EP2285728B1 - Dispositif pour remplir des contenants - Google Patents
Dispositif pour remplir des contenants Download PDFInfo
- Publication number
- EP2285728B1 EP2285728B1 EP09765506A EP09765506A EP2285728B1 EP 2285728 B1 EP2285728 B1 EP 2285728B1 EP 09765506 A EP09765506 A EP 09765506A EP 09765506 A EP09765506 A EP 09765506A EP 2285728 B1 EP2285728 B1 EP 2285728B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- dosing
- valve
- flow path
- diaphragm
- filling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/02—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
- B67C3/22—Details
- B67C3/26—Filling-heads; Means for engaging filling-heads with bottle necks
- B67C3/2608—Filling-heads; Means for engaging filling-heads with bottle necks comprising anti-dripping means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B3/00—Packaging plastic material, semiliquids, liquids or mixed solids and liquids, in individual containers or receptacles, e.g. bags, sacks, boxes, cartons, cans, or jars
- B65B3/02—Machines characterised by the incorporation of means for making the containers or receptacles
- B65B3/022—Making containers by moulding of a thermoplastic material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B3/00—Packaging plastic material, semiliquids, liquids or mixed solids and liquids, in individual containers or receptacles, e.g. bags, sacks, boxes, cartons, cans, or jars
- B65B3/26—Methods or devices for controlling the quantity of the material fed or filled
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B2210/00—Specific aspects of the packaging machine
- B65B2210/06—Sterilising or cleaning machinery or conduits
Definitions
- the invention relates to a device for filling containers, with a device for supplying filling material to at least one metering device, which forms a flow path in which a dosing valve which can be opened at least for the period of metering operations is arranged, in order to supply metered quantities of the contents via at least one filling line dispensing containers in question, wherein the metering device in the flow path downstream of the metering valve has a device for selectively generating a suction effect on the flow path, and wherein a control device is provided which activates the suction effect generating device in dependence on each completed by closing the metering metering operations.
- Such a device is off US 5,193,593 known.
- a container is filled with a liquid such that a metering device as an elongated annular nozzle with a flow path for the supply of a liquid to a container with a plurality of screens and a suction effect generating device in these screens.
- the nozzle is introduced into a container to the bottom and moved during filling of the container with a liquid upwards so that the nozzle tip is always located above the liquid level.
- the soaking device is activated to remove liquid from the area of the sieves.
- bottelpack® which enables an automated molding (blowing or vacuum forming), filling and closing of containers in an economical manner.
- bottelpack® enables an automated molding (blowing or vacuum forming), filling and closing of containers in an economical manner.
- the international standard for aseptic packaging must be met, and on the other hand it must be ensured that a certain dosage is filled in each filling process, with the highest possible accuracy of the filling quantity is, especially when it comes to highly effective pharmaceuticals.
- the invention has the object to provide a device of the type considered, which is distinguished from the prior art by increased dosing accuracy.
- a significant feature of the invention is that between the metering valve and the filling line, the flow path during metering narrowing throttle point is present, wherein in the region of the throttle point, a movable, in dependence on its position adjustment, the width of the flow path defining control member is present, which is on activation of the suction effect generating device in a flow path at the throttle point by forming a bypass expanding position can be transferred.
- the throttle point which determines the metering in conjunction with the timing of the opening time of the metering, forms in conjunction with the width of the flow path defining control member also part of the suction effect generating device, whose operating principle is that the movable control member as an extension in the flow path Bypass forms the throttle point, resulting in an increase in the clear volume of the flow path and thus results in a Nachström bin.
- a controllable means is provided by means of which at the end of each metering, namely when closing a respective metering valve, at the flow path a suction effect can be generated, created at the end of the dosing in the filling line, a suction effect, a sucking back of residual liquid causes the filling or at least prevents dripping of liquid. In any case, a maximum of dosing accuracy can be achieved.
