EP3266832B1 - Thermally decomposable binder - Google Patents

Thermally decomposable binder Download PDF

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Publication number
EP3266832B1
EP3266832B1 EP15883997.7A EP15883997A EP3266832B1 EP 3266832 B1 EP3266832 B1 EP 3266832B1 EP 15883997 A EP15883997 A EP 15883997A EP 3266832 B1 EP3266832 B1 EP 3266832B1
Authority
EP
European Patent Office
Prior art keywords
group
polycarbonate resin
aliphatic polycarbonate
carbon atoms
fine inorganic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
EP15883997.7A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP3266832A1 (en
EP3266832A4 (en
Inventor
Koji Nakano
Kiyoshi Nishioka
Masahiro Suzuki
Nobutaka Fujimoto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Seika Chemicals Co Ltd
Tokyo University of Agriculture and Technology NUC
Original Assignee
Sumitomo Seika Chemicals Co Ltd
Tokyo University of Agriculture and Technology NUC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Seika Chemicals Co Ltd, Tokyo University of Agriculture and Technology NUC filed Critical Sumitomo Seika Chemicals Co Ltd
Publication of EP3266832A1 publication Critical patent/EP3266832A1/en
Publication of EP3266832A4 publication Critical patent/EP3266832A4/en
Application granted granted Critical
Publication of EP3266832B1 publication Critical patent/EP3266832B1/en
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/02—Aliphatic polycarbonates
    • C08G64/0208—Aliphatic polycarbonates saturated
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/02—Aliphatic polycarbonates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/20—General preparatory processes
    • C08G64/32—General preparatory processes using carbon dioxide
    • C08G64/34—General preparatory processes using carbon dioxide and cyclic ethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/42—Chemical after-treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/01—Use of inorganic substances as compounding ingredients characterized by their specific function
    • C08K3/013—Fillers, pigments or reinforcing additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/02—Elements
    • C08K3/08—Metals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L69/00—Compositions of polycarbonates; Compositions of derivatives of polycarbonates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/02—Elements
    • C08K3/08—Metals
    • C08K2003/0806—Silver

Definitions

  • a reaction solvent may be optionally used.
  • the reaction solvent is not particularly limited, and various organic solvents can be used.
  • the organic solvent includes aliphatic hydrocarbon-based solvents such as pentane, hexane, octane, decane, and cyclohexane; aromatic hydrocarbon-based solvents such as benzene, toluene, and xylene; halogenated hydrocarbon-based solvents such as methylene chloride, chloroform, carbon tetrachloride, 1,1-dichloroethane, 1,2-dichloroethane, ethyl chloride, trichloroethane, 1-chloropropane, 2-chloropropane, 1-chlorobutane, 2-chlorobutane, 1-chloro-2-methylpropane, chlorobenzene, and bromobenzene; ether-based solvents such as dimethoxyethane, tetrahydr
  • the aliphatic polycarbonate resin of the present invention has a mass loss percentage after keeping at 160°C for 1 hour in a thermogravimetric analysis measurement is preferably 90% or more, more preferably 95% or more, and even more preferably 99% or more, and the mass loss percentage after keeping at 100°C for 1 hour is preferably 5% or less, more preferably 3% or less, and even more preferably 1% or less, from the viewpoint of inhibiting the decomposition during the process before the thermal decomposition step.
  • the thermal decomposition temperature can be adjusted by a content of the constituting unit represented by the formula (1).
  • the content of the constituting unit represented by the formula (1) in the aliphatic polycarbonate resin of the present invention in the entire constituting units constituting the aliphatic polycarbonate resin is preferably 30% by mol or less, more preferably 20% by mol or less, and even more preferably 10% by mol or less, from the viewpoint of reducing the residual carbon after thermal decomposition, and the content is preferably 0.001% by mol or more, more preferably 0.1% by mol or more, even more preferably 0.5% by mol or more, even more preferably 1.0% by mol or more, from the viewpoint of lowering a decomposition temperature.
  • the content of the constituting unit represented by the formula (1) in the entire monomer units constituting the aliphatic polycarbonate resin contained in the thermally decomposable binder and the fine inorganic particle-dispersed paste composition is within the range described as the content of the constituting unit represented by the formula (1) in the aliphatic polycarbonate resin of the present invention.
  • the electroconductive particles include, for example, metal particles made of copper, iron, nickel, palladium, platinum, gold, silver, aluminum, tungsten, alloys thereof, and the like.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
EP15883997.7A 2015-03-02 2015-09-02 Thermally decomposable binder Active EP3266832B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2015040238 2015-03-02
PCT/JP2015/074937 WO2016139831A1 (ja) 2015-03-02 2015-09-02 熱分解性バインダー

