EP0710716A3 - Granulierte Bleichaktivatoren und ihre Herstellung - Google Patents

Granulierte Bleichaktivatoren und ihre Herstellung Download PDF

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Publication number
EP0710716A3
EP0710716A3 EP95116730A EP95116730A EP0710716A3 EP 0710716 A3 EP0710716 A3 EP 0710716A3 EP 95116730 A EP95116730 A EP 95116730A EP 95116730 A EP95116730 A EP 95116730A EP 0710716 A3 EP0710716 A3 EP 0710716A3
Authority
EP
European Patent Office
Prior art keywords
actuators
production
inorganic binder
granulated bleach
bleach activator
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP95116730A
Other languages
English (en)
French (fr)
Other versions
EP0710716B1 (de
EP0710716A2 (de
Inventor
Helmut Dr. Berenbold
Georg Borchers
Jürgen Dr. Cramer
Gerhard Nöltner
Gerd Dr. Reinhardt
Wilfried Schuler
Wolfgang Dr. Heininger
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Clariant Produkte Deutschland GmbH
Original Assignee
Hoechst AG
Clariant GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG, Clariant GmbH filed Critical Hoechst AG
Publication of EP0710716A2 publication Critical patent/EP0710716A2/de
Publication of EP0710716A3 publication Critical patent/EP0710716A3/de
Application granted granted Critical
Publication of EP0710716B1 publication Critical patent/EP0710716B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/395—Bleaching agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/39—Organic or inorganic per-compounds
    • C11D3/3902—Organic or inorganic per-compounds combined with specific additives
    • C11D3/3905—Bleach activators or bleach catalysts
    • C11D3/3935—Bleach activators or bleach catalysts granulated, coated or protected
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/126—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in solid compositions

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

Gegenstand der vorliegenden Erfindung ist ein Verfahren zur Herstellung eines lagerstabilen Granulates bestehend im wesentlichen aus einem Bleichaktivator und einem anorganischen Bindematerial, gekennzeichnet durch die Verfahrensschritte:
  • a) Vermischen eines trockenen Bleichaktivators mit einem trockenen anorganischen Bindematerial,
  • b) Verpressen dieser Mischung zu größeren Agglomeraten und
  • c) Zerkleinern dieser Agglomerate auf die gewünschte Korngröße.
    • Weiterer Gegenstand der Erfindung ist die Verwendung, der nach diesen Verfahren hergestellten Granulate in Wasch-, Reinigungs-, Blech- und Desinfektionsmitteln.
    EP95116730A 1994-11-02 1995-10-24 Granulierte Bleichaktivatoren und ihre Herstellung Expired - Lifetime EP0710716B1 (de)

    Applications Claiming Priority (2)

    Application Number Priority Date Filing Date Title
    DE4439039A DE4439039A1 (de) 1994-11-02 1994-11-02 Granulierte Bleichaktivatoren und ihre Herstellung
    DE4439039 1994-11-02

    Publications (3)

    Publication Number Publication Date
    EP0710716A2 EP0710716A2 (de) 1996-05-08
    EP0710716A3 true EP0710716A3 (de) 1998-07-08
    EP0710716B1 EP0710716B1 (de) 2002-07-24

    Family

    ID=6532247

    Family Applications (1)

    Application Number Title Priority Date Filing Date
    EP95116730A Expired - Lifetime EP0710716B1 (de) 1994-11-02 1995-10-24 Granulierte Bleichaktivatoren und ihre Herstellung

    Country Status (10)

    Country Link
    US (1) US5716569A (de)
    EP (1) EP0710716B1 (de)
    JP (1) JP4249271B2 (de)
    KR (1) KR100388367B1 (de)
    AT (1) ATE221114T1 (de)
    BR (1) BR9505059A (de)
    CA (1) CA2161943C (de)
    DE (2) DE4439039A1 (de)
    ES (1) ES2180602T3 (de)
    TW (1) TW353114B (de)

