EP0892097B1 - Méthode de fabrication de fils à coudre texturés par jet d'air - Google Patents
Méthode de fabrication de fils à coudre texturés par jet d'air Download PDFInfo
- Publication number
- EP0892097B1 EP0892097B1 EP98112784A EP98112784A EP0892097B1 EP 0892097 B1 EP0892097 B1 EP 0892097B1 EP 98112784 A EP98112784 A EP 98112784A EP 98112784 A EP98112784 A EP 98112784A EP 0892097 B1 EP0892097 B1 EP 0892097B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- thread
- effect
- ground
- accordance
- textured yarn
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Revoked
Links
- 238000009958 sewing Methods 0.000 title claims abstract description 6
- 238000000034 method Methods 0.000 title claims description 22
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- 230000000694 effects Effects 0.000 claims abstract description 68
- 238000010438 heat treatment Methods 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000004952 Polyamide Substances 0.000 claims description 6
- 229920002647 polyamide Polymers 0.000 claims description 6
- 229910052799 carbon Inorganic materials 0.000 claims description 5
- 229920002292 Nylon 6 Polymers 0.000 claims description 2
- 239000004698 Polyethylene Substances 0.000 claims description 2
- 229920000297 Rayon Polymers 0.000 claims description 2
- 229920000728 polyester Polymers 0.000 claims description 2
- -1 polyethylene Polymers 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 238000009736 wetting Methods 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
Images
Classifications
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/22—Yarns or threads characterised by constructional features, e.g. blending, filament/fibre
- D02G3/34—Yarns or threads having slubs, knops, spirals, loops, tufts, or other irregular or decorative effects, i.e. effect yarns
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G1/00—Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics
- D02G1/16—Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics using jets or streams of turbulent gases, e.g. air, steam
- D02G1/161—Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics using jets or streams of turbulent gases, e.g. air, steam yarn crimping air jets
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G1/00—Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics
- D02G1/20—Combinations of two or more of the above-mentioned operations or devices; After-treatments for fixing crimp or curl
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02J—FINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
- D02J1/00—Modifying the structure or properties resulting from a particular structure; Modifying, retaining, or restoring the physical form or cross-sectional shape, e.g. by use of dies or squeeze rollers
- D02J1/08—Interlacing constituent filaments without breakage thereof, e.g. by use of turbulent air streams
Definitions
- the invention relates to a method for producing air-textured Threads from at least one upright thread and at least an effect thread in which at least the upright thread is drawn before using a Texturing unit is supplied and in which the textured, yarn consisting of stand and effect thread is heated.
- Such methods take advantage of the effect that during the heating of the after the texturing unit textured yarn of the upright thread stretched before texturing shrinks less than the effect thread. This has the consequence that in the texturing formed by the effect thread Loops contracted during said heating be, which ultimately makes the thread more desirable Way gets a relatively smooth surface.
- An object of the invention is the method of continue to develop in such a way that also thin, very fine threads with sufficient strength are producible.
- this object is achieved in that a Upright thread with a fineness between 80 and 200 dtex and an effect thread with a fineness between 60 and 165 dtex is used, the effect thread is finer than the upright thread.
- Threads is, for example, between 11 and 12%, i.e. the length of the textured thread can be stretched by 11 to 12% be without tearing.
- the method according to the invention therefore makes them very fine Threads producible that are both high strength as well a high level of uniformity with a high degree of freedom from errors exhibit.
- a stand thread with a fineness between 140 and 160 dtex and / or an effect thread with a Fineness between 70 and 90 dtex is used.
- Rise Around / or Effect threads can have between 36 and 144 filaments each exhibit.
- the upright thread is in front of the Texturing unit by 1.8 to 2.6 times, in particular by stretched 2 to 2.4 times. Furthermore, it is from Advantage if, in addition to the upright thread, the effect thread is stretched in front of the texturing unit, the stretching of the effect thread is preferably smaller than the stretching of the thread.
- the effect thread can, for example 1.5 to 1.9 times, in particular 1.6 to Be stretched 1.8 times.
- the upright thread can be heated more than the effect thread, with temperatures regarding the heating of the standing thread between 150 ° and 240 °, in particular between 160 ° and offer 220 °.
- Temperatures between 100 ° C and 200 ° C, in particular between 140 ° C and 180 ° C makes sense.
- the upright and / or the effect thread in front of the texturing unit each over two successive godets be performed.
- the drawing of upright and / or effect thread can then, for example, by different drive speeds two successive godets are effected, the rear godet in the direction of the conveyor runs faster than the front godet.
