EP1547772B2 - Procédé d'impression pour réaliser des surfaces mates et brillantes - Google Patents

Procédé d'impression pour réaliser des surfaces mates et brillantes Download PDF

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Publication number
EP1547772B2
EP1547772B2 EP04106770A EP04106770A EP1547772B2 EP 1547772 B2 EP1547772 B2 EP 1547772B2 EP 04106770 A EP04106770 A EP 04106770A EP 04106770 A EP04106770 A EP 04106770A EP 1547772 B2 EP1547772 B2 EP 1547772B2
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Prior art keywords
varnish
printing
printed
glossy
percent
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EP04106770A
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German (de)
English (en)
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EP1547772A1 (fr
EP1547772B1 (fr
Inventor
Rolf Thal
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Heidelberger Druckmaschinen AG
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Heidelberger Druckmaschinen AG
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Priority claimed from DE2003160050 external-priority patent/DE10360050B3/de
Application filed by Heidelberger Druckmaschinen AG filed Critical Heidelberger Druckmaschinen AG
Priority to PL04106770T priority Critical patent/PL1547772T5/pl
Publication of EP1547772A1 publication Critical patent/EP1547772A1/fr
Publication of EP1547772B1 publication Critical patent/EP1547772B1/fr
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M7/00—After-treatment of prints, e.g. heating, irradiating, setting of the ink, protection of the printed stock
    • B41M7/02—Dusting, e.g. with an anti-offset powder for obtaining raised printing such as by thermogravure ; Varnishing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41F—PRINTING MACHINES OR PRESSES
    • B41F23/00—Devices for treating the surfaces of sheets, webs, or other articles in connection with printing
    • B41F23/08—Print finishing devices, e.g. for glossing prints

