DE69911068T2 - Nichtwässriges schlichtesystem für glasfasern und spritzgussfähige polymere - Google Patents

Nichtwässriges schlichtesystem für glasfasern und spritzgussfähige polymere Download PDF

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Publication number
DE69911068T2
DE69911068T2 DE69911068T DE69911068T DE69911068T2 DE 69911068 T2 DE69911068 T2 DE 69911068T2 DE 69911068 T DE69911068 T DE 69911068T DE 69911068 T DE69911068 T DE 69911068T DE 69911068 T2 DE69911068 T2 DE 69911068T2
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DE
Germany
Prior art keywords
composition
glass
nylon
molecular weight
size
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69911068T
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German (de)
English (en)
Other versions
DE69911068D1 (de
Inventor
G. David MILLER
J. Leonard ADZIMA
J. David WAMER
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Owens Corning
Original Assignee
Owens Corning
Owens Corning Fiberglas Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Owens Corning, Owens Corning Fiberglas Corp filed Critical Owens Corning
Publication of DE69911068D1 publication Critical patent/DE69911068D1/de
Application granted granted Critical
Publication of DE69911068T2 publication Critical patent/DE69911068T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
    • C08J5/06—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials
    • C08J5/08—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials glass fibres
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
    • C03C25/10—Coating
    • C03C25/24—Coatings containing organic materials
    • C03C25/26—Macromolecular compounds or prepolymers
    • C03C25/32—Macromolecular compounds or prepolymers obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds
    • C03C25/323—Polyesters, e.g. alkyd resins
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
    • C03C25/10—Coating
    • C03C25/24—Coatings containing organic materials
    • C03C25/255—Oils, waxes, fats or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
    • C03C25/10—Coating
    • C03C25/465—Coatings containing composite materials
    • C03C25/47—Coatings containing composite materials containing particles, fibres or flakes, e.g. in a continuous phase
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/249921—Web or sheet containing structurally defined element or component
    • Y10T428/249924—Noninterengaged fiber-containing paper-free web or sheet which is not of specified porosity
    • Y10T428/24994—Fiber embedded in or on the surface of a polymeric matrix
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/249921—Web or sheet containing structurally defined element or component
    • Y10T428/249924—Noninterengaged fiber-containing paper-free web or sheet which is not of specified porosity
    • Y10T428/24994—Fiber embedded in or on the surface of a polymeric matrix
    • Y10T428/249942—Fibers are aligned substantially parallel
    • Y10T428/249946—Glass fiber
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/25—Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
    • Y10T428/252—Glass or ceramic [i.e., fired or glazed clay, cement, etc.] [porcelain, quartz, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2904—Staple length fiber
    • Y10T428/2907—Staple length fiber with coating or impregnation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913—Rod, strand, filament or fiber
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913—Rod, strand, filament or fiber
    • Y10T428/2933—Coated or with bond, impregnation or core
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913—Rod, strand, filament or fiber
    • Y10T428/2933—Coated or with bond, impregnation or core
    • Y10T428/2938—Coating on discrete and individual rods, strands or filaments
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913—Rod, strand, filament or fiber
    • Y10T428/2933—Coated or with bond, impregnation or core
    • Y10T428/2962—Silane, silicone or siloxane in coating
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913—Rod, strand, filament or fiber
    • Y10T428/2933—Coated or with bond, impregnation or core
    • Y10T428/2964—Artificial fiber or filament

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Composite Materials (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Manufacturing & Machinery (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Reinforced Plastic Materials (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Surface Treatment Of Glass Fibres Or Filaments (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)
DE69911068T 1998-12-23 1999-12-13 Nichtwässriges schlichtesystem für glasfasern und spritzgussfähige polymere Expired - Lifetime DE69911068T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US220221 1980-12-24
US09/220,221 US6399198B1 (en) 1998-12-23 1998-12-23 Nonaqueous sizing system for glass fibers and