EP0834364A2 - Méthode et dispositif pour des machines de coulée continue à haute vitesse avec réduction d'épaisseur pendant la solidification - Google Patents
Méthode et dispositif pour des machines de coulée continue à haute vitesse avec réduction d'épaisseur pendant la solidification Download PDFInfo
- Publication number
- EP0834364A2 EP0834364A2 EP97116428A EP97116428A EP0834364A2 EP 0834364 A2 EP0834364 A2 EP 0834364A2 EP 97116428 A EP97116428 A EP 97116428A EP 97116428 A EP97116428 A EP 97116428A EP 0834364 A2 EP0834364 A2 EP 0834364A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- strand
- reduction
- thickness
- segment
- casting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 230000009467 reduction Effects 0.000 title claims abstract description 131
- 238000007711 solidification Methods 0.000 title claims abstract description 46
- 230000008023 solidification Effects 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 22
- 238000009749 continuous casting Methods 0.000 title claims abstract description 7
- 238000005266 casting Methods 0.000 claims abstract description 68
- 238000005452 bending Methods 0.000 claims description 20
- 238000005096 rolling process Methods 0.000 claims description 11
- 230000007423 decrease Effects 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims 1
- IHQKEDIOMGYHEB-UHFFFAOYSA-M sodium dimethylarsinate Chemical class [Na+].C[As](C)([O-])=O IHQKEDIOMGYHEB-UHFFFAOYSA-M 0.000 claims 1
- 238000009826 distribution Methods 0.000 description 12
- 230000008014 freezing Effects 0.000 description 8
- 238000007710 freezing Methods 0.000 description 8
- 239000012071 phase Substances 0.000 description 8
- 229910000831 Steel Inorganic materials 0.000 description 6
- 239000010959 steel Substances 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000035515 penetration Effects 0.000 description 3
- 239000013078 crystal Substances 0.000 description 2
- 238000013021 overheating Methods 0.000 description 2
- 239000007790 solid phase Substances 0.000 description 2
- 241000163925 Bembidion minimum Species 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 230000009189 diving Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000011089 mechanical engineering Methods 0.000 description 1
- 238000010327 methods by industry Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229910000658 steel phase Inorganic materials 0.000 description 1
- 230000001960 triggered effect Effects 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/12—Accessories for subsequent treating or working cast stock in situ
- B22D11/1206—Accessories for subsequent treating or working cast stock in situ for plastic shaping of strands
Definitions
- the invention relates to a method and an apparatus for Continuous caster for the production of strands, their cross section is reduced during solidification.
- the strands on such high speed equipment generally with a solidification thickness between 18 and 450 mm and casting speeds up to a maximum of 12 m / min e.g. on plants for casting slabs, blooms and sticks with a square or round profile, one of which Reduction of the strand cross-section, preferably in the thickness direction made after it emerged from the mold during solidification becomes.
- So z. B a thin slab with a thickness of, for example, 65 to 40 mm in segment 0, which is located directly under the mold, reduced.
- This strand thickness reduction by 25 mm or 38.5% can qualitatively disadvantageous for certain steel grades sensitive to internal cracks be.
- the inner strand deformation can be caused by the Strand thickness reduction or also called casting rolls, for the trigger of internal cracks because of the critical deformation of the material liquid / solid on the inner strand shell, but also on the outer Strand shell is exceeded.
- This example is based on a 2 m long arc segment 0, that no bending work or bending deformation in the strand shell brings in.
- the forming speed of the strand shell when Casting rolls during solidification which is a measure of the strand deformation represents 1.25 mm / s with a casting speed of 6 m / min. This value of the forming speed increases with a casting speed increase to z. B. 10 m / min to 2.08 mm / s, which makes it very critical.
- Such alone internal deformation caused by the casting rolling not just for the deep-drawn steel grades, which are relatively insensitive against internal information, but especially for sensitive ones Steels like microalloyed APX - 80 grades critical.