Definitions

  • the invention relates to a printing method, in particular a sheet-fed offset printing method in which a substrate after printing by spot coating with transparent paints or overprinting with a matting agent-containing paint on a part of the previously printed area with a matte surface and on another part of the printed area provided with a glossy surface. Due to the different surface texture and the contrast between adjacent matte and glossy faces, for example, different colors of the printed image stand out from each other, give the matt lacquered faces a velvety appearance or the glossy painted faces a reflective, silvery or golden appearance or other appealing visual Achieve effects.
  • the invention further relates to a printed product produced by an offset printing process.
  • the substrate is printed in the first pass in the printing units of the printing press with the desired inks and coated in a downstream coating unit of the printing press either in the area of the later glossy surfaces with a gloss varnish or in the later matte surfaces with a matt varnish, while each remain spared other areas and painted only during the second pass through the printing press.
  • this process in which the second coating application takes place on the already dried printing ink, has three significant disadvantages. First, two passes through the press are required, making the print more expensive.
  • a device for producing spot finishes on substrates in a large-format printing machine is already known, with which the substrate is coated in two of four printing units of the printing press with a so-called hybrid or UV color system, which is cured by irradiation with UV light before the substrate is printed in the two subsequent printing units with a typical oil-based offset printing ink system and finally coated in a subsequent coating tower or coating unit over the entire surface with a colorless paint that is absorbed to different degrees by the two color systems or otherwise chemically or physically cooperates and thus the degree of gloss of the color layers influenced divergently.
  • this device it is possible to produce printed products whose surfaces have strongly contrasting matt or high-gloss partial surfaces.
  • the known device requires two of the offset printing units downstream coating units, of which the first, adjacent to the offset printing units coating unit is designed as a flexographic printing and application of rapidly evaporating water-based liquids allowed while the second, downstream coating unit, for example, for full-surface painting of the substrate ,
  • the known device it is not possible to produce printed products which have both very matt and high-gloss painted surfaces which contrast strongly.
  • offset printing machines are very expensive with the known device and have therefore found no widespread use.
  • the object of the invention is to improve a printing method and in particular, but not exclusively, a sheetfed offset printing method such that a printing substrate is produced on commercially available printing machines in a single pass with matte and high-gloss surfaces lying next to one another. Further, the invention is based on the object alone using commercial offset printing machines and conventional oil-based offset printing inks a printed product with a high contrast juxtaposed matte and high gloss Produce surfaces.
  • a substrate during a run through an offset or flexographic printing machine (2) with multiple printing units (6, 8, 10, 12) and a downstream coating unit (14 ) is first printed in at least one of the printing units (6, 8, 10) with an oil-based ink, wherein the substrate is then coated in a subsequent printing unit (12) on a part of the ink-printed surface with an oil-based matt paint, the matting agent contains, wherein the mat lacquer one or more substance (s) are added, which have a low surface energy, and in which the substrate is then coated in the coating unit (14) on the entire printed surface with a transparent gloss varnish.
  • the printing process according to the invention which in the context of this application comprises both offset printing and flexographic printing processes, can readily be carried out in commercial printing presses, since the partial coating with the oil-based matt paint in one of the e.g. Offset printing can be performed without this needs to be converted or modified.
  • the subsequent full-surface coating with the water-based gloss varnish can be carried out in a commercial coating unit for offset printing presses, to which, however, to improve the gloss value of the later shiny part surfaces expediently some smaller and therefore easy to make changes are made.
  • the invention is based on the idea, the matte or glossy faces of the printed product not as in the subject matter of DE 200 20 798 by using two different color systems, but by a single color system of oil-based paints. It has been found that the varnish layer modified by its content of particulate matting agents retains a dull appearance because of the low-surface-energy substance it contains, despite a subsequent full-surface application of the gloss varnish.
