EP0286141B1 - Lubrifiant ou concentré de lubrifiant - Google Patents
Lubrifiant ou concentré de lubrifiant Download PDFInfo
- Publication number
- EP0286141B1 EP0286141B1 EP88105727A EP88105727A EP0286141B1 EP 0286141 B1 EP0286141 B1 EP 0286141B1 EP 88105727 A EP88105727 A EP 88105727A EP 88105727 A EP88105727 A EP 88105727A EP 0286141 B1 EP0286141 B1 EP 0286141B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- lubricant
- mpa
- weight
- oil
- viscosity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M101/00—Lubricating compositions characterised by the base-material being a mineral or fatty oil
- C10M101/02—Petroleum fractions
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M101/00—Lubricating compositions characterised by the base-material being a mineral or fatty oil
- C10M101/04—Fatty oil fractions
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
- C10M105/02—Well-defined hydrocarbons
- C10M105/06—Well-defined hydrocarbons aromatic
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- C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
- C10M105/08—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing oxygen
- C10M105/18—Ethers, e.g. epoxides
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
- C10M105/08—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing oxygen
- C10M105/32—Esters
- C10M105/36—Esters of polycarboxylic acids
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- C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
- C10M105/08—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing oxygen
- C10M105/32—Esters
- C10M105/38—Esters of polyhydroxy compounds
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- C10M105/40—Esters containing free hydroxy or carboxyl groups
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- C10M107/00—Lubricating compositions characterised by the base-material being a macromolecular compound
- C10M107/02—Hydrocarbon polymers; Hydrocarbon polymers modified by oxidation
- C10M107/08—Hydrocarbon polymers; Hydrocarbon polymers modified by oxidation containing butene
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- C10M107/20—Lubricating compositions characterised by the base-material being a macromolecular compound containing oxygen
- C10M107/22—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C10M107/28—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate
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- C10M107/30—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M107/32—Condensation polymers of aldehydes or ketones; Polyesters; Polyethers
- C10M107/34—Polyoxyalkylenes
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- C10M129/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen
- C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
- C10M129/16—Ethers
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- C10M129/74—Esters of polyhydroxy compounds
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- C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
- C10M129/68—Esters
- C10M129/76—Esters containing free hydroxy or carboxyl groups
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- C10M135/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing sulfur, selenium or tellurium
- C10M135/12—Thio-acids; Thiocyanates; Derivatives thereof
- C10M135/14—Thio-acids; Thiocyanates; Derivatives thereof having a carbon-to-sulfur double bond
- C10M135/18—Thio-acids; Thiocyanates; Derivatives thereof having a carbon-to-sulfur double bond thiocarbamic type, e.g. containing the groups
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- C10M135/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing sulfur, selenium or tellurium
- C10M135/32—Heterocyclic sulfur, selenium or tellurium compounds
- C10M135/36—Heterocyclic sulfur, selenium or tellurium compounds the ring containing sulfur and carbon with nitrogen or oxygen
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- C10M137/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing phosphorus
- C10M137/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing phosphorus having no phosphorus-to-carbon bond
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- C10M137/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing phosphorus
- C10M137/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing phosphorus having no phosphorus-to-carbon bond
- C10M137/04—Phosphate esters
- C10M137/10—Thio derivatives
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- C10M141/00—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential
- C10M141/10—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential at least one of them being an organic phosphorus-containing compound
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- C10M161/00—Lubricating compositions characterised by the additive being a mixture of a macromolecular compound and a non-macromolecular compound, each of these compounds being essential
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- C10M169/06—Mixtures of thickeners and additives
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- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/06—Well-defined aromatic compounds
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Definitions
- the invention relates to a new lubricant or lubricant concentrate based on mineral oil and / or synthetic oil with improved lubricating properties, in particular improved load bearing, sliding and corrosion protection properties.