- the deformation caused by casting rolling can also in vertical turning systems, where normally in Segment under the mold also bends the strand takes place, still by the bending deformation introduced into the strand greatly exaggerate, increasing the risk of exceeding the critical deformation and thus the crack formation increased again becomes.
- the description of the invention is based on an example Thin slab with a thickness of 100 mm at the mold outlet and a solidification thickness of 80 mm.
- the invention now proposes one Type of distribution and implementation of strand thickness reduction during the solidification of the thin slab in the strand guide frame for the exemplary casting speeds of 6 and 10 m / min before.
- Tables 1 and 1.1 are the essential process and device data contrasted the invention with the prior art.
- Table 1 provides the data for casting speeds of 6 m / min and Table 1.1 for speeds of 10 m / min represents.
- FIGS 1 to 7 illustrate the invention in detail in comparison the state of the art.
- the pure melting phase or penetration zone is in the range of segment 0, in which a strand thickness reduction or casting rolling of 2 x 10 mm or 20 mm and no more in the following segments 1 to 13, - Description of the state of the art (Image 1) -, or of 2 x 5 mm or 10 mm, casting rolls, and another 10 mm in the following segments 1 to 13, "soft reduction", part of the invention (Photo 2).
- the reduction in strand thickness in the segment 0, the z. B. as pliers segment with two clamping devices, e.g. B. hydraulic cylinders (14), formed at the segment exit is linear over a length of 3 m; the reduction in the area of segments 1 - 13, but also across all segments, both linear and non-linear, i.e. for example following a square root.
- the strand thickness reduction of 10 mm in the segments 1-13 "soft reduction" - linear distribution.
- FIG. 4 schematically represents the situation of a Strands with a thickness in the mold of 100 mm and a solidification thickness of 80 mm for the casting speeds VG of 6 m / min, Figure 3, and of 10 m / min, Figure 4 compared.
- the strand thickness reduction is 6 m / min from Z. B. 10 mm in segment 0 and of the remaining 10 mm in the Segments 1 to 8, corresponding to the shorter solidification path, performed. So the lowest liquidus point (1.2) is at already about 1.8 m and the swamp tip (2.2) at about 18.12 m.
- the picture 4 in Figure 4 shows the situation of the strand like Figure 2 in Figure 1 at a casting speed of VG 10 m / min.
- FIG. 5 shows the effect of a distribution of the strand thickness reduction in segment 0 and in segments 1 to 13 in the sense of Invention ( Figure 6) using the example of a vertical bending machine, FIG. 6, compared to the prior art (FIG. 5), on the inner strand deformation, caused by the bending deformations and the strand thickness reduction, depending on the strand guide for the maximum casting speed of, for example, 10 m / min shown.
- Vg-10 maximum casting speed
- the strand undergoes a further increase in the internal deformation (D) due to the deformation (DR) when it bends back in segment 4 from the inner circular arc into the horizontal, which, however, cannot become critical since the number of back bending points at design the system is selected so that the rebending process at maximum casting speed cannot trigger any critical internal deformation in the strand shell of the most crack-sensitive steel grade.
- D internal deformation
- DR deformation
- Figure 6 in Figure 5 shows the procedural features the invention using the example of a vertical turning system, Figure 6, schematically.
- the inner deformation (D) of the strand shell (3) is never in a moment of solidification, H. from the mold exit critical to the end of scaffold 13. This is due to the distribution the total strand thickness reduction from 20 mm to, for example 10 mm in segment 0 (D-Gw) and 10 mm in frames 1 to 13 (D-SR) ensured according to the invention.
- This machine configuration with a maximum casting speed of 10 m / min and a maximum capacity of approx. 3 million t / a represents an extremely advantageous solution when using the Invention represents a minimal deformation density of the strand occurs during its solidification.