  • a low surface energy fabric preferably less than 40 milli Newton per meter and especially less than 25 mN / m, e.g. Silicone oil, the known under the name "Teflon” PTFE (polytetrafluoroethylene) or derivatives of these substances, such as hexafluoropropylene, fluorinated ethylene-propylene copolymer (FEP), Hostaflon be used.
  • Teflon polytetrafluoroethylene
  • FEP fluorinated ethylene-propylene copolymer
  • the matt varnish and the gloss varnish are respectively applied before the previously applied glossy printing ink or, in the latter case, the previously applied matt varnish has been completely cured or struck off.
  • the gloss varnish used is preferably a water-based dispersion varnish, since aqueous dispersion varnishes can be processed well on the varnishing units of commercially available offset printing machines and, on the other hand, provide the desired matt surface in conjunction with the matt or matt varnish, while they do not interfere with the matt varnish coated surfaces provide a high-gloss surface.
  • a dispersion paint based on a styrene-acrylate copolymer is used, but also dispersion coatings based on other polymers can be used.
  • the lowest possible gloss value of the matt partial surfaces and / or the highest possible gloss value of the glossy surfaces is sought.
  • the lowest possible gloss value of the matt partial surfaces is, according to a preferred embodiment of the invention, supported by the fact that the proportion of matting agents is set as high as is possible without impairing the processing properties and the transparency of the matt lacquer. Finely ground silicates are preferably used as matting agents, although other commercially available matting agents may also be used. Due to the high proportion of particulate matting agent, the matt lacquer has a rough surface, from which the gloss lacquer can be almost completely absorbed, at least in smaller amounts.
  • a similar effect is achieved if the matt lacquer wets the previously applied ink only incompletely, which also leads to a structured surface. Also contributes to the silicone oil or PTFE, which is the matte paint, preferably in a range of 0.2 to 0.6 wt .-%, mixed.
  • the Silicone oil caused incomplete wetting of the offset printing ink pad causes, together with the matting agent, that the matt paint after its application has a uniform, hammer-like, scaly surface.
  • a first measure is to make the amount of applied gloss paint on the one hand sufficiently large, so that there is a continuous high-gloss surface on the not coated with the matt surfaces, on the other hand, but not so large that it on the previously coated with the matt Partial surfaces cause a complete flooding and leveling of the rough surface.
  • both specifications can be achieved with an application amount between 12 and 14 cm 3 gloss paint per m 2 application area, which is why the gloss varnish in the coating unit preferably with the aid of a chamber doctor blade and an anilox roller with a Schöpfvolumen of about 13 cm 3 / m 2 is metered.
  • a second measure is to use a gloss varnish with a high viscosity, which also counteracts a leveling of the rough surface.
  • the viscosity of the gloss varnish more than 70 s -1 , preferably more than 75 s -1 and most preferably more than 80 s -1 , measured according to DIN 53 211.
  • the high viscosity of the gloss varnish is preferably achieved in that the gloss varnish a contains high content of resin, for example in the form of a styrene-acrylate copolymer, said content is suitably more than 20 wt .-%, preferably more than 25 wt .-% and most preferably more than 30 wt .-%.
  • the stated high viscosities of the gloss varnish can lead to difficulties in its processing, provides a further preferred embodiment of the invention to apply the gloss varnish in the heated state on the printed and partially coated with the matt-coated substrate, that is with a temperature of more than 20 ° C, preferably greater than 25 ° C, and most preferably greater than 30 ° C.
  • a temperature of more than 20 ° C preferably greater than 25 ° C, and most preferably greater than 30 ° C.
  • the gloss varnish is expediently heated in a heated container to a temperature of more than 30 ° C and preferably more than 40 ° C and pumped as needed into the chambered doctor blade.
  • this is preferably equipped with a stirrer with scrapers.
  • a third measure is to reduce as much as possible the concentration of a wetting agent normally contained in water-dispersed gloss paints, suitably to less than 3% by weight, preferably to less than 2.5% by weight and most preferably to less than 2 Wt .-%, wherein these values relate to a sulfosuccinate as an example wetting agent.
  • the varnish preferably contains a plasticizer, its content in the gloss lacquer is advantageously between 0.2 to 1.5 wt .-%, and preferably between 0.5 and 1 wt .-%.
