DE69916090D1 - Verfahren zur herstellung des alpha-tocopherol acetats - Google Patents

Verfahren zur herstellung des alpha-tocopherol acetats

Info

Publication number
DE69916090D1
DE69916090D1 DE69916090T DE69916090T DE69916090D1 DE 69916090 D1 DE69916090 D1 DE 69916090D1 DE 69916090 T DE69916090 T DE 69916090T DE 69916090 T DE69916090 T DE 69916090T DE 69916090 D1 DE69916090 D1 DE 69916090D1
Authority
DE
Germany
Prior art keywords
alpha
producing
tocopherol acetate
novel method
concerns
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69916090T
Other languages
English (en)
Other versions
DE69916090T2 (de
Inventor
Jildaz Dhainaut
Thierry Durand
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Adisseo France SAS
Original Assignee
Aventis Animal Nutrition SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aventis Animal Nutrition SA filed Critical Aventis Animal Nutrition SA
Publication of DE69916090D1 publication Critical patent/DE69916090D1/de
Application granted granted Critical
Publication of DE69916090T2 publication Critical patent/DE69916090T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • C07D311/70—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with two hydrocarbon radicals attached in position 2 and elements other than carbon and hydrogen in position 6
    • C07D311/72—3,4-Dihydro derivatives having in position 2 at least one methyl radical and in position 6 one oxygen atom, e.g. tocopherols

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Pyrane Compounds (AREA)
  • Steroid Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69916090T 1998-09-18 1999-09-15 Verfahren zur herstellung des alpha-tocopherol acetats Expired - Lifetime DE69916090T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR9811679 1998-09-18
FR9811679A FR2784104B1 (fr) 1998-09-18 1998-09-18 Procede de preparation de la vitamine e
PCT/FR1999/002196 WO2000017185A1 (fr) 1998-09-18 1999-09-15 Procede de preparation de la vitamine e

Publications (2)

Publication Number Publication Date
DE69916090D1 true DE69916090D1 (de) 2004-05-06
DE69916090T2 DE69916090T2 (de) 2005-02-17

Family

ID=9530589

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69916090T Expired - Lifetime DE69916090T2 (de) 1998-09-18 1999-09-15 Verfahren zur herstellung des alpha-tocopherol acetats

Country Status (9)

Country Link
US (2) US6518439B1 (de)
EP (1) EP1114041B1 (de)
JP (1) JP2002526489A (de)
CN (1) CN1141304C (de)
AT (1) ATE263161T1 (de)
AU (1) AU5628699A (de)
DE (1) DE69916090T2 (de)
FR (1) FR2784104B1 (de)
WO (1) WO2000017185A1 (de)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1186337C (zh) * 2000-10-23 2005-01-26 Sk株式会社 以高产率制备DL－α－生育酚的方法
ATE411307T1 (de) * 2003-12-05 2008-10-15 Dsm Ip Assets Bv Verfahren zur herstellung von alkenylierten hydroxylierten aromatischen verbindungen, von chromanverbindungen und deren acylierten derivaten
CN1332667C (zh) * 2004-05-26 2007-08-22 中国科学院生物物理研究所 一种抗帕金森症（pd）复合制剂
CN1332666C (zh) * 2004-05-26 2007-08-22 中国科学院生物物理研究所 一种抗老年痴呆症复合制剂
US8183396B2 (en) * 2004-08-19 2012-05-22 Dsm Ip Assets B.V. Process for the working-up of a vitamin E- and vitamin E-acetate- containing mixture or products stream
ATE502931T1 (de) 2004-08-19 2011-04-15 Dsm Ip Assets Bv Verfahren zur rektifikation von vitamin e acetat
CN102294240B (zh) * 2011-05-07 2013-02-13 浙江师范大学 一种用于TMBQ加氢生产TMHQ的Pd/C催化剂及制备方法
CN102295536B (zh) * 2011-07-14 2013-07-24 福建省福抗药业股份有限公司 一种高含量三甲基氢醌的制备方法
CN102336732A (zh) * 2011-07-14 2012-02-01 福建省福抗药业股份有限公司 一锅法制备维生素e乙酸酯的生产方法
JP2013063912A (ja) * 2011-08-31 2013-04-11 Eisai R & D Management Co Ltd α−トコフェロールおよび酢酸α−トコフェロールの製造方法
CN102351831A (zh) * 2011-09-09 2012-02-15 重庆大学 一种制备D,L-α-生育酚乙酸酯的方法
CN102276572B (zh) * 2011-09-14 2013-03-27 重庆大学 一种制备维生素e乙酸酯的方法
CN111253218A (zh) * 2019-12-30 2020-06-09 上虞新和成生物化工有限公司 一种2,3,5-三甲基氢醌的合成方法和装置