- a segment should preferably be an odd one Number of 3, 5, 7 or 9 pairs of rollers (15) consisting of Lower (16) and upper roller (17) can be built. Every segment alternately consists of a pair of driven rollers (18), which is position and force controlled with a hydraulic system (19) and two with a hydraulic system (20) in the area the top rollers (17) connected non-driven roller pairs (21), which are provided with a machine element (22) that it allowed the pair of rollers of the top web in the casting direction by one Angle of z. B. to allow +/- 5 ° to swing in any casting situation for a given decrease in strand thickness, the strand if secured its shape.
- This structure of segments 1 to 13 leads to an optimal one Strand guidance in any type of distribution of strand thickness reduction, every casting situation, every kind of steel grade, with regard to their internal crack sensitivity, d. H. Critical Deformation Limit and the use of a minimum of hydraulic Systems per pair of rollers. So come 0.66 hydraulic systems per pair of rollers.
- the use of driven Roll pairs of 0.33 units per roll pair a mechanical engineering Minimum at maximum procedural and qualitative effect on the strand to be cast and its surface and interior quality, d. H. for example a minimal one Structure and a minimized accumulation of tensile stresses in the Strand shell between the driven roller pairs.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Continuous Casting (AREA)
- Metal Rolling (AREA)
- Consolidation Of Soil By Introduction Of Solidifying Substances Into Soil (AREA)
Applications Claiming Priority (9)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19639297 | 1996-09-25 | ||
DE19639297A DE19639297C2 (de) | 1996-09-25 | 1996-09-25 | Verfahren und Vorrichtung für Hochgeschwindigkeits-Stranggießanlagen mit einer Strangdickenreduktion während der Erstarrung |
BR9707100A BR9707100A (pt) | 1996-09-25 | 1997-12-16 | Processo e dispositivo para instalações de fundição contínua de elevada velocidade com uma redução da espessura do bilete a solidifição |
JP34813897A JP4057119B2 (ja) | 1996-09-25 | 1997-12-17 | 凝固中に板厚減少を行う高速連続鋳造装置のための方法及び装置 |
CNB981039030A CN1191898C (zh) | 1996-09-25 | 1998-01-08 | 用于高速连铸设备的、凝固时压下铸坯的方法和装置 |
US09/004,430 US6276436B1 (en) | 1996-09-25 | 1998-01-08 | Method and apparatus for high-speed continuous casting plants with a strand thickness reduction during solidification |
AU51080/98A AU753199B2 (en) | 1996-09-25 | 1998-01-12 | Method and apparatus for high-speed continuous casting plants with a strand thickness reduction during solidification |
ZA9800204A ZA98204B (en) | 1996-09-25 | 1998-01-12 | Method and apparatus for high-speed continuous casting plants with a strand thickeness reduction during solidification. |
CA002226859A CA2226859C (fr) | 1996-09-25 | 1998-01-13 | Methode et appareil pour une installation de coulee continue a haute vitesse avec une reduction d'epaisseur du brin pendant la solidification |
Publications (3)
Publication Number | Publication Date |
---|---|
EP0834364A2 true EP0834364A2 (fr) | 1998-04-08 |
EP0834364A3 EP0834364A3 (fr) | 1998-10-28 |
EP0834364B1 EP0834364B1 (fr) | 2001-07-04 |