- solid lubricants were developed which were introduced between the moving metal parts, such as graphite, MoS2, TiO2, Ca3 (PO4) 2, Teflon and the like, which were introduced as lubricious outer layers, suspensions, pastes or greases. Thereby the friction partners were better separated and their resilience increased. With centripetal movements of higher peripheral speed and at higher temperature, however, the solid lubricants and carrier media separate sooner or later due to their different specific densities. This limited the long-term lubrication. In a further step, it was possible to apply suitable metal cations to rubbing surfaces during operation from chemical complexes dissolved in a lubricant.
- DE-PS 941 678 discloses lubricating oils containing soluble reaction products of phosphorus pentasulfide with liquid or solid aliphatic hydrocarbons or terpene hydrocarbons.
- a lubricating oil is known which contains metal-containing alkylphenol sulfide esters in combination with zinc sulfonates.
- DE-AS 1 444 892 a lubricating oil is known which contains a salt of an aromatic zinc dithiophosphate and a zinc carboxylic acid salt in the presence of water. While the first two products are lubricating oil detergents, the latter product is intended to prevent corrosion of silver bearing surfaces.
- a lubricating oil which contains a salt of a substituted succinic acid, optionally together with a salt of an alkylated or esterified phosphoric acid. It is an antioxidant with a detergent effect.
- a combination of dithiophosphate and dithiophosphinate salts is known from DE-AS 1 271 878.
- From DE-OS 15 94 555 cutting oils containing free sulfur, a dialkyldithiophosphate and a chlorinated hydrocarbon are known.
- Lubricating oils containing zinc or antimondithiocarbamate are known from US Pat. No. 3,462,367. Lubricating oils are known from US Pat. No.
- Lubricating oil additives are also known from US Pat. No. 2,734,864, which are formed from a dithiophosphate of the alkaline earth metal salts in combination with a complex reaction product of phosphorus sulfides, wool fat and alcohol esters.
- the undefined product contains considerable amounts of barium and zinc.
- Such a lubricating oil additive cannot be used in practice because of its unbearable odor, which also endangers the people who come into contact with it.
- lubricants based on mineral oil or synthetic oil which, in addition to the mineral or synthetic oil, contain an ester of an epoxidized fatty acid having 10 to 18 carbon atoms with mono- or polyhydric alcohols, an alkyl -, Aralkyl- or aryldithiophosphate of zinc, lead, tin, tungsten, molybdenum, niobium or lanthanum and optionally contain a sulfur phosphorus compound.
- lubricants based on mineral or synthetic oil or lubricant concentrates which, in addition to a lead, tungsten, molybdenum and / or vanadium dithiophosphate esterified with alkyl, aryl or aralkyl groups, also contain at least one zinc dialkyldithiophosphate - And contain a metal-free sulfur-phosphorus compound.
- These last-mentioned lubricants which have found widespread use, no longer meet all of the requirements placed on modern long-term and high-performance lubricants. Their coefficient of friction and abrasion are too high, their shelf life is inadequate, and long-term use shows that the complaint rate in the lubrication area is too high.
- the object of the invention was therefore to create a new lubricant or lubricant concentrate based on mineral or synthetic oil which is further improved with regard to its lubricating properties, in particular its friction and wear properties, thus noticeably reducing the energy and spare parts requirement and thus also meets the highest requirements.
- this object can be achieved according to the invention by adding at least one compound to a mineral and / or synthetic oil in addition to the usual additives which has at least one quaternary carbon atom and at least one ester and / or ether bond in the molecule .
- the lubricants or lubricant concentrates according to the invention have significantly improved properties compared to the known lubricants or lubricant concentrates, in particular with regard to friction and wear, and thus a reduced need for energy and spare parts. It is believed that this is due to the fact that when they are used in the rubbing and sliding area, metallic glass surfaces are formed from amorphously solidified metal melts, which no longer have metal crystal lattice structures.
- the glass-like smooth friction and sliding surfaces which are probably generated with the lubricant or lubricant concentrate according to the invention, significantly improve the entire lubrication process, since the Coefficient of friction and with it the abrasion, oxidation and corrosion are significantly reduced.
