystallizing material
US3071447A (en) * 1958-09-09 1963-01-01 Whiting Corp Hydraulic classifier
US3628919A (en) * 1968-10-29 1971-12-21 Allied Chem Crystallization procedure for sodium carbonate precursor crystals
US3873275A (en) * 1969-09-29 1975-03-25 Whiting Corp Crystallization apparatus and method

Also Published As

Publication number Publication date
KR950700778A (ko) 1995-02-20
EP0632738B1 (en) 1995-11-08
EP0632738A1 (en) 1995-01-11
WO1993019826A1 (en) 1993-10-14
DE69300767D1 (de) 1995-12-14
JPH07505087A (ja) 1995-06-08
DE69300767T2 (de) 1996-04-25

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