  • the substrate after coating with the gloss paint at least on the printed Apply hot air and / or heat radiation to the painted side to dry the gloss varnish and the ink more quickly.
  • a printing material of the printed product preferably art paper
  • the commercial four-color sheetfed offset printing machine 2 shown schematically in the drawing consists essentially of a sheet feeder 4 (only partially shown), a total of four offset printing units 6, 8, 10, 12, a printing units 6, 8, 10, 12 downstream coating unit 14, a Drying device 16 and a sheet delivery 18.
  • sheets of a printing material in particular of art paper, spot-varnished after their printing to emphasize different inks by a matte or glossy surface of different parts of the printed image to enhance contrasts, or the To give printing inks a velvety or glossy appearance.
  • the sheets in the first, second and third printing unit 6, 8 and 10 are printed one or more colors with commercial oil-based offset inks, then coated in the last printing unit 12 on a portion of the printed area with an oil-based matt lacquer and in the downstream coating unit 14th coated with a water-based gloss varnish on the entire printed surface before drying in the drying device 16 are stored as finished printed products by means of the sheet delivery 18 on a sheet stack 20.
  • the printing unit 12 is for this purpose as usual with a printing cylinder 22, a blanket cylinder 24, a plate cylinder 26, an inking unit 28, and a dampening unit 30 equipped with the inking unit 28 is used for dosing the matt varnish, which is then transferred together with dampening solution from the dampening unit 30 on the plate cylinder 26 and a pressure plate spanned thereon and the blanket cylinder 24 on the sheet 22 supported by the printing cylinder.
  • the matt lacquer is applied to those portions of the plate cylinder 26 and the sheet corresponding to the matte faces of the finished printed product, while the dampening solution is applied to the remaining portions, that is, those corresponding to the glossy faces of the finished printed product.
  • the application of the matt lacquer on the offset printing inks is wet in damp, ie before complete drying of the printing inks by knocking off and crosslinking.
  • the matte lacquer used has a composition similar to the commercial oil-based offset inks, but contains no color pigments, but contains a high proportion of matting agents in the form of finely ground silicates, and 0.2 to 0.6 wt .-% silicone oil or another silicone compound , which ensures that the offset inks applied before the matt varnish are not completely or evenly wetted by the matt varnish.
  • a matt lacquer with a very high degree of matting is used, which is offered by Aquaprint GmbH in Hoyen, Germany, under the name Hi Dual 0 700 Matte Litho Lithic.
  • the printed sheets which have been partially coated with the matt lacquer are then completely coated in the coating unit 14 with the water-based gloss lacquer, which is a modified transparent dispersion lacquer based on a styrene-acrylate copolymer.
  • the proportion of the styrene-acrylate copolymer in the dispersion varnish becomes adjusted more than 25 wt .-%, in order to increase the viscosity of the dispersion varnish (measured according to DIN 53 211) to more than 75 s -1 .
  • the coating unit 14 is equipped with a heatable paint container 34 in which the paint at a temperature of about 40 ° C by means of a stirrer with scrapers (not shown) is kept in constant motion, to prevent it from adhering to the walls of the container 34.
  • the gloss varnish in the coating unit 14 is applied in a precisely defined limited amount, on the one hand on the not coated with matt varnish surfaces still a sufficient high-gloss surface can be achieved, on the other hand, however, the gloss varnish is almost completely absorbed on the matt lacquered surfaces, without significantly increase the matte value of these surfaces.
  • a gloss paint amount of about 13 cm 3 / m 2 coated substrate surface.
  • the varnishing unit 14 is provided with a chambered doctor blade 36 and an anilox roller 38, whose scoop volume is approximately at the above-mentioned value of 13 cm 3 / m 2 . From the anilox roller 38, the gloss lacquer is transferred to the sheets by means of a blanket or blanket cylinder 40.
  • the finished printed product is dried in the drying device 16 with the aid of infrared radiators and / or by supplying hot air at least on the printed and varnished side, before it is deposited on the stack 20.
  • a printed matter can be obtained which at the same time, i. side by side, having printed faces with a matte finish of which the former has a gloss value of about 20% and the latter a gloss value of about 80% (each measured at a light incidence and light drop angle of 60 degrees) such that the Difference is about 60%, which could not be achieved so far on standard printing presses.