    Families Citing this family (14)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    US5843879A (en) * 1996-02-06 1998-12-01 Lion Corporation Bleaching activator granulate
    DE19641708A1 (de) 1996-10-10 1998-04-16 Clariant Gmbh Verfahren zur Herstellung eines gecoateten Bleichaktivatorgranulats
    DE19642491A1 (de) * 1996-10-15 1998-04-16 Basf Ag Flammwidrige thermoplastische Formmassen auf Basis von Polyphenylenethern und vinylaromatischen Polymeren
    KR100416934B1 (ko) * 1996-10-31 2004-05-20 주식회사 엘지생활건강 캡슐화된 표백활성화제
    DE19740671A1 (de) * 1997-09-16 1999-03-18 Clariant Gmbh Bleichaktivator-Granulate
    DE19740668A1 (de) 1997-09-16 1999-03-18 Clariant Gmbh Lagerstabiles Bleichaktivator-Granulat
    KR100497521B1 (ko) * 1998-04-08 2005-09-14 주식회사 엘지생활건강 캡슐형 세탁용 세제의 제조방법
    DE19908051A1 (de) * 1999-02-25 2000-08-31 Henkel Kgaa Verfahren zur Herstellung compoundierter Acetonitril-Derivate
    DE10334046A1 (de) * 2003-07-25 2005-02-10 Clariant Gmbh Verfahren zur Herstellung von granulierten Acyloxybenzolsulfonaten oder Acyloxybenzolcarbonsäuren und deren Salze
    US9371556B2 (en) 2004-03-05 2016-06-21 Gen-Probe Incorporated Solutions, methods and kits for deactivating nucleic acids
    DE102004043360A1 (de) * 2004-09-08 2006-03-09 Clariant Gmbh Bleichaktivator-Mischungen
    KR101069043B1 (ko) * 2005-07-06 2011-09-29 주식회사 엘지생활건강 표백활성화제 입자의 제조방법 및 이로부터 형성된표백활성화제 입자
    EP1847590B1 (de) * 2006-04-20 2013-06-19 The Procter & Gamble Company Verfahren zur Herstellung von Bleichpartikeln
    US7709437B2 (en) * 2006-04-27 2010-05-04 Oci Chemical Corp. Co-granulates of bleach activator-peroxide compounds

    Citations (6)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    EP0051987A1 (de) * 1980-11-06 1982-05-19 THE PROCTER & GAMBLE COMPANY Bleichaktivatorzusammensetzungen, deren Herstellung und Anwendung in granulierten Reinigungsmittelzusammensetzungen
    US4695397A (en) * 1981-09-28 1987-09-22 Basf Aktiengesellschaft Granular bleaching activator
    EP0240057A1 (de) * 1986-03-25 1987-10-07 Unilever N.V. Körnige kein Phosphor enthaltende Bleichaktivatorzusammensetzungen und ihre Verwendung in körnigen Detergensbleichmittelzusammensetzungen
    GB2249104A (en) * 1990-10-23 1992-04-29 Bp Chem Int Ltd Bleach activators
    US5182054A (en) * 1989-08-19 1993-01-26 Henkel Kommanditgesellschaft Auf Aktien Process for granulating perborate monohydrate
    US5203877A (en) * 1990-08-16 1993-04-20 Peroxid-Chemie Gmbh Process for producing sodium perborate monohydrate agglomerate