- the arrangement may in this case be such that the suction effect generating means is formed by a bypass valve in the manner of a diaphragm valve, the movable control member forming membrane bounded with its one closing side of the flow path at the throttle point and at the other control side for the generation of the suction effect a negative pressure can be applied to leave the membrane to the flow path expanding deflection movement, the hub generates the suction effect on the filling line.
- the suction effect generating device is characterized by a particularly simple construction.
- the metering valve can also be formed by a diaphragm valve.
- metering valve and downstream bypass valve are diaphragm valves which are controlled by a common membrane extending along the flow path.
- the arrangement can advantageously be made such that for a plurality of filling lines respectively associated dosing units are combined in a dosing, wherein the input sides of the respective metering valves with a common, under discontinuous buffer pressure Medgutverteiler are in communication.
- the membrane at the bypass valves from a common control line can be jointly controlled, while for the control sides of the diaphragm to the metering valves for each filling line each have their own control line for pressure and vacuum are provided.
- the device comprises a plurality of metering devices, namely as shown in FIG Fig. 1 contains fifteen metering devices 5, which are combined in a common metering block 1.
- each of the metering devices 5 receives within the metering block 1, the filling liquid via a supply line 7, of which Fig. 1 only a few are numbered.
- the metering devices 5 each deliver the metered quantities to an associated filling line 9 (in FIG Fig. 1 also not all quantified).
- Each filling line 9 leads to an in Fig. 1 Not shown apparatus for producing and filling containers, such as a device according to the known bottelpack® system.
- each of these devices has a Guanguar 1 11, at its end in the Fig. Top end a supply head 13 is provided for the supply of channels in the Artdorn 11 with media.
- a respective filling line 9 with a Biharmonic nail 11 centrally extending Gresman 15 in connection As can be seen from this figure, each of these devices has a Gudorn 11, at its end in the Fig. Top end a supply head 13 is provided for the supply of channels in the Artdorn 11 with media.
- Fig. 3 shows, at the supply head 13 a respective filling line 9 with a Bidorn 11 centrally extending Bigutkanal 15 in connection.
- the metered via the respective filling lines 9 supplied contents occurs at the bottom, filling needle-like end 17 of the Rantelpack® system for filling a respective container 19, in a mold 21 in the manner of the mentioned bottelpack® system is formed from a plastic tube 23 which is produced by means of an extruder head 25 made of plasticized plastic material.
- Fig. 2 and 4 Further details of the summarized in Dosierblock 1 metering units 5 are off Fig. 2 and 4 seen.
- two valves are connected in series, namely an upstream metering valve 29 and a bypass valve located downstream 31 on a running between feed line 7 and filling line 9, two valves.
- Both valves are diaphragm valves with a pneumatically controlled for deflection and return movements membrane 33rd Die
- membrane 33 is common to both valves 29 and 31 of a metering device 5, as well as all, in Dosierblock 1 containing metering devices 5 together, that is, the membrane 33 extends over the length range of the dosing.
- Each metering valve 29 has its own pneumatic connection 35 for an individual admission of the control side 37 to the respective metering valve 29 with pressure or negative pressure.
- Fig. 1 not all of the pneumatic connections 35 are numbered.
- the bypass valves 31 all have a common pneumatic connection 39 to pressurize the control side 37 of the diaphragm 33 at the respective bypass valve 21 with pressure or negative pressure.
- Fig. 4a to 4d The functioning of the metering devices 5 is best Fig. 4a to 4d seen.
- located on the metering valve 29 and bypass valve 31 on the control side 37 of the membrane 33 each have a kugelkalottenartiger space 43 into which a surface region of the diaphragm 33 is deflected when applied via the pneumatic connections 35 or 39 negative pressure on the control side 37, whereby the opposite closing side 45 of the diaphragm 33 is lifted from the closed position and deflected into the respective space 43, which causes the opening of the relevant valve 29 or 31.
- Fig. 4a shows the metering valve 29 in the closed position, while the bypass valve 31 is open.
- Fig. 4b shows the metering valve 29 is opened while the bypass valve 31 is closed.
