EP3458415A4 - PREPARATION OF IODOSILANES CONTAINING SI-H VIA A HALOGENURE EXCHANGE REACTION - Google Patents

PREPARATION OF IODOSILANES CONTAINING SI-H VIA A HALOGENURE EXCHANGE REACTION Download PDF

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Publication number
EP3458415A4
EP3458415A4 EP17800276.2A EP17800276A EP3458415A4 EP 3458415 A4 EP3458415 A4 EP 3458415A4 EP 17800276 A EP17800276 A EP 17800276A EP 3458415 A4 EP3458415 A4 EP 3458415A4
Authority
EP
European Patent Office
Prior art keywords
preparation
exchange reaction
halide exchange
containing iodosilanes
via halide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
EP17800276.2A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP3458415A1 (en
Inventor
Cole RITTER
Gennadiy Itov
Manish Khandelwal
Jean-Marc Girard
Glenn KUCHENBEISER
Sean KERRIGAN
Peng Zhang
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Publication of EP3458415A1 publication Critical patent/EP3458415A1/en
Publication of EP3458415A4 publication Critical patent/EP3458415A4/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/08Compounds containing halogen
    • C01B33/107Halogenated silanes
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/12Organo silicon halides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/12Organo silicon halides
    • C07F7/121Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/123Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving the formation of Si-halogen linkages
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/30Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/30Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
    • C23C16/40Oxides
    • C23C16/401Oxides containing silicon
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/448Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/455Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
    • C23C16/45523Pulsed gas flow or change of composition over time
    • C23C16/45525Atomic layer deposition [ALD]
    • C23C16/45553Atomic layer deposition [ALD] characterized by the use of precursors specially adapted for ALD

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
EP17800276.2A 2016-05-19 2017-05-19 PREPARATION OF IODOSILANES CONTAINING SI-H VIA A HALOGENURE EXCHANGE REACTION Pending EP3458415A4 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201662338882P 2016-05-19 2016-05-19
PCT/US2017/033620 WO2017201456A1 (en) 2016-05-19 2017-05-19 Preparation of si-h containing iodosilanes via halide exchange reaction

Publications (2)

Publication Number Publication Date
EP3458415A1 EP3458415A1 (en) 2019-03-27
EP3458415A4 true EP3458415A4 (en) 2019-11-27

Family

ID=60326369

Family Applications (1)

Application Number Title Priority Date Filing Date
EP17800276.2A Pending EP3458415A4 (en) 2016-05-19 2017-05-19 PREPARATION OF IODOSILANES CONTAINING SI-H VIA A HALOGENURE EXCHANGE REACTION

Country Status (7)

Country Link
EP (1) EP3458415A4 (zh)
JP (2) JP6543354B2 (zh)
KR (1) KR102038215B1 (zh)
CN (1) CN107864649B (zh)
SG (1) SG11201709441TA (zh)
TW (1) TWI805561B (zh)
WO (1) WO2017201456A1 (zh)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10384944B2 (en) 2016-05-19 2019-08-20 L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Preparation of Si—H containing iodosilanes via halide exchange reaction
WO2019212808A1 (en) * 2018-05-01 2019-11-07 Milliken & Company Method for producing halosilane compounds
JP6688513B2 (ja) 2018-10-18 2020-04-28 ヤマナカヒューテック株式会社 ジヨードシランの製造方法
EP3894418B1 (en) * 2018-12-10 2023-09-27 Entegris, Inc. Preparation of triiodosilanes
CN115605432A (zh) * 2020-04-24 2023-01-13 恩特格里斯公司(Us) 制备碘硅烷的方法及由其所得的组合物
US11905174B2 (en) * 2020-10-23 2024-02-20 Entegris, Inc. Method for preparing iodosilanes
KR102331310B1 (ko) * 2020-11-12 2021-12-01 (주)엘케이켐 디아이오도실란의 제조 방법 및 이에 의해 제조된 조성물
CN113548669B (zh) * 2021-09-01 2022-11-11 福建福豆新材料有限公司 一种高纯电子级二碘硅烷的制备装置及其制备方法
JP2023157339A (ja) * 2022-04-14 2023-10-26 ヤマナカヒューテック株式会社 化合物の製造方法
CN116375038A (zh) * 2023-02-23 2023-07-04 安徽博泰电子材料有限公司 一种二碘硅烷的制备方法
CN116081626B (zh) * 2023-03-30 2023-06-27 研峰科技(北京)有限公司 一种二碘硅烷的制备方法