Family
ID=31950970
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP97116428A Expired - Lifetime EP0834364B1 (fr) | 1996-09-25 | 1997-09-20 | Méthode et dispositif pour des machines de coulée continue à haute vitesse avec réduction d'épaisseur pendant la solidification |
Country Status (11)
Country | Link |
---|---|
US (2) | US6276436B1 (fr) |
EP (1) | EP0834364B1 (fr) |
JP (1) | JP4057119B2 (fr) |
CN (1) | CN1191898C (fr) |
AT (1) | ATE202735T1 (fr) |
AU (1) | AU753199B2 (fr) |
BR (1) | BR9707100A (fr) |
CA (1) | CA2226859C (fr) |
DE (2) | DE19639297C2 (fr) |
ES (1) | ES2160877T3 (fr) |
ZA (1) | ZA98204B (fr) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1050355A2 (fr) * | 1999-05-07 | 2000-11-08 | Sms Schloemann-Siemag Aktiengesellschaft | Procédé et installation pour la production d'un produit en acier coulé en continu |
EP1132161A1 (fr) * | 2000-03-10 | 2001-09-12 | SMS Demag AG | Procédé pour la coulée continue de brames, en particulier de brames minces |
AT408323B (de) * | 1999-12-01 | 2001-10-25 | Voest Alpine Ind Anlagen | Verfahren zum stahl-stranggiessen |
WO2002083340A2 (fr) * | 2001-04-14 | 2002-10-24 | Sms Demag Aktiengesellschaft | Augmentation d'epaisseur de format pour des installations de coulee continue pour brames minces |
WO2002085559A1 (fr) * | 2001-04-21 | 2002-10-31 | Sms Demag Aktiengesellschaft | Procede et dispositif pour produire une matiere de base de coulee continue |
WO2002090019A1 (fr) * | 2001-05-07 | 2002-11-14 | Sms Demag Aktiengesellschaft | Procede et dispositif permettant la coulee continue de blocs, de brames ou de brames minces |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10027324C2 (de) * | 1999-06-07 | 2003-04-10 | Sms Demag Ag | Verfahren zum Gießen eines metallischen Strangs sowie System hierzu |
DE19933635A1 (de) * | 1999-07-17 | 2001-01-18 | Sms Demag Ag | Verfahren und Vorrichtung zur Formatdickenänderung des Gußstranges einer Stranggießanlage im kontinuierlichen Gießbetrieb |
DE19956556A1 (de) * | 1999-11-24 | 2001-05-31 | Sms Demag Ag | Radien-Konfiguration der Strangführung einer Vertikalabbiege-Stranggießanlage |
ES2258438T3 (es) | 1999-12-15 | 2006-09-01 | Sms Demag Ag | Procedimiento para la modificacion del formato de una colada continua debajo de la coquilla de una instalacion de fundicion de colada continua. |
DE10057160A1 (de) | 2000-11-16 | 2002-05-29 | Sms Demag Ag | Verfahren und Vorrichtung zum Herstellen von Dünnbrammen |
KR100701185B1 (ko) | 2001-05-23 | 2007-03-29 | 주식회사 포스코 | 세그먼트 제로 소프트리덕션 장치 |
ITMI20021996A1 (it) * | 2002-09-19 | 2004-03-20 | Giovanni Arvedi | Procedimento e linea di produzione per la fabbricazione di nastro a caldo ultrasottile sulla base della tecnologia della bramma sottile |
DE102005055529B4 (de) * | 2005-11-22 | 2013-03-07 | Sms Siemag Aktiengesellschaft | Verfahren und Computerprogramm zum Herstellen einer Probe aus einem Stranggussmaterial |
DE102006048511A1 (de) | 2006-10-13 | 2008-04-17 | Sms Demag Ag | Strangführungsvorrichtung und Verfahren für deren Betrieb |
BRPI0818962B1 (pt) * | 2007-11-19 | 2017-07-04 | Posco | Continuous injection plate and method for manufacturing the same |