- the so-called fretting rust is also prevented by the lubricant or lubricant concentrate according to the invention.
- the lubricants or lubricant concentrates according to the invention are extremely environmentally friendly since they contain no lead, no sulfurized whale sperm oil and hardly any phosphorus. This has been shown by fish tests and bacterial growth tests which were carried out with the lubricants or lubricant concentrates according to the invention. It was also found that they are 60% biodegradable in normal soil within 3 to 4 months, so that they can also be described as extremely environmentally friendly.
- the compounds containing quaternary carbon atoms used according to the invention are thermally very stable and therefore allow high operating temperatures of up to 300 ° C. They therefore open up the possibility of lifetime lubrication of highly loaded motors, turbines, rolling bearings, constant velocity joints and other high-performance machine elements.
- lubricant or lubricant concentrate based on mineral and / or synthetic oil used here means both lubricating oils and lubricating greases based on mineral and / or synthetic oil.
- Compounds containing quaternary carbon atoms are to be understood here as those compounds in which the four main valences of at least one carbon atom per molecule are occupied by four carbon atoms.
- Such compounds are mono-, di- and trimeric Pentaerythritol esters, other polyol esters, pentaerythritol ethoxy esters, pentaerythrity ethers and pentaerythritol ethoxy ethers as well as adamantane ester or ether derivatives or telomeric acid diolesters or neopentyl polyol esters and the corresponding ethoxylated esters and ethers.
- the lubricants or lubricant concentrates according to the invention have significantly improved properties compared to the known lubricants or lubricant concentrates, as the examples below show.
- the glass-like smooth friction and sliding surfaces produced by the lubricant according to the invention save drive energy and lower the coefficient of friction per se and by building up a very adhesive boundary lubrication film which enables elastohydrodynamic lubrication even under point loads.
- the friction temperature of the lubricant and lubrication point is reduced, the oxidation resistance of both is extended and the metallic friction partners are subjected to less specific alternating loads and temperatures. Overall, these effects greatly reduce wear and significantly increase the service life of the friction partners and the lubricant.
- the lubricant or lubricant concentrate contains, as compound A, a compound having 1 to 3 quaternary carbon atoms and optionally additionally at least one free one Hydroxyl group in the molecule, the compound A preferably having a density d20 of at least 0.900 and an enthalpy H of at least 350 kcal / kg.
- a 4-to 8-valent alcohol with at least one quaternary carbon atom and at least one ester and / or ether bond in the molecule with a density d20 of at least 0.900 and an enthalpy H of at least 350 kcal / kg is used as compound A according to the invention.
- the compound A used according to the invention is selected from the mono-, di- and tripentaerythritol ester and / or ether derivatives, the adamantane esters and / or ether derivatives, the telomeric acid diesters and / or neopentyl polyol esters, preferably the telomeric acid neopentyl glycol, trimethylol propane and / / or pentaerythritol esters and their ethoxylated derivatives.
- the lubricant or lubricant concentrate contains the compound A in an amount of 0.1 to 40% by weight, preferably 0.1 to 20% by weight, in particular 1 to 12% by weight, especially 1 , 5 to 8 wt .-%, based on the weight of the mineral and / or synthetic oil.
- the lubricant or lubricant concentrate according to the invention preferably contains beet oil, natural oil and / or a synthetic oil with a viscosity in the range from 1.0 mPa.s at 20 ° C to 2.106 mPa.s at 20 ° C.