- a stretching can also be carried out by means of the godets Heating of upright and / or effect threads are effected, by at least one of the upright and / or effect threads assigned godets is heated.
- the Godets to the temperatures already mentioned above be heated.
- the threads can each between 5 and 20 times, in particular between 6 and 10 times helically around a godet, so that the frictional forces between godets and threads are sufficient are high.
- this stretching can, for example, by a factor between 0.95 and 1.1, in particular between 1.01 and 1.05.
- the stretching is preferably carried out in such a way that the distance of the textured yarn that is currently heating is also post-stretched at the same time. This can prevent that the textured yarn during overall heating contracts too much.
- Concrete is achieved by a post-stretching factor greater than 1, that the main thread component of the textured yarn during of the heating process is stretched. With a post-stretch factor less than 1 ensures that the upright component maximum by the post-stretching factor can shrink.
- the shrinkage of the upright component of the textured Yarn is thus limited by the post-stretching mentioned, and the loops formed by the effect thread can decrease in size in the desired manner due to the heating or contract.
- the heating of the textured yarn after the texturing unit is preferably carried out such that the temperature of the textured yarn in the range between 200 ° C and 300 ° C, in particular between 210 ° C and 260 ° C.
- this can textured yarn the texturing unit at a speed between 300 m / min and 500 m / min, especially at 400 leave m / min.
- both effect thread and upright thread are delivered at a speed which is about the speed at which the textured yarn Texturing unit leaves.
- the delivery speed of the standing thread is preferred between 4% and 8%, especially about 6% above speed, with which the textured yarn the texturing unit leaves.
- the speed of delivery of the effect thread is preferred between 14% and 20%, in particular between 16% and 18% over the speed at which the textured yarn Texturing unit leaves.
- the texturing unit which is preferably designed as a texturing nozzle with a pressure between 6 and operated at 14 bar.
- the water throughput for example between 0.1 l / h and 1 l / h, in particular can be approximately 0.25 l / h.
- the thread can be normal, for example Drinking water can be used, which previously had an activated carbon filter happens.
- Standard and / or effect thread can be made of polyester, polyamide, Polyamide 6, polyamide 6.6, polyamide 4.6, polyethylene and / or Made of viscose.
- the texturing unit instead of using only one standing and one It is alternatively possible to effect threads, the texturing unit one stand and two effect threads or two stand and one Feed effect thread or two upright and effect threads.
- the textured yarn can in particular produce sewing thread be twisted after being heated.
- the twist is, for example, between 150 and 600, in particular between 300 and 500 turns per meter.
- the standing thread 1 is used during the operation of the device subtracted from a supply spool 2. In an analogous way the effect thread 3 is drawn off from a second supply spool 4.
- the upright thread arrives at a first one Galette 5, from the upright thread 1 several times helically is entwined.
- the upright thread 1 is a second Galette 6 excited, which he also wraps around several times.
- the effect thread 3 is in an analogous manner via a third godet 7 and a fourth godet 8 performed.
- the upright thread 1 arrives to a wetting station 9 where he wets with water becomes.
- the textured yarn 11 leaving the texturing nozzle becomes fed to a heating device 13 via a fifth godet 12, from where the heated textured yarn 11 to one sixth godet 14 arrives.
- the godets 12 and 14 are of the textured yarn 11 in turn entwined several times.
- the textured yarn becomes one Rewinder 15 fed.
- the described device can, for example, in the following Mode operated, the sizes mentioned, of course can be varied in the above-mentioned areas:
- the upright thread 1 is removed from the supply bobbin 2 at one speed deducted from about 240 m / min and the first Galette 5 fed. In a corresponding way, the effect thread 3 at a speed of approximately 310 m / min from deducted the supply spool 4 and fed to the third godet 7.
- the upright thread has a fineness of approximately 160 dtex, while the effect thread has a fineness of approximately 90 dtex owns.
- the second godet 6 runs faster by a factor of 1.8 than the first godet 5, which results in a corresponding stretching of the thread 1 results.
- the fourth godet 8 runs faster by a factor of 1.5 than the third godet 7, with a corresponding one also here Stretching of the effect thread 2 results.
- the second godet 6 is heated to a temperature of 240 ° C. so that a corresponding heating of the standing thread 1 is effected.
- the fourth godet is similar 8 for heating the effect thread to a temperature of 200 ° C designed.
- the first godet 5 and the third godet 7 both are not heated.