WO2010051981A1 (fr) * | 2008-11-04 | 2010-05-14 | Sms Siemag Ag | Procédé et dispositif de commande de la solidification d'une barre de coulée dans une installation de coulée continue lors de la mise en marche du processus de coulée |
ITMI20120046A1 (it) * | 2012-01-18 | 2013-07-19 | Arvedi Steel Engineering S P A | Impianto e procedimento per la colata continua veloce di bramme sottili di acciaio e di bramme di acciaio |
CN107081412B (zh) * | 2017-04-01 | 2019-08-09 | 唐山钢铁集团有限责任公司 | 高品质塑料模具钢特厚板连铸母坯的制备方法 |
CN108941493A (zh) * | 2018-08-30 | 2018-12-07 | 东北大学 | 一种实验室用小方坯立式连铸机辊列及其使用方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3501422A1 (de) * | 1984-02-16 | 1985-08-22 | Voest-Alpine Ag, Linz | Durchlaufkokille fuer eine stranggiessanlage |
EP0350431A2 (fr) * | 1988-07-04 | 1990-01-10 | MANNESMANN Aktiengesellschaft | Procédé de coulée continue pour la fabrication de brames avec une épaisseur réduite en présence d'état brut de coulée |
EP0611610A1 (fr) * | 1993-02-16 | 1994-08-24 | Voest-Alpine Industrieanlagenbau Gmbh | Procédé pour la production d'un feuillard, d'un feuillard ébauché ou d'une brame |
DE4436328A1 (de) * | 1993-10-14 | 1995-04-20 | Voest Alpine Ind Anlagen | Verfahren und Anlage zum Stranggießen |
DE19639302A1 (de) * | 1996-09-25 | 1998-03-26 | Schloemann Siemag Ag | Verfahren und Vorrichtung zur Erzeugung von dünnen Brammen auf einer Stranggießanlage |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4139242C3 (de) | 1991-11-26 | 1999-08-19 | Mannesmann Ag | Verfahren zur Erzeugung von Langprodukten aus Stahl |
DE4403049C1 (de) * | 1994-01-28 | 1995-09-07 | Mannesmann Ag | Stranggießanlage und Verfahren zur Erzeugung von Dünnbrammen |
DE4403048C1 (de) * | 1994-01-28 | 1995-07-13 | Mannesmann Ag | Stranggießanlage und Verfahren zur Erzeugung von Rechteck-Dünnbrammen |
JP3008821B2 (ja) * | 1994-07-29 | 2000-02-14 | 住友金属工業株式会社 | 薄鋳片の連続鋳造方法および装置 |
IT1280171B1 (it) * | 1995-05-18 | 1998-01-05 | Danieli Off Mecc | Linea di colata verticale per bramme |
-
1996
- 1996-09-25 DE DE19639297A patent/DE19639297C2/de not_active Expired - Fee Related
-
1997
- 1997-09-20 EP EP97116428A patent/EP0834364B1/fr not_active Expired - Lifetime
- 1997-09-20 ES ES97116428T patent/ES2160877T3/es not_active Expired - Lifetime
- 1997-09-20 AT AT97116428T patent/ATE202735T1/de active
- 1997-09-20 DE DE59703945T patent/DE59703945D1/de not_active Expired - Lifetime
- 1997-12-16 BR BR9707100A patent/BR9707100A/pt not_active IP Right Cessation
- 1997-12-17 JP JP34813897A patent/JP4057119B2/ja not_active Expired - Lifetime
-
1998
- 1998-01-08 CN CNB981039030A patent/CN1191898C/zh not_active Expired - Lifetime
- 1998-01-08 US US09/004,430 patent/US6276436B1/en not_active Expired - Lifetime
- 1998-01-12 ZA ZA9800204A patent/ZA98204B/xx unknown
- 1998-01-12 AU AU51080/98A patent/AU753199B2/en not_active Ceased
- 1998-01-13 CA CA002226859A patent/CA2226859C/fr not_active Expired - Fee Related
-
2001
- 2001-05-11 US US09/854,202 patent/US20020017375A1/en not_active Abandoned
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3501422A1 (de) * | 1984-02-16 | 1985-08-22 | Voest-Alpine Ag, Linz | Durchlaufkokille fuer eine stranggiessanlage |