- a mineral oil with a viscosity is particularly preferred from 1.0 mPa.s at 20 ° C to 540 mPa.s at 50 ° C as a natural oil and the use of an aromatic or aliphatic dicarboxylic acid ester, in particular poly- ⁇ -olefin dicarboxylic acid ester, especially butyl ester, with a molecular weight in the range from 1000 to 3000, preferably of diisocyanate phthalate, trimethyladipate and dioctyl sebacate, a polyisobutylene with a molecular weight of 1000 to 100,000 and a viscosity of 200 to 43,000 mPa.s at 100 ° C, a polymethacrylate with a viscosity of 1000 mPa.s at 100 ° C , a non-water-soluble polyglycol with a viscosity of 5 to 60 mPa.s at 100 ° C, an isoparaffin oil and /
- lubricant according to the invention and lubricant concentrate preferably contains a sulfur carrier, particularly a thiazole, at least one metal dialkyldithiocarbamate and / or a metal dialkyldithiophosphate and / or a phosphorus carrier, in particular an organo phosphite, preferably a Dialkylarylphosphit, particularly didecyl or Didodecylphenylphosphit, and / or a metal dialkyldithiophosphate .
- a sulfur carrier particularly a thiazole
- at least one metal dialkyldithiocarbamate and / or a metal dialkyldithiophosphate and / or a phosphorus carrier in particular an organo phosphite, preferably a Dialkylarylphosphit, particularly didecyl or Didodecylphenylphosphit, and / or a metal dialkyldithiophosphate
- the sulfur carrier is preferably present in the lubricant or lubricant concentrate in an amount of 0.5 to 10% by weight, in particular 1 to 3% by weight, while the phosphorus carrier is preferably present in an amount of 0.1 to 10 % By weight, in particular from 0.1 to 5% by weight, especially from 0.5 to 2% by weight.
- the lubricant or lubricant concentrate according to the invention can contain conventional antioxidants, metal deactivators, detergents, dispersants, antifoams and / or viscosity index improvers as further conventional additives.
- the additives according to the invention can be added individually or in the form of a composition as a concentrate to the carrier medium (base oil or base fat) in the amounts mentioned above.
- pentaerythritol ester examples include pentaerythritol monohexyl, pentaerythritol monooctyl, pentaerythritol moncnonylester, pentaerythritol monodecylester, pentaerythritol monododecylester, pentaerythritol monomyristylester, pentaerythritol monohexadecylester, pentaerythritol monostearyl ester, pentaerythritol monooleylester, pentaerythritol monoisostearyl- and -isopalmitinklarester; the corresponding dihexyl, dioctyl, dinonyl, didecyl, didodecyl, dimyristyl, dihexadecyl, distearyl, dioleyl, diiso
- telomeric acids are compounds with relatively high molecular weights and long-chain, star-branched structures which can be esterified in the usual way and whose esters are valuable lubricants (commercial product Kortacid T from Akzo Chemie).
- Mineral oils which can be used according to the invention are all the usual mineral oils, from isoparaffin oil with a viscosity of 1.0 mPa.s at 20 ° C to thin spindle oil with a viscosity of 12 mPa.s at 20 ° C to highly viscous bright stock and cylinder oil with a viscosity of 540 mPa .s at 50 ° C.
- Ucolub N9 with a viscosity of 5.7 mPa.s at 100 ° C
- Ucolub N36A with a viscosity of 18 mPa.s at 100 ° C
- Ucolub N 120A with a viscosity of 55 mPa.s at 100 ° C (all non-water-soluble polyglycols) from Union Carbide
- Isopar J from Esso (an isoparaffin oil) with a viscosity at 20 ° C of 1.0 mPa.s.
- organophosphorus compounds which can be used as phosphorus supports according to the invention are compounds of the formula in which R in each case denotes a straight-chain, branched or cyclic alkyl group having 6 to 12 carbon atoms or phenyl group substituted in the o- or p-position by a lower alkyl radical having 1 to 6 carbon atoms.
- organophosphorus compounds of the above formula are monodecyl diphenyl phosphite, didecylphenyl phosphite, triphenyl phosphite, dioctyl phenyl phosphite, dihexyl phenyl phosphite, diisodecyl phenyl phosphite, diisooctyl phenyl phosphite, didecyl p-methylphenylphosphite.