- the stretched and heated is in the wetting station 9 Standard thread wetted with water, with a water throughput here of 0.7 l / h comes into play.
- the texturing nozzle 10 is at an air pressure of approximately 7 operated bar.
- the intermingled and textured yarn 11 is between the fifth godet 12 and sixth godet 14 by a factor of 1.01, which is caused by the fact that the sixth godet 14 faster by a corresponding factor runs as the fifth godet 12.
- the textured yarn 11 leaves the texturing nozzle 10 with a Speed of about 400 m / min and is dependent on that Rewinder 15 added at approximately the same speed.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
- Air Bags (AREA)
Claims (13)
- Procédé pour produire des fils à coudre texturés par jet d'air à partir d'au moins un fil de fond (1) et d'au moins un fil formant la fantaisie (3), dans lequel au moins le fil de fond (1) est étiré avant d'être amené, conjointement avec le fil de fantaisie (3), à une unité de texturation (10), et dans lequel le fil composite texturé (11) constitué par le fil de fond et par le fil de fantaisie (1, 3) est chauffé,
caractérisé en ce que l'on utilise un fil de fond (1) d'une finesse entre 80 et 200 dtex et un fil de fantaisie (3) d'une finesse entre 60 et 165 dtex, le fil de fantaisie (3) étant plus fin que le fil de fond (1). - Procédé selon la revendication 1, caractérisé en ce que l'on utilise un fil de fond (1) d'une finesse entre 140 et 160 dtex, et/ou en ce que l'on utilise un fil de fantaisie (3) d'une finesse entre 70 et 90 dtex, et/ou en ce que l'on utilise un fil de fond et/ou un fil de fantaisie (1, 3) qui présentent chacun entre 36 et 144 filaments.
- Procédé selon l'une des revendications précédentes, caractérisé en ce que le fil de fond (1) est étiré en avant de l'unité de texturation (10) de 1,8 à 2,6 fois, en particulier de 2 à 2,4 fois, et/ou en ce que le fil de fantaisie (3) est également étiré en avant de l'unité de texturation, le fil de fond (1) étant en particulier étiré plus fortement en avant de l'unité de texturation (10) que le fil de fantaisie (3), et/ou en ce que le fil de fantaisie (3) est étiré en avant de l'unité de texturation (10) de 1,5 à 1,9 fois, en particulier de 1,6 à 1,8 fois.
- Procédé selon l'une des revendications précédentes, caractérisé en ce que le fil de fond et/ou le fil de fantaisie (1, 3) est chauffé en avant de l'unité de texturation (10), le fil de fond (1) étant en particulier chauffé plus fortement que le fil de fantaisie, et/ou en ce que le fil de fond (1) est chauffé à une température comprise entre 150°C et 240°C, en particulier entre 160°C et 220°C, et/ou en ce que le fil de fantaisie (3) est chauffé à une température entre 100°C et 200°C, en particulier entre 140°C et 180°C.
- Procédé selon l'une des revendications précédentes, caractérisé en ce que le fil de fond et/ou le fil de fantaisie (1, 3) est guidé en avant de l'unité de texturation (10) via deux galettes successives (5, 6 ; 7, 8), en particulier l'étirage du fil de fond et/ou du fil de fantaisie (1, 3) étant provoqué par des vitesses d'entraínement différentes des deux galettes successives (5, 6 ; 7, 8), et/ou la chauffe du fil de fond et/ou du fil de fantaisie (1, 3) est provoquée par échauffement d'au moins une galette (6 ; 8), les galettes (6 ; 8) étant chauffées de préférence aux températures selon la revendication 4.
- Procédé selon la revendication 5, caractérisé en ce que les galettes (5, 6 ; 7, 8) sont entourées par le fil de fond et/ou par le fil de fantaisie (1, 3) chacune entre 5 et 20 fois, en particulier entre 7 et 10 fois.
- Procédé selon l'une des revendications précédentes, caractérisé en ce que le fil composite texturé (11) est étiré à posteriori, le fil composite texturé (11) étant étiré à posteriori en particulier de 0,95 à 1,1 fois, en particulier de 1,01 à 1,05 fois, et/ou en ce que le fil composite texturé (11) est chauffé à une température entre 200°C et 300°C, en particulier entre 210°C et 260°C.
- Procédé selon l'une des revendications précédentes, caractérisé en ce que le fil composite texturé (11) est guidé via deux galettes successives (12, 14), l'étirage du fil composite texturé (11) étant provoqué en particulier par des vitesses d'entraínement différentes des deux galettes successives (12, 14), et/ou l'échauffement du fil composite texturé (11) est provoqué par un dispositif de chauffage (13) situé entre les galettes (12, 14), et/ou les galettes sont entourées par le fil composite texturé chacune entre 5 et 20 fois, en particulier entre 6 et 10 fois.