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DE3047995C2 (de) * 1980-12-19 1984-05-10 Degussa Ag, 6000 Frankfurt Verfahren zur Herstellung von (Jodorganyl)-alkoxysilanen
US5997637A (en) * 1993-06-18 1999-12-07 Nippon Oil Co., Ltd. Method of producing a semiconducting material
JPH07252271A (ja) * 1994-03-14 1995-10-03 Shin Etsu Chem Co Ltd ヨードシランの製造方法
JP3895053B2 (ja) * 1998-07-30 2007-03-22 独立行政法人科学技術振興機構 ジハロメチルシラン類の製法
US20060084283A1 (en) * 2004-10-20 2006-04-20 Paranjpe Ajit P Low temperature sin deposition methods
US20060121192A1 (en) 2004-12-02 2006-06-08 Jurcik Benjamin J Liquid precursor refill system
US9034105B2 (en) 2008-01-10 2015-05-19 American Air Liquide, Inc. Solid precursor sublimator
US20160046408A1 (en) 2015-10-27 2016-02-18 L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Internally coated vessel for housing a metal halide
US9777373B2 (en) * 2015-12-30 2017-10-03 American Air Liquide, Inc. Amino(iodo)silane precursors for ALD/CVD silicon-containing film applications and methods of using the same
US10106425B2 (en) 2016-05-19 2018-10-23 L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Synthesis methods for halosilanes

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
HASSLER K ET AL: "Synthese und Eigenschaften chlorierter und bromierter Aryltrisilane und Aryltetrasilane", JOURNAL OF ORGANOMETALLIC CHEMISTRY, ELSEVIER, AMSTERDAM, NL, vol. 538, no. 1-2, 20 June 1997 (1997-06-20), pages 135 - 143, XP004082229, ISSN: 0022-328X, DOI: 10.1016/S0022-328X(96)06893-3 *
KIM SOO ET AL: "Fourier-transform infrared spectroscopic studies of pristine polysilanes as precursor molecules for the solution deposition of amorphous silicon thin-films", SOLAR ENERGY MATERIALS AND SOLAR CELLS, vol. 100, 2012, pages 61 - 64, XP028902547, ISSN: 0927-0248, DOI: 10.1016/J.SOLMAT.2011.04.023 *
LISSEL MANFRED ET AL: "Ein einfaches Verfahren zur Herstellung von Iodotrimethylsilan", SYNTHESIS, vol. 1983, no. 6, 1 January 1983 (1983-01-01), pages 459, XP055595770 *
WANG Z ET AL: "Synthesis of monolithic 3D ordered macroporous carbon/nano-silicon composites by diiodosilane decomposition", CARBON, ELSEVIER, OXFORD, GB, vol. 46, no. 13, 1 November 2008 (2008-11-01), pages 1702 - 1710, XP025469434, ISSN: 0008-6223, [retrieved on 20080724], DOI: 10.1016/J.CARBON.2008.07.015 *

Also Published As

Publication number Publication date
EP3458415A1 (en) 2019-03-27
JP2019189523A (ja) 2019-10-31
TWI805561B (zh) 2023-06-21
WO2017201456A1 (en) 2017-11-23
JP2018519233A (ja) 2018-07-19
WO2017201456A8 (en) 2017-12-28
JP6543354B2 (ja) 2019-07-10
JP7014753B2 (ja) 2022-02-01
KR102038215B1 (ko) 2019-10-29
TW201900659A (zh) 2019-01-01
KR20170141261A (ko) 2017-12-22
CN107864649A (zh) 2018-03-30
SG11201709441TA (en) 2018-05-30
CN107864649B (zh) 2021-07-20

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Inventor name: ZHANG, PENG

Inventor name: RITTER, COLE

Inventor name: ITOV, GENNADIY

Inventor name: GIRARD, JEAN-MARC

Inventor name: KUCHENBEISER, GLENN

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Inventor name: KHANDELWAL, MANISH

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Owner name: L'AIR LIQUIDE, SOCIETE ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCEDES GEORGES CLAUDE