- the metal dialkyldithiocarbamates which can be used according to the invention as sulfur carriers are compounds of the formula wherein Me is a metal from the group copper, silver, zinc, cadmium, boron, titanium, zirconium, tin, lead, vanadium, tantalum, antimony, chromium, molybdenum, tungsten, manganese, cobalt and nickel, preferably boron, nickel, cobalt or Molybdenum means.
- the metal dialkyldithiophosphates which can be used according to the invention both as a sulfur carrier and as a phosphorus carrier are compounds of the formula wherein Me for a metal from the group copper, silver, zinc, cadmium, boron, titanium, zirconium, tin, lead, vanadium, tantalum, antimony, chromium, molybdenum, tungsten, manganese, cobalt and nickel, preferably for zinc, nickel, Titanium, vanadium, molybdenum, tungsten and manganese.
- the alkyl group in the above-mentioned metal dialkyldithiocarbamates and metal dialkyldithiophosphates each preferably contain 4 to 8 carbon atoms, so that the metal salts mentioned are still soluble in the commercially available base oils.
- particularly advantageous alkyl groups include the n-, i- and tert-butyl group, the n- and i-amyl group, the n- and i-hexyl group, the n- and i-heptyl group and the 2-ethylhexyl group.
- the i-butyl group, the n- and i-amyl group and the 2-ethylhexyl group are very particularly preferred.
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Engineering & Computer Science (AREA)
- Lubricants (AREA)
Claims (8)
- Un lubrifiant ou concentré de lubrifiant à base d'une huile minérale et/ou synthétique contenant au moins un compose comportant au moins un atome de carbone quaternaire et au moins une liaison esterique et/ou éthérique dans la molécule et autres additives usuels,
characterisé en ce qu'il contienta) au moins un composé comportant de 1 à 3 atomes de carbone quaternaires et au moins un groupe hydroxyle libre dans la molécule ayant une densité d₂₀ d'au moins 0,900 et une enthalpie ΔH d'au moins 350 kcal/kg, choisi parmi le groupe des esters et éthers de mono-, di- et tri-pentaerythritole, des esters et éthers d'adamantane, des esters et éthers des dérivés d'adamantane étant substitués en 1- ou 2-position par -COOH,-CH₂OH ou -C₂H₅OH, et des diolesters et néopentylglycolesters de l'acide télomèrique et leurs dérivés éthoxylés, les groupes esteriques et éthériques étant des groupes alkyles, aralkyles ou aryles comportant de 6 à 18 atomes de carbone,b) au moins un dialkyldithiocarbamate de métal ayant la formule généraleMe représente un métal choisi parmi le groupe de cuivre, argent, zinc, cadmium, bore, titane, zirconium, étain, plomb, vanadium, tantale, antimoine, chrome, molybdène, tungstène, manganèse, cobalt et nickel etAlkyl représente un groupe alkyle comportant de 4 à 8 atomes de carbone, etc) comme autres additives usuels des agents antioxidants, des desactivateurs de métal, des détergents, des agents dispersants, des agents antimousses et/ou des agents améliorants la viscosité, connus en soi. - Le lubrifiant ou concentré de lubrifiant selon la revendication 1, characterisé en ce qu'il contient comme une autre composante(d) au moins un dialkyldithiophosphate de métal ayant la formule généraleMe représente un métal choisi parmi le groupe de cuivre, argent, zinc, cadmium, bore, titane, zirconium, étain, plomb, vanadium, tantale, antimoine, chrome, molybdène, tungstène, manganèse, cobalt et nickel etAlkyl représente un groupe alkyle comportant de 4 à 8 atomes de carbone.
- Le lubrifiant ou concentré de lubrifiant selon la revendication 1 ou 2, characterisé en ce qu'il contient la composante (a) en une quantité de 0,1 à 40 % en poids, préférablement de 0,1 à 20 % en poids, en particulier de 1 à 12 % en poids, spécialement de 1,5 à 8 % en poids, par rapport au poids de l'huile minérale et/ou synthétique.