- Procédé selon l'une des revendications précédentes, caractérisé en ce que le fil composite texturé (11) quitte l'unité de texturation (10) à une vitesse entre 300 m/min et 500 m/min, en particulier d'environ 400 m/min, et/ou en ce que la vitesse de livraison du fil de fond (1) est supérieure à ladite vitesse d'une valeur comprise entre 4 % et 8 %, en particulier de 6 %, et/ou en ce que la vitesse de livraison du fil de fantaisie (3) est supérieure à ladite vitesse d'une valeur comprise entre 14 % et 20 %, en particulier entre 16 % et 18 %.
- Procédé selon l'une des revendications précédentes, caractérisé en ce que l'unité de texturation (10) fonctionne à une pression d'environ 9 bar, et/ou en ce que le fil de fond (1) est attaqué avec de l'eau en avant de l'unité de texturation (10), le débit d'eau étant compris en particulier entre 0,2 l/h et 1 l/h, en particulier d'environ 0,25 l/h.
- Procédé selon l'une des revendications précédentes, caractérisé en ce que le fil de fond et/ou le fil de fantaisie (1, 3) est constitué en polyester, polyamide, polyamide 6, polyamide 6.6, polyamide 4.6, polyéthylène et/ou en viscose, et/ou en ce que l'on amène à l'unité de texturation (10) un fil de fond et deux fils de fantaisie ou deux fils de fond et un fil de fantaisie ou encore deux fils de fond et deux fils de fantaisie.
- Procédé selon l'une des revendications précédentes, caractérisé en ce que le fil composite texturé (11) est torsadé en particulier après son échauffement, afin de produire ainsi un fil à coudre, la torsion étant en particulier comprise entre 150 et 600, en particulier entre 300 et 500 tours par mètre.
- Fil composite ou fil à coudre, réalisé selon l'une ou plusieurs des revendications précédentes, en utilisant un fil de fond d'une finesse entre 80 et 200 dtex et un fil de fantaisie d'une finesse entre 60 et 165 dtex, le fil de fantaisie étant plus fin que le fil de fond.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19730977A DE19730977A1 (de) | 1997-07-18 | 1997-07-18 | Verfahren zur Herstellung lufttexturierter Nähfäden |
DE19730977 | 1997-07-18 |
Publications (3)
Publication Number | Publication Date |
---|---|
EP0892097A2 EP0892097A2 (fr) | 1999-01-20 |
EP0892097A3 EP0892097A3 (fr) | 1999-09-01 |
EP0892097B1 true EP0892097B1 (fr) | 2003-01-22 |
Family
ID=7836202
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP98112784A Revoked EP0892097B1 (fr) | 1997-07-18 | 1998-07-09 | Méthode de fabrication de fils à coudre texturés par jet d'air |
Country Status (8)
Country | Link |
---|---|
US (1) | US6055712A (fr) |
EP (1) | EP0892097B1 (fr) |
AT (1) | ATE231569T1 (fr) |
CA (1) | CA2243841A1 (fr) |
DE (2) | DE19730977A1 (fr) |
DK (1) | DK0892097T3 (fr) |
ES (1) | ES2186946T3 (fr) |
PT (1) | PT892097E (fr) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6374470B1 (en) * | 2000-10-06 | 2002-04-23 | Milliken & Company | Face plate for spun-like textured yarn |
DE10124161A1 (de) * | 2001-05-17 | 2002-11-21 | Guetermann Ag | Lufttexturierter Faden sowie Verfahren und dessen Herstellung |
DE10124162A1 (de) * | 2001-05-17 | 2002-11-21 | Guetermann Ag | Lufttexturierter Faden sowie Verfahren zu dessen Herstellung |
DE10221170A1 (de) * | 2002-05-13 | 2003-11-27 | Guetermann Ag | Verwendung eines mechanisch texturierten Fadens |
CN101265627B (zh) * | 2007-05-16 | 2011-05-11 | 桐昆集团股份有限公司 | 涤纶中速混纺型fdy和poy混纺纤维的混纺方法及其装置 |