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Printing Methods (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Glass Compositions (AREA)
  • Laminated Bodies (AREA)
  • Paper (AREA)

Claims (29)

  1. Procédé d'impression au cours duquel un matériau à imprimer, pendant un passage dans une machine d'impression offset ou une machine à imprimer par flexographie (2) comprenant plusieurs groupes d'impression (6, 8, 10, 12) et un groupe de vernissage (14) en aval, est tout d'abord imprimé dans au moins l'un des groupes d'impression (6, 8, 10) avec une encre d'impression à base d'huile, puis, dans un groupe d'impression suivant (12), le matériau à imprimer est, revêtu sur une partie de la surface imprimée avec l'encre d'impression par un vernis mat à base d'huile, ce vernis mat renfermant des agents de matité, une ou plusieurs substances à faible énergie superficielle étant additionnées au vernis mat, le procédé prévoyant ensuite de revêtir, dans le groupe de vernissage (14), le matériau à imprimer sur la totalité de la surface imprimée, avec un vernis brillant transparent.
  2. Procédé selon la revendication 1,
    caractérisé en ce que le vernis mat est appliqué avant que l'encre d'impression ait durcie.
  3. Procédé selon les revendications 1 ou 2,
    caractérisé en ce que le vernis brillant est appliqué avant que l'encre d'impression et le vernis mat aient durcis.
  4. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le vernis mat renferment une teneur élevée en agents de matité.
  5. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le matériau à imprimer est revêtu d'un vernis brillant à base d'eau.
  6. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le vernis brillant est un vernis de dispersion.
  7. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le vernis brillant présente une viscosité de plus de 70 s-1, de préférence de plus de 75 s-1, et pour le mieux de plus de 80 s-1, mesurée selon DIN 53 211.
  8. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le vernis brillant est appliqué dans un état échauffé sur le matériau à imprimer, qui a été imprimé et revêtu sur une partie de la surface avec le vernis mat.
  9. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le vernis brillant, lors de l'application sur le matériau à imprimer ayant été imprimé et revêtu sur une partie de la surface avec le vernis mat, présente une température de plus de 20°C, de préférence de plus de 25°C et pour le mieux de plus de 30°C.
  10. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le vernis brillant, avant l'application, est maintenu en mouvement dans un récipient, à une température de plus de 30°C et de préférence à plus de 40°C.
  11. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le vernis brillant renferme moins de 3% en poids, de préférence moins de 2,5% en poids et pour le mieux moins de 2% en poids d'agent mouillant.
  12. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le vernis brillant renferme un plastifiant.
  13. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que la teneur en plastifiant dans le vernis brillant est comprise entre 0,2 à 1,5% en poids et de préférence entre 0,5 et 1% en poids.
  14. Procédé selon l'une des revendications précédentes,
    caractérisé en ce qu'une teneur en résine du vernis brillant vaut plus de 20% en poids, de préférence plus de 25% en poids et pour le mieux plus de 30% en poids.
  15. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le vernis brillant renferme un copolymère styrène-acrylate.
  16. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le vernis brillant est dosé dans le groupe de vernissage en utilisant un rouleau tramé d'un volume d'absorption d'environ 13 cm3/m2 de surface vernie du matériau à imprimer.
  17. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que le matériau à imprimer, après revêtement avec le vernis brillant, est soumis, au moins sur le côté imprimé et vernis, à un balayage par air chaud et/ou à un rayonnement thermique.
  18. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que l'énergie superficielle de la substance additionnelle vaut moins de 40.10-3 N/m.
  19. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que l'énergie superficielle de la substance additionnelle vaut moins de 25.10-3 N/m.
  20. Procédé selon l'une des revendications précédentes,
    caractérisé en ce qu'en ce qui concerne la substance additionnelle, il s'agit d'huile de silicone ou de PTFE (polytétrafluoroéthylène) ou de leurs dérivés.
  21. Procédé selon l'une des revendications précédentes,
    caractérisé en ce que la teneur des substances à faible énergie superficielle additionnées au vernis mat, vaut moins de 2% en poids.
  22. Produit imprimé, comprenant un matériau à imprimer qui est imprimé sur au moins un côté avec une encre d'impression offset à base d'huile, qui, sur une partie de la surface imprimée, est, en outre, revêtu d'un vernis mat à base d'huile renfermant un agent de matité, au moins une substance à faible énergie superficielle étant additionnée au vernis mat, et qui est revêtu sur la totalité de la surface imprimée, y compris la surface partielle revêtue de vernis mat, d'un vernis brillant transparent à base d'eau.
  23. Produit imprimé selon la revendication 22,
    caractérisé en ce que la valeur de brillance de la surface partielle mate revêtue par le vernis brillant vaut moins de 25% et de préférence moins de 20%.
  24. Produit imprimé selon les revendications 22 ou 23,
    caractérisé en ce que la valeur de brillance de l'encre d'impression revêtue uniquement avec le vernis brillant, vaut plus de 60%, de préférence plus de 70% et pour le mieux environ 80%.
  25. Produit imprimé selon l'une des revendications 22 à 24,
    caractérisé en ce que le vernis mat renferme une teneur élevée en agents de matité.
  26. Produit imprimé selon l'une des revendications 22 à 25,
    caractérisé en ce que le vernis mat renferme un plastifiant.
  27. Produit imprimé selon l'une des revendications 22 à 26,
    caractérisé en ce que le vernis mat renferme une substance d'une faible énergie superficielle de moins de 40.10-3 N/m.
  28. Produit imprimé selon la revendication 27,
    l'énergie superficielle valant moins de 25.10-3 N/m.
  29. Produit imprimé selon les revendications 27 ou 28,
    la substance de faible énergie superficielle étant de l'huile de silicone ou du PTFE (polytétrafluoroéthylène) ou un dérivé de ceux-ci.
EP04106770A 2003-12-22 2004-12-21 Procédé d'impression pour réaliser des surfaces mates et brillantes Active EP1547772B2 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL04106770T PL1547772T5 (pl) 2003-12-22 2004-12-21 Sposób drukowania do wytwarzania powierzchni matowych i połyskowych

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10360050 2003-12-22
DE2003160050 DE10360050B3 (de) 2003-12-22 2003-12-22 Offsetdruckverfahren und Druckerzeugnis