- Le lubrifiant ou concentré de lubrifiant selon l'une des revendications 1 à 3, characterisé en ce qu'il contient comme huile de base une huile de navette, une huile naturelle et/ou une huile synthétique ayant une viscosité de 1,0 mPa.s à 20°C à 2.10⁶ mPa.s à 20°C.
- Le lubrifiant ou concentré de lubrifiant selon la revendications 4, characterisé en ce qu'il contient comme huile de base une huile synthétique ayant une viscosité de 1,0 mPa.s à 20°C à 540 mPa.s à 50°C.
- Le lubrifiant ou concentré de lubrifiant selon la revendication 4, characterisé en ce qu'il contient comme huile synthétique un ester d'un acide aromatique ou aliphatique, en particulier un ester d'un acide poly-α-olefin-dicarboxylique, spécialement le butylester, ayant un poids moléculaire de 1000 à 3000, préférablement le diisodecylester de l'acide phtalique, le didecylester de l'acide trimethyladipinique et le dioctylester de l'acide sébacique, un polyisobutylène ayant un poids moléculaire de 1000 à 100 000 et une viscosité de 200 à 43 000 mPa.s à 100°C, un polymethacrylate ayant une viscosité de 100 mPa.s à 100°C, un polyglycol non-soluble dans l'eau ayant une viscosité de 5 à 60 mPa.s à 100°C, une huile isoparaffinique et/ou un alkylbenzène ayant un point d'inflammation de plus de 50°C et une viscosité de 1,0 mPa.s à 20°C à 2 000 000 mPa.s à 20°C.
- Le lubrifiant ou concentré de lubrifiant selon l'une des revendications 1 à 6, characterisé en ce qu'il contient le(les) composé(s) comportant du soufre en une quantité de 0,5 à 10 % en poids, préférablement de 1 à 3 % en poids.
- Le lubrifiant ou concentré de lubrifiant selon l'une des revendications 2 à 7, characterisé en ce qu'il contient le(les) composé(s) comportant du phosphore en une quantité de 0,1 à 10 % en poids, préférablement de 0,1 à 5 % en poids, spécialement de 0,5 à 2 % en poids.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19873712132 DE3712132A1 (de) | 1987-04-10 | 1987-04-10 | Schmiermittel bzw. schmiermittelkonzentrat |
DE3712132 | 1987-04-10 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0286141A1 EP0286141A1 (fr) | 1988-10-12 |
EP0286141B1 true EP0286141B1 (fr) | 1994-09-07 |
Family
ID=6325304
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP88105727A Expired - Lifetime EP0286141B1 (fr) | 1987-04-10 | 1988-04-11 | Lubrifiant ou concentré de lubrifiant |
Country Status (7)
Country | Link |
---|---|
EP (1) | EP0286141B1 (fr) |
JP (1) | JP2853135B2 (fr) |
AT (1) | ATE111151T1 (fr) |
CA (1) | CA1339482C (fr) |
DE (2) | DE3712132A1 (fr) |
ES (1) | ES2063743T3 (fr) |
WO (1) | WO1988008023A1 (fr) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0816230B2 (ja) * | 1988-10-20 | 1996-02-21 | 日本石油株式会社 | 2サイクルエンジン油組成物 |
EP0430657A1 (fr) * | 1989-11-29 | 1991-06-05 | Asahi Denka Kogyo Kabushiki Kaisha | Lubrifiant pour réfrigérateurs |
DE4214653A1 (de) * | 1992-05-02 | 1993-11-04 | Henkel Kgaa | Motorengrundoele mit verbesserter dichtungsvertraeglichkeit |
EP0612832B1 (fr) * | 1992-12-07 | 1998-07-22 | Idemitsu Kosan Company Limited | Huile hydraulique ignifuge |