EP0350431A2 (fr) * | 1988-07-04 | 1990-01-10 | MANNESMANN Aktiengesellschaft | Procédé de coulée continue pour la fabrication de brames avec une épaisseur réduite en présence d'état brut de coulée |
EP0611610A1 (fr) * | 1993-02-16 | 1994-08-24 | Voest-Alpine Industrieanlagenbau Gmbh | Procédé pour la production d'un feuillard, d'un feuillard ébauché ou d'une brame |
DE4436328A1 (de) * | 1993-10-14 | 1995-04-20 | Voest Alpine Ind Anlagen | Verfahren und Anlage zum Stranggießen |
DE19639302A1 (de) * | 1996-09-25 | 1998-03-26 | Schloemann Siemag Ag | Verfahren und Vorrichtung zur Erzeugung von dünnen Brammen auf einer Stranggießanlage |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1050355A2 (fr) * | 1999-05-07 | 2000-11-08 | Sms Schloemann-Siemag Aktiengesellschaft | Procédé et installation pour la production d'un produit en acier coulé en continu |
EP1050355A3 (fr) * | 1999-05-07 | 2001-03-28 | Sms Schloemann-Siemag Aktiengesellschaft | Procédé et installation pour la production d'un produit en acier coulé en continu |
KR100707785B1 (ko) * | 1999-05-07 | 2007-04-13 | 에스엠에스 데마그 악티엔게젤샤프트 | 연속적인 주물을 제조하는 방법 및 장치 |
AT408323B (de) * | 1999-12-01 | 2001-10-25 | Voest Alpine Ind Anlagen | Verfahren zum stahl-stranggiessen |
DE10058205C5 (de) * | 1999-12-01 | 2009-06-18 | Voest-Alpine Industrieanlagenbau Gmbh & Co. Kg | Verfahren zum Stahl-Stranggießen |
EP1132161A1 (fr) * | 2000-03-10 | 2001-09-12 | SMS Demag AG | Procédé pour la coulée continue de brames, en particulier de brames minces |
US6612364B2 (en) | 2000-03-10 | 2003-09-02 | Demag Aktiengesellschaft | Continuous casting method with soft reduction |
WO2002083340A2 (fr) * | 2001-04-14 | 2002-10-24 | Sms Demag Aktiengesellschaft | Augmentation d'epaisseur de format pour des installations de coulee continue pour brames minces |
WO2002083340A3 (fr) * | 2001-04-14 | 2002-12-19 | Sms Demag Ag | Augmentation d'epaisseur de format pour des installations de coulee continue pour brames minces |
WO2002085559A1 (fr) * | 2001-04-21 | 2002-10-31 | Sms Demag Aktiengesellschaft | Procede et dispositif pour produire une matiere de base de coulee continue |
WO2002090019A1 (fr) * | 2001-05-07 | 2002-11-14 | Sms Demag Aktiengesellschaft | Procede et dispositif permettant la coulee continue de blocs, de brames ou de brames minces |
US7025118B2 (en) | 2001-05-07 | 2006-04-11 | Sms Demag Aktiengesellschaft | Method and device for continuously casting ingots, slabs or thin slabs |
Also Published As
Publication number | Publication date |
---|---|
ES2160877T3 (es) | 2001-11-16 |
US20020017375A1 (en) | 2002-02-14 |
EP0834364A3 (fr) | 1998-10-28 |
ATE202735T1 (de) | 2001-07-15 |
ZA98204B (en) | 1998-06-24 |
JPH11179505A (ja) | 1999-07-06 |
AU753199B2 (en) | 2002-10-10 |
JP4057119B2 (ja) | 2008-03-05 |
US6276436B1 (en) | 2001-08-21 |
CA2226859C (fr) | 2006-11-07 |
DE19639297C2 (de) | 2000-02-03 |
BR9707100A (pt) | 1999-07-27 |
DE59703945D1 (de) | 2001-08-09 |
DE19639297A1 (de) | 1998-03-26 |
CA2226859A1 (fr) | 1999-07-13 |
CN1191898C (zh) | 2005-03-09 |
AU5108098A (en) | 1999-07-29 |
CN1222419A (zh) | 1999-07-14 |
EP0834364B1 (fr) | 2001-07-04 |
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