- Fig. 4a shows the metering valve 29 in the closed position, while the bypass valve 31 is open.
- Fig. 4b shows the metering valve 29 is opened while the bypass valve 31 is closed.
- FIG. 4c shows both valves 29 and 31 in the closed position, while Fig. 4d in turn, the metering valve 29 is closed and the bypass valve 31 is open.
- Fig. 4a shows the rest position of the device before a respective dosing, wherein the metering valve 29 is still closed, while the bypass valve 31 is in the open position.
- Fig. 4b illustrates the metering process, in which the metering valve 29 is opened, while the bypass valve 31 is closed, so that the passage size of the throttle point 41 in conjunction with the timed opening duration of the metering valve 29 determines the metered amount.
- Fig. 4c and 4d illustrate the completion of a dosing by closing the metering valve 29 ( Fig. 4c ).
- the bypass valve 31 is opened.
- the corresponding deflection movement of the diaphragm 33 into the dome-like space 43 leads to a substantial widening of the flow path 27 at the bypass valve 31.
- This stroke movement of the diaphragm 33 generates a suction effect when the dosing valve 29 is closed, causing a subsequent sucking of liquid from the downstream filling line 9 comes.
- the determination of the metered amount is carried out by timing the opening duration of the respective metering valve 29 via the Individual pneumatic connection 35.
- the generation of the suction effect on the filling lines 9 can be carried out simultaneously for all metering devices 5 by controlling the pneumatic connection 39 common to them.
- the metering valves 29 and the bypass valves 31 are controlled in the open position.
- the unthrottled flow path 27 is available for the passage of cleaning and sterilizing media, ie starting from the product distributor 3, via supply line 7, metering device 5, filling line 9 to the product channel 15 of a respective filling mandrel 11.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Basic Packing Technique (AREA)
- Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)
- External Artificial Organs (AREA)
Claims (9)
- Système de remplissage de récipients, comprenant un dispositif (7) pour apporter du produit de remplissage à au moins un dispositif (5) de dosage, qui forme un trajet (27) d'écoulement, dans lequel est montée au moins une vanne (29) de dosage pouvant s'ouvrir pendant le laps de temps d'opérations de dosage afin de céder des quantités de dosage du produit de remplissage aux récipients (19) concernés, par l'intermédiaire d'au moins un conduit (9) de remplissage, le dispositif (5) de dosage ayant, dans le trajet (27) d'écoulement en aval de la vanne (29) de dosage, un dispositif (31, 33, 43) de production au choix d'un effet de succion sur le trajet (27) d'écoulement et dans lequel il est prévu un dispositif (39) de commande, qui active le dispositif (31, 33, 43) produisant l'effet de succion en fonction d'opérations de dosage terminées respectivement par une fermeture de la vanne (29) de dosage, caractérisé en ce qu'il y a, entre la vanne (29) de dosage et le conduit (9) de remplissage, un étranglement (41) rétrécissant le trajet (27) d'écoulement pendant des opérations de dosage et en ce qu'il y a dans la région de l'étranglement (41) un organe (33) de commande mobile et définissant la largeur du trajet (27) d'écoulement en fonction de son réglage de position, qui, lors de l'activation du dispositif (31, 33, 43) produisant l'effet de succion, peut être mis en une position élargissant le trajet (27) d'écoulement à l'étranglement (41) par formation d'une dérivation.
- Système suivant la revendication 1, caractérisé en ce que le dispositif produisant l'effet de succion comporte une vanne (31) de dérivation à la manière d'une vanne à membrane, dont la membrane (33) formant l'organe de commande mobile délimite par sa face (45) de fermeture le trajet (27) d'écoulement à l'étranglement (41) et une dépression pour l'obtention de l'effet de succion peut être appliquée à l'autre face (37) de commande, pour faire que la membrane (33) soit déviée en élargissant le trajet (27) d'écoulement, dont la course produit l'effet de succion au conduit (9) de remplissage.
- Système suivant la revendication 2, caractérisé en ce que la vanne (29) de dosage est formée par une vanne à membrane.