    Family Cites Families (23)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    DE2048331A1 (de) * 1970-10-01 1972-04-06 Henkel & Cie GmbH, 4000 Dusseldorf Feste, pulverförmige bis kornige Mittel zur Herstellung von kaltwirksamen Bleich flotten, insbesondere von kaltwirksamen blei chenden Waschlaugen, und Verfahren zur Her stellung dieser Mittel
    GB1368400A (en) 1971-08-05 1974-09-25 Procter & Gamble Bleaching process and compositions therefor
    GB1507312A (en) 1974-12-04 1978-04-12 Unilever Ltd Encapsulation of particles
    DE2733849A1 (de) 1977-07-27 1979-02-15 Basf Ag Feste kaltbleichaktivatoren fuer aktivsauerstoff abgebende verbindungen enthaltende wasch- und reinigungsmittel
    DE3011998C2 (de) 1980-03-28 1982-06-16 Henkel KGaA, 4000 Düsseldorf Verfahren zur Herstellung eines lagerstabilen, leichtlöslichen Granulates mit einem Gehalt an Bleichaktivatoren
    US4399049A (en) 1981-04-08 1983-08-16 The Procter & Gamble Company Detergent additive compositions
    DE3128336A1 (de) 1981-07-17 1983-01-27 Henkel KGaA, 4000 Düsseldorf "verfahren zur herstellung umhuellter koerniger bleichaktivatoren"
    GB8311865D0 (en) * 1983-04-29 1983-06-02 Procter & Gamble Ltd Bleach compositions
    US4539130A (en) * 1983-12-22 1985-09-03 The Procter & Gamble Company Peroxygen bleach activators and bleaching compositions
    DE3644564A1 (de) * 1986-12-27 1988-07-07 Henkel Kgaa Verfahren zur herstellung von rieselfaehigen, stabilen persaeure-konzentraten durch kompaktierende granulation
    US4889651A (en) 1988-01-21 1989-12-26 Colgate-Palmolive Company Acetylated sugar ethers as bleach activators and detergency boosters
    US5318714A (en) * 1988-03-14 1994-06-07 Novo Nordisk A/S Stabilized particulate composition
    DE3826092A1 (de) 1988-08-01 1990-02-08 Henkel Kgaa Granulares, bleichaktivatoren enthaltendes bleichhilfsmittel mit verbesserten eigenschaften
    DE4010533A1 (de) * 1990-04-02 1991-10-10 Henkel Kgaa Tablettierte wasch- und/oder reinigungsmittel fuer haushalt und gewerbe und verfahren zu ihrer herstellung
    GB8925621D0 (en) * 1989-11-13 1990-01-04 Unilever Plc Process for preparing particulate detergent additive bodies and use thereof in detergent compositions
    DK17290D0 (de) 1990-01-22 1990-01-22 Novo Nordisk As
    US5047163A (en) 1990-03-16 1991-09-10 Lever Brothers Company, Division Of Conopco, Inc. Activation of bleach precursors with sulfonimines
    DE69125310T2 (de) * 1990-05-21 1997-07-03 Unilever Nv Bleichmittelaktivierung
    DE4024759A1 (de) * 1990-08-03 1992-02-06 Henkel Kgaa Bleichaktivatoren in granulatform
    DE69030443T2 (de) * 1990-12-28 1997-11-13 Ausimont Spa Verfahren zur Erhöhung der Bleichwirksamkeit von anorganischen Persalzen
    GB9102507D0 (en) 1991-02-06 1991-03-27 Procter & Gamble Peroxyacid bleach precursor compositions
    US5411673A (en) * 1991-02-06 1995-05-02 The Procter & Gamble Company Peroxyacid bleach precursor compositions
    AU4777093A (en) 1992-08-01 1994-03-03 Procter & Gamble Company, The Peroxyacid bleach precursor compositions

    Patent Citations (6)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    EP0051987A1 (de) * 1980-11-06 1982-05-19 THE PROCTER & GAMBLE COMPANY Bleichaktivatorzusammensetzungen, deren Herstellung und Anwendung in granulierten Reinigungsmittelzusammensetzungen
    US4695397A (en) * 1981-09-28 1987-09-22 Basf Aktiengesellschaft Granular bleaching activator
    EP0240057A1 (de) * 1986-03-25 1987-10-07 Unilever N.V. Körnige kein Phosphor enthaltende Bleichaktivatorzusammensetzungen und ihre Verwendung in körnigen Detergensbleichmittelzusammensetzungen
    US5182054A (en) * 1989-08-19 1993-01-26 Henkel Kommanditgesellschaft Auf Aktien Process for granulating perborate monohydrate
    US5203877A (en) * 1990-08-16 1993-04-20 Peroxid-Chemie Gmbh Process for producing sodium perborate monohydrate agglomerate
    GB2249104A (en) * 1990-10-23 1992-04-29 Bp Chem Int Ltd Bleach activators

    Also Published As

    Publication number Publication date
    CA2161943A1 (en) 1996-05-03
    KR960017832A (ko) 1996-06-17
    ATE221114T1 (de) 2002-08-15
    EP0710716B1 (de) 2002-07-24
    US5716569A (en) 1998-02-10
    EP0710716A2 (de) 1996-05-08
    DE4439039A1 (de) 1996-05-09
    TW353114B (en) 1999-02-21
    ES2180602T3 (es) 2003-02-16
    CA2161943C (en) 2007-02-06
    JPH08209192A (ja) 1996-08-13
    JP4249271B2 (ja) 2009-04-02
    BR9505059A (pt) 1997-10-14
    DE59510290D1 (de) 2002-08-29
    KR100388367B1 (ko) 2003-09-22

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