DE102017100487A1 (de) * | 2017-01-12 | 2018-07-12 | Trützschler GmbH & Co Kommanditgesellschaft | Vorrichtung und Verfahren zur Erzeugung eines mehrfarbigen Garnes |
DE102017100488A1 (de) | 2017-01-12 | 2018-07-12 | Trützschler GmbH & Co Kommanditgesellschaft | Vorrichtung und Verfahren zur Erzeugung eines texturierten Filamentes oder Garnes |
US11098418B2 (en) * | 2017-09-27 | 2021-08-24 | Abhishek Mandawewala | Process and system for manufacturing twisted and textured yarns |
CN110804780B (zh) * | 2019-10-29 | 2021-08-13 | 江苏恒力化纤股份有限公司 | 一种异收缩珍珠纱及其制备方法 |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4025595A (en) * | 1975-10-15 | 1977-05-24 | E. I. Du Pont De Nemours And Company | Process for preparing mixed filament yarns |
US4248036A (en) * | 1979-03-08 | 1981-02-03 | E. I. Du Pont De Nemours And Company | Bulky yarn |
US4437301A (en) * | 1982-03-25 | 1984-03-20 | Milliken Research Corporation | Method of making yarn |
DE3720237A1 (de) * | 1987-06-15 | 1989-01-05 | Amann & Soehne | Verfahren zum herstellen von luftblastexturiertem naehgarn |
GB8811842D0 (en) * | 1988-05-19 | 1988-06-22 | Rieter Scragg Ltd | Yarn texturing machine |
DE3834139A1 (de) * | 1988-10-07 | 1990-04-19 | Hoechst Ag | Zweikomponenten-schlingennaehgarn und verfahren zu seiner herstellung |
JP2754601B2 (ja) * | 1988-10-12 | 1998-05-20 | 東洋紡績株式会社 | フイラメント複合ミシン糸 |
GB9223102D0 (en) * | 1992-11-04 | 1992-12-16 | Coats Ltd J & P | Making textile strands |
DE4424547C2 (de) * | 1993-07-15 | 2001-05-17 | Staehle Gmbh H | Verfahren zur Herstellung eines Nähfadens und Nähfaden |
GB9323441D0 (en) * | 1993-11-13 | 1994-01-05 | Coats Ltd J & P | Method for making thread |
EP0664352B1 (fr) * | 1994-01-20 | 1999-03-17 | Hoechst Aktiengesellschaft | Fil bouclé à deux composants, procédé pour sa fabrication et son utilisation comme fil à coudre ou à broder |
DE4430633A1 (de) * | 1994-08-29 | 1996-03-07 | Hoechst Ag | Zweikomponenten-Schlingengarne, Verfahren zu deren Herstellung und deren Verwendung als Nähgarne und Stickgarne |
DE4401513A1 (de) * | 1994-01-20 | 1995-07-27 | Hoechst Ag | Zweikomponenten-Schlingengarne, Verfahren zu deren Herstellung und deren Verwendung als Nähgarne und Stickgarne |
DE4443456A1 (de) * | 1994-12-07 | 1996-07-04 | Hoechst Trevira Gmbh & Co Kg | Zweikomponenten-Schlingengarne aus Aramidfilamenten, Verfahren zu deren Herstellung und deren Verwendung |
-
1997
- 1997-07-18 DE DE19730977A patent/DE19730977A1/de not_active Withdrawn
-
1998
- 1998-07-09 ES ES98112784T patent/ES2186946T3/es not_active Expired - Lifetime
- 1998-07-09 DE DE59806975T patent/DE59806975D1/de not_active Revoked
- 1998-07-09 EP EP98112784A patent/EP0892097B1/fr not_active Revoked
- 1998-07-09 AT AT98112784T patent/ATE231569T1/de not_active IP Right Cessation
- 1998-07-09 DK DK98112784T patent/DK0892097T3/da active
- 1998-07-09 PT PT98112784T patent/PT892097E/pt unknown
- 1998-07-16 US US09/116,293 patent/US6055712A/en not_active Expired - Lifetime
- 1998-07-17 CA CA002243841A patent/CA2243841A1/fr not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
DE59806975D1 (de) | 2003-02-27 |
EP0892097A2 (fr) | 1999-01-20 |
ES2186946T3 (es) | 2003-05-16 |
DE19730977A1 (de) | 1999-01-21 |
EP0892097A3 (fr) | 1999-09-01 |
US6055712A (en) | 2000-05-02 |
CA2243841A1 (fr) | 1999-01-18 |
ATE231569T1 (de) | 2003-02-15 |
DK0892097T3 (da) | 2003-04-14 |
PT892097E (pt) | 2003-06-30 |
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