- Système suivant la revendication 3, caractérisé en ce que la vanne (29) de dosage et la vanne (31) de dérivation en aval sont des vannes à membrane, qui sont commandées par une membrane (33) commune s'étendant le long du trajet (27) d'écoulement.
- Système suivant la revendication 4, caractérisé en ce que, sur la face (37) de commande opposée à la face (45) de fermeture de la membrane (33), peuvent être appliquées, à la vanne (29) de dosage concernée et à la vanne (31) de dérivation par des conduits (35, 39) de commande associés, au choix une surpression comme pression de fermeture et une dépression comme pression d'ouverture.
- Système suivant l'une des revendications 1 à 5, caractérisé en ce que, pour une pluralité de conduits (9) de remplissage, des dispositifs (5) de dosage, associés respectivement, sont rassemblés en un bloc (1) de dosage, les côtés entrée des vannes (19) respectives de dosage étant en liaison avec un répartiteur (3) commun de produit de remplissage se trouvant sous une pression tampon réglée.
- Système suivant la revendication 6, caractérisé en ce qu'il est prévu dans le bloc (1) de dosage une membrane (33) commune à l'ensemble des dispositifs (5) de dosage et associée aux vannes (29) de dosage et aux vannes (31) de dérivation.
- Système suivant la revendication 7, caractérisé en ce que, pour la face (37) de commande de la membrane (33), il est prévu sur les vannes (29) de dosage pour chaque conduit (9) de remplissage respectivement son propre conduit (35) de commande pour la pression et la dépression.
- Système suivant la revendication 8, caractérisé en ce qu'à la face (37) de commande de la membrane (33) est associé, sur les vannes (31) de dérivation en tant que dispositif de commande, un conduit (39) commun, par lequel peut être appliquée la dépression pour l'activation simultanée des dispositifs respectifs produisant l'effet de succion.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL09765506T PL2285728T3 (pl) | 2008-06-17 | 2009-05-26 | Instalacja do napełniania pojemników |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102008028772A DE102008028772A1 (de) | 2008-06-17 | 2008-06-17 | Vorrichtung zum Befüllen von Behältnissen |
PCT/EP2009/003706 WO2009152926A1 (fr) | 2008-06-17 | 2009-05-26 | Dispositif pour remplir des contenants |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2285728A1 EP2285728A1 (fr) | 2011-02-23 |
EP2285728B1 true EP2285728B1 (fr) | 2011-10-26 |
Family
ID=40933837
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP09765506A Active EP2285728B1 (fr) | 2008-06-17 | 2009-05-26 | Dispositif pour remplir des contenants |
Country Status (17)
Country | Link |
---|---|
US (1) | US8602070B2 (fr) |
EP (1) | EP2285728B1 (fr) |
JP (1) | JP5571658B2 (fr) |
KR (1) | KR101572015B1 (fr) |
CN (1) | CN102056836B (fr) |
AT (1) | ATE530492T1 (fr) |
AU (1) | AU2009259770B2 (fr) |
BR (1) | BRPI0913373B1 (fr) |
CA (1) | CA2725850C (fr) |
DE (1) | DE102008028772A1 (fr) |
ES (1) | ES2373525T3 (fr) |
HK (1) | HK1153182A1 (fr) |