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3708505A (en) * 1971-02-25 1973-01-02 Diamond Shamrock Corp Process for preparation of d,l-alpha tocopherol
JPS5180859A (en) * 1975-01-11 1976-07-15 Teijin Ltd Arufua tokofuerooruruino seizoho
DE3203487A1 (de) * 1982-02-03 1983-08-11 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von tocopherylacetat oder tocopherylpropionat
FR2523494A1 (fr) * 1982-03-22 1983-09-23 Ferraz & Cie Lucien Machine a rectifier les collecteurs electriques et analogues
JPS59190987A (ja) * 1983-04-11 1984-10-29 Mitsui Toatsu Chem Inc ｄｌ−α−トコフエロ−ルの製造方法
JPS6054380A (ja) * 1983-09-05 1985-03-28 Sumitomo Chem Co Ltd α−トコフエロ−ルの製造法
JPH0772184B2 (ja) * 1986-03-28 1995-08-02 エーザイ株式会社 ｄ▲ｌ▼−α−トコフエロ−ルの製造方法
US4966914A (en) * 1988-12-15 1990-10-30 E. I. Du Pont De Nemours And Company Oculoselective beta-blockers as antiglaucoma agents
US5411969A (en) * 1993-04-16 1995-05-02 Bristol-Myers Squibb Company Antihyperlipidemic/antioxidant dihydroquinolines
US5663376A (en) * 1994-07-27 1997-09-02 Eisai Co., Ltd. Process for the preparation of α-tocopherol
US6020505A (en) * 1994-07-27 2000-02-01 Eisai Co., Ltd. Process for the preparation of α-tocopherol
JPH09188673A (ja) * 1994-07-27 1997-07-22 Eisai Co Ltd α−トコフェロールの製造方法
ES2191078T3 (es) * 1996-01-05 2003-09-01 Hoffmann La Roche Procedimiento de obtencion de d,1-alfa-tocoferol en presencia de un catalizador de acido perfluoroalquilensulfonico.
US5908939A (en) * 1996-11-11 1999-06-01 Roche Vitamins Inc. Method of making D,L-A-tocopherol
US6005122A (en) * 1996-12-23 1999-12-21 Basf Aktiengesellschaft Preparation of α-tocopherol or α-tocopheryl acetate by reacting trimethylhydroquinone and phytol or isophytol, with recycling of the zinc halide condensation catalyst
DE19757124A1 (de) * 1997-12-20 1999-06-24 Degussa Verfahren zur Herstellung von alpha-Tocopherolestern

Also Published As

Publication number Publication date
US20030153772A1 (en) 2003-08-14
US6518439B1 (en) 2003-02-11
DE69916090T2 (de) 2005-02-17
WO2000017185A1 (fr) 2000-03-30
EP1114041A1 (de) 2001-07-11
JP2002526489A (ja) 2002-08-20
US6790967B2 (en) 2004-09-14
CN1318064A (zh) 2001-10-17
CN1141304C (zh) 2004-03-10
AU5628699A (en) 2000-04-10
ATE263161T1 (de) 2004-04-15
FR2784104B1 (fr) 2002-12-27
FR2784104A1 (fr) 2000-04-07
EP1114041B1 (de) 2004-03-31

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Legal Events

Date Code Title Description
8327 Change in the person/name/address of the patent owner

Owner name: ADISSEO FRANCE S.A.S., ANTONY, FR

8364 No opposition during term of opposition