Publications (3)

Publication Number Publication Date
EP3266832A1 EP3266832A1 (en) 2018-01-10
EP3266832A4 EP3266832A4 (en) 2018-08-29
EP3266832B1 true EP3266832B1 (en) 2020-02-26

Family

ID=56848071

Family Applications (1)

Application Number Title Priority Date Filing Date
EP15883997.7A Active EP3266832B1 (en) 2015-03-02 2015-09-02 Thermally decomposable binder

Country Status (8)

Country Link
US (1) US10759901B2 (ja)
EP (1) EP3266832B1 (ja)
JP (1) JP6646036B2 (ja)
KR (1) KR102270299B1 (ja)
CN (1) CN107406666B (ja)
ES (1) ES2790656T3 (ja)
TW (1) TWI664258B (ja)
WO (1) WO2016139831A1 (ja)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10759901B2 (en) 2015-03-02 2020-09-01 National University Corporation Tokyo University Of Agriculture And Technology Thermally decomposable binder
JP6704322B2 (ja) * 2015-09-30 2020-06-03 日東電工株式会社 シートおよび複合シート
JP2017066485A (ja) * 2015-09-30 2017-04-06 日東電工株式会社 シートおよび複合シート
JP6967839B2 (ja) * 2016-03-23 2021-11-17 日東電工株式会社 加熱接合用シート、ダイシングテープ付き加熱接合用シート、及び、接合体の製造方法、パワー半導体装置
WO2017170079A1 (ja) 2016-04-01 2017-10-05 国立大学法人東京農工大学 熱分解性バインダー
EP3483198A4 (en) 2016-07-08 2020-01-08 National University Corporation Tokyo University of Agriculture and Technology NOVEL ALIPHATIC POLYCARBONATE AND BINDING RESIN COMPOSITION CONTAINING SAID POLYCARBONATE
JP2019043975A (ja) * 2017-08-29 2019-03-22 住友化学株式会社 コアシェル型粒子
TW202037634A (zh) * 2019-01-24 2020-10-16 日商住友精化股份有限公司 脂肪族聚碳酸酯
WO2023190951A1 (ja) * 2022-03-31 2023-10-05 リンテック株式会社 加熱加圧用フィルム状焼成材料、及び半導体デバイスの製造方法
WO2023190950A1 (ja) * 2022-03-31 2023-10-05 リンテック株式会社 積層体の製造方法

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WO2005105875A1 (en) 2004-04-30 2005-11-10 Polymers Australia Pty Limited Photochromic compositions and articles comprising siloxane, alkylene or substituted alkylene oligomers
JP4997461B2 (ja) 2007-05-16 2012-08-08 学校法人東京理科大学 ポリカーボネートの製造方法及びポリカーボネート
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JP5664875B2 (ja) * 2010-01-22 2015-02-04 荒川化学工業株式会社 易熱分解性バインダー樹脂、バインダー樹脂組成物および該組成物の用途
EP2536777B1 (de) * 2010-02-18 2016-04-20 Basf Se Polymerdispersion, die ein hochverzweigtes polycarbonat mit ungesättigten fettsäuregruppen enthält
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US10759901B2 (en) 2015-03-02 2020-09-01 National University Corporation Tokyo University Of Agriculture And Technology Thermally decomposable binder
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Also Published As

Publication number Publication date
CN107406666B (zh) 2020-02-21
ES2790656T3 (es) 2020-10-28
US10759901B2 (en) 2020-09-01
CN107406666A (zh) 2017-11-28
US20180030203A1 (en) 2018-02-01
EP3266832A1 (en) 2018-01-10
KR20170125871A (ko) 2017-11-15
WO2016139831A1 (ja) 2016-09-09
EP3266832A4 (en) 2018-08-29
TWI664258B (zh) 2019-07-01
TW201632601A (zh) 2016-09-16
JPWO2016139831A1 (ja) 2017-12-14
KR102270299B1 (ko) 2021-06-28
JP6646036B2 (ja) 2020-02-14

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