MX (1) | MX2010014167A (fr) |
PL (1) | PL2285728T3 (fr) |
PT (1) | PT2285728E (fr) |
RU (1) | RU2503597C2 (fr) |
WO (1) | WO2009152926A1 (fr) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE202012003948U1 (de) | 2012-04-20 | 2012-05-15 | Bürkert Werke GmbH | Pneumatische Dosiereinheit sowie pneumatische Dosiersystem |
DE102012108526A1 (de) * | 2012-09-12 | 2014-03-13 | Krones Ag | Vorrichtung und Verfahren zum Befüllen eines Behälters mit einem Füllprodukt |
DE202013103016U1 (de) * | 2013-07-08 | 2013-07-15 | Bürkert Werke GmbH | Mikrofluiddosiereinheit und Testvorrichtung für Biomaterial |
DE102015007690A1 (de) | 2015-06-11 | 2016-12-15 | Kocher-Plastik Maschinenbau Gmbh | Verfahren zum Herstellen eines befüllten und geschlossenen Behälters sowie Vorrichtung zum Durchführen des Verfahrens und ein danach hergestellter Behälter |
DE102017008802A1 (de) | 2017-09-20 | 2019-03-21 | Kocher-Plastik Maschinenbau Gmbh | Vorrichtung zum Herstellen und Befüllen von Behältern |
CN108150672A (zh) * | 2017-12-08 | 2018-06-12 | 北京大学 | 截止阀 |
CN108773823A (zh) * | 2018-07-25 | 2018-11-09 | 上海位山科技有限公司 | 一种回吸功能的膜片式灌装阀 |
CN109625364B (zh) * | 2018-12-03 | 2020-12-01 | 佛山科学技术学院 | 一种定量供水装置 |
CN113929041B (zh) * | 2021-09-27 | 2022-12-27 | 东富龙科技集团股份有限公司 | 一种适用于吹灌封一体机的容器灌装机构 |
ES2940738B2 (es) * | 2021-11-10 | 2023-09-12 | Decam Tech Solutions 2000 S L | Sistema antigoteo de boquilla con membrana |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
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DE1657206A1 (de) * | 1968-01-03 | 1971-01-07 | Gerhard Hansen | Verfahren und Vorrichtung zum Fuellen einer nach aussen abgeschlossenen Kammer |
DE2107647A1 (de) * | 1971-02-17 | 1972-09-07 | Gebr. Netzsch, Maschinenfabrik, 8672 Selb | Vorrichtung zum Verhindern des Nachtropfens bei einer Abfüllanlage |
DE2528975A1 (de) * | 1975-06-28 | 1977-01-13 | Gundermann Unionpack | Vorrichtung zum gleichzeitigen dosierten fuellen von klein- und kleinstpackungen |
JPS5474526A (en) * | 1977-11-28 | 1979-06-14 | Yutaka Seimitsu Kogyo Ltd | Diaphragm system fluid change over valve |
US4394945A (en) * | 1981-08-06 | 1983-07-26 | Loctite Corporation | Valve having suck-back feature |
NL8302358A (nl) * | 1983-07-01 | 1985-02-01 | Tebel Maschf Bv | Inrichting voor ladingsgewijs doseren van een afgepaste volumehoeveelheid van een onder persdruk continu aan de inrichting toegevoerd stromend medium. |
DE3430721A1 (de) * | 1984-08-21 | 1986-03-06 | Alldos Eichler Kg, 7507 Pfinztal | Membranpumpe, insbesondere zum dosieren von fluessigkeiten |
US5016687A (en) * | 1989-06-15 | 1991-05-21 | Shikoku Kakoki Co., Ltd. | Device for preventing liquid from dripping from filling nozzle of liquid filling machine |
DE3919913C1 (fr) * | 1989-06-19 | 1990-04-26 | Benz & Hilgers Gmbh, 4000 Duesseldorf, De | |
DE3921791C1 (fr) * | 1989-07-03 | 1990-05-31 | Hassia Verpackungsmaschinen Gmbh, 6479 Ranstadt, De | |
US4997014A (en) | 1989-09-14 | 1991-03-05 | Automatic Liquid Packaging, Inc. | Fill nozzle assembly |