FR2986801B1 (fr) * | 2012-02-15 | 2014-09-05 | Total Raffinage Marketing | Compositions lubrifiantes pour transmissions |
JP6544953B2 (ja) * | 2014-05-29 | 2019-07-17 | 株式会社リコー | 画像形成装置及びグリース組成物 |
WO2017222018A1 (fr) * | 2016-06-23 | 2017-12-28 | Jxtgエネルギー株式会社 | Composition de graisse pour joints homocinétiques, et joint homocinétique dans lequel ladite composition de graisse est scellée |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1543830A (fr) * | 1966-11-10 | 1968-10-25 | Mobil Oil Corp | Compositions lubrifiantes contenant des additifs anti-corrosion perfectionnés |
FR2051665A1 (fr) * | 1969-07-10 | 1971-04-09 | Ethyl Corp | |
JPS5328862B2 (fr) * | 1972-04-18 | 1978-08-17 | ||
US3843542A (en) * | 1972-07-31 | 1974-10-22 | Chevron Res | Hydraulic oil |
IT1010487B (it) * | 1974-05-08 | 1977-01-10 | Snam Progetti | Esteri come componenti di lubrifi canti |
US3896050A (en) * | 1974-07-05 | 1975-07-22 | Texaco Inc | Lubricating oil additives |
US3962105A (en) * | 1975-03-25 | 1976-06-08 | The Lubrizol Corporation | Lubricating compositions |
US4097388A (en) * | 1976-10-12 | 1978-06-27 | The United States Of America As Represented By The Secretary Of The Air Force | Linear fluorinated polyether lubricant compositions containing perfluoroalkylether substituted phosphines |
AT381719B (de) * | 1979-10-15 | 1986-11-25 | Elf France | Schmiermittel oder schmiermittelzusaetze |
GB2065148A (en) * | 1979-12-14 | 1981-06-24 | Cooper & Co Ltd Edwin | Lubricating composition |
JPS59133297A (ja) * | 1983-01-20 | 1984-07-31 | Idemitsu Kosan Co Ltd | 高温用潤滑油組成物 |
FR2540104B1 (fr) * | 1983-02-01 | 1987-07-17 | Elf France | Synthese des ethers de polyols |
GB8422562D0 (en) * | 1984-09-06 | 1984-10-10 | Exxon Research Engineering Co | Hot forming lubricant compositions |
IT1188166B (it) * | 1985-04-24 | 1988-01-07 | Montefluos Spa | Stabilizzanti a struttura arilfosfinica per olii e grassi perfluoropolieterei |
EP0208541B1 (fr) * | 1985-07-08 | 1991-12-04 | Nippon Oil Co. Ltd. | Compositions lubrifiantes |
JPS6210193A (ja) * | 1985-07-08 | 1987-01-19 | Nippon Oil Co Ltd | トラクシヨンドライブ用流体組成物 |
-
1987
- 1987-04-10 DE DE19873712132 patent/DE3712132A1/de active Granted
-
1988
- 1988-04-08 CA CA000563060A patent/CA1339482C/fr not_active Expired - Fee Related
- 1988-04-11 AT AT88105727T patent/ATE111151T1/de not_active IP Right Cessation
- 1988-04-11 JP JP63503325A patent/JP2853135B2/ja not_active Expired - Lifetime
- 1988-04-11 WO PCT/EP1988/000303 patent/WO1988008023A1/fr unknown
- 1988-04-11 DE DE3851357T patent/DE3851357D1/de not_active Expired - Fee Related
- 1988-04-11 EP EP88105727A patent/EP0286141B1/fr not_active Expired - Lifetime
- 1988-04-11 ES ES88105727T patent/ES2063743T3/es not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
JP2853135B2 (ja) | 1999-02-03 |
ATE111151T1 (de) | 1994-09-15 |
WO1988008023A1 (fr) | 1988-10-20 |
DE3712132A1 (de) | 1988-10-20 |
CA1339482C (fr) | 1997-09-30 |
EP0286141A1 (fr) | 1988-10-12 |
DE3712132C2 (fr) | 1993-07-08 |
ES2063743T3 (es) | 1995-01-16 |
JPH01503789A (ja) | 1989-12-21 |
DE3851357D1 (de) | 1994-10-13 |
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