Publications (3)

Publication Number Publication Date
EP1547772A1 EP1547772A1 (fr) 2005-06-29
EP1547772B1 EP1547772B1 (fr) 2007-05-30
EP1547772B2 true EP1547772B2 (fr) 2011-03-16

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ID=34530340

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EP04106770A Active EP1547772B2 (fr) 2003-12-22 2004-12-21 Procédé d'impression pour réaliser des surfaces mates et brillantes

Country Status (10)

Country Link
US (1) US7856926B2 (fr)
EP (1) EP1547772B2 (fr)
JP (1) JP4153546B2 (fr)
CN (1) CN100488776C (fr)
AT (1) ATE363391T1 (fr)
DE (2) DE10362054B4 (fr)
DK (1) DK1547772T4 (fr)
ES (1) ES2286565T5 (fr)
PL (1) PL1547772T5 (fr)
WO (1) WO2005063489A1 (fr)

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ATE554943T1 (de) * 2007-01-02 2012-05-15 Actega Terra Gmbh Druckerzeugnis und verfahren zu dessen herstellung
CN101220568B (zh) * 2007-11-30 2011-09-21 大亚科技股份有限公司 防水雾uv上光油配方
DE102007059911A1 (de) * 2007-12-12 2009-06-18 Koenig & Bauer Aktiengesellschaft Verfahren und Vorrichtung zur Erzeugung von Effektlackierungen auf Bedruckstoffen in Druckmaschinen
GB2457922A (en) 2008-02-28 2009-09-02 Sun Chemical Ltd Coldset web offset printing process and compositions
DE102008043767A1 (de) * 2008-11-14 2010-06-02 Koenig & Bauer Aktiengesellschaft Druckmaschine und Verfahren zur Handhabung einer durch die Druckmaschine geführten Bahn
DE102009002228B4 (de) * 2009-04-06 2015-01-08 Koenig & Bauer Aktiengesellschaft Lackierwerk einer Rollen-Rotations-Offsetdruckmaschine
WO2010128842A1 (fr) * 2009-05-04 2010-11-11 Kek Ken Kiong Effet martelé 3d
CN101691720B (zh) * 2009-10-23 2011-05-11 上海美声服饰辅料有限公司 一种克服黑卡纸掉墨的处理方法
EP2319703B2 (fr) * 2009-11-10 2023-09-06 Heidelberger Druckmaschinen Intellectual Property AG & Co. KG Procédé d'application tramées de fluides sur des substrats
DE102010030267B4 (de) * 2010-06-18 2013-08-14 Koenig & Bauer Aktiengesellschaft Verfahren und Vorrichtung zur Steuerung einer Rollenrotationsdruckmaschine sowie Verfahren zum Betrieb einer Rollenrotationsdruckmaschine
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CN102756578A (zh) * 2012-07-30 2012-10-31 昆山科望快速印务有限公司 一种印刷工艺
CN102825929A (zh) * 2012-09-14 2012-12-19 昆山科望快速印务有限公司 一种印刷工艺
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CN110217009B (zh) * 2019-07-16 2021-09-28 深圳劲嘉集团股份有限公司 一种替代胶印逆向印刷工艺的凹版印刷方法
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WO2005063489A1 (fr) 2005-07-14
EP1547772B1 (fr) 2007-05-30
DE502004003934D1 (de) 2007-07-12
PL1547772T3 (pl) 2007-10-31
US20060230965A1 (en) 2006-10-19
DK1547772T4 (da) 2011-05-30
DK1547772T3 (da) 2007-09-03
ATE363391T1 (de) 2007-06-15
DE10362054B4 (de) 2010-12-30
JP2007518594A (ja) 2007-07-12
ES2286565T5 (es) 2011-06-22
ES2286565T3 (es) 2007-12-01
PL1547772T5 (pl) 2011-07-29
JP4153546B2 (ja) 2008-09-24
US7856926B2 (en) 2010-12-28
CN1882438A (zh) 2006-12-20
DE10362054A1 (de) 2005-07-21
CN100488776C (zh) 2009-05-20

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