US5255720A (en) * | 1990-04-03 | 1993-10-26 | Mcpherson Dripless Systems Co., Inc. | Method and apparatus for dripless filling of containers |
US5193593A (en) * | 1990-08-13 | 1993-03-16 | Colgate-Palmolive Company | Package filling method and apparatus |
JP3454875B2 (ja) * | 1993-08-11 | 2003-10-06 | 澁谷工業株式会社 | 液体充填機 |
EP0997643B1 (fr) * | 1998-09-25 | 2006-07-12 | ALLDOS Eichler GmbH | Pompe doseuse à membrane |
DE19913689A1 (de) * | 1999-03-25 | 2000-09-28 | Focke & Co | Vorrichtung zur Steuerung strömender Medien |
JP2001031195A (ja) * | 1999-07-16 | 2001-02-06 | Hitachi Zosen Corp | ダイヤフラム式液体充填装置 |
JP2001031197A (ja) * | 1999-07-22 | 2001-02-06 | Hitachi Zosen Corp | 液面規制型充填装置 |
CN2492548Y (zh) * | 2001-06-04 | 2002-05-22 | 邹利生 | 一种用于活塞式灌装机的灌装阀 |
JP4035728B2 (ja) * | 2003-07-07 | 2008-01-23 | Smc株式会社 | サックバックバルブ |
JP2006010038A (ja) * | 2004-06-29 | 2006-01-12 | Smc Corp | サックバックバルブ |
-
2008
- 2008-06-17 DE DE102008028772A patent/DE102008028772A1/de not_active Withdrawn
-
2009
- 2009-05-26 WO PCT/EP2009/003706 patent/WO2009152926A1/fr active Application Filing
- 2009-05-26 US US12/736,594 patent/US8602070B2/en active Active
- 2009-05-26 CA CA2725850A patent/CA2725850C/fr active Active
- 2009-05-26 BR BRPI0913373-9A patent/BRPI0913373B1/pt active IP Right Grant
- 2009-05-26 PT PT09765506T patent/PT2285728E/pt unknown
- 2009-05-26 AU AU2009259770A patent/AU2009259770B2/en active Active
- 2009-05-26 JP JP2011513900A patent/JP5571658B2/ja active Active
- 2009-05-26 CN CN2009801209806A patent/CN102056836B/zh active Active
- 2009-05-26 ES ES09765506T patent/ES2373525T3/es active Active
- 2009-05-26 RU RU2010153047/12A patent/RU2503597C2/ru active
- 2009-05-26 EP EP09765506A patent/EP2285728B1/fr active Active
- 2009-05-26 AT AT09765506T patent/ATE530492T1/de active
- 2009-05-26 PL PL09765506T patent/PL2285728T3/pl unknown
- 2009-05-26 MX MX2010014167A patent/MX2010014167A/es active IP Right Grant
- 2009-05-26 KR KR1020107027351A patent/KR101572015B1/ko active IP Right Grant
-
2011
- 2011-07-13 HK HK11107269.6A patent/HK1153182A1/xx not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
DE102008028772A1 (de) | 2009-12-24 |
ATE530492T1 (de) | 2011-11-15 |
KR101572015B1 (ko) | 2015-11-26 |
PT2285728E (pt) | 2011-11-15 |
EP2285728A1 (fr) | 2011-02-23 |
CN102056836B (zh) | 2012-10-31 |
ES2373525T3 (es) | 2012-02-06 |
US20120018038A1 (en) | 2012-01-26 |
CN102056836A (zh) | 2011-05-11 |
AU2009259770A1 (en) | 2009-12-23 |
HK1153182A1 (en) | 2012-03-23 |
PL2285728T3 (pl) | 2012-03-30 |
WO2009152926A1 (fr) | 2009-12-23 |
US8602070B2 (en) | 2013-12-10 |
JP5571658B2 (ja) | 2014-08-13 |
BRPI0913373B1 (pt) | 2019-06-18 |
JP2011524312A (ja) | 2011-09-01 |
RU2010153047A (ru) | 2012-07-27 |
CA2725850A1 (fr) | 2009-12-23 |
AU2009259770B2 (en) | 2014-01-09 |
CA2725850C (fr) | 2015-01-27 |
MX2010014167A (es) | 2011-02-21 |
KR20110025173A (ko) | 2011-03-09 |
RU2503597C2 (ru) | 2014-01-10 |
BRPI0913373A2 (pt) | 2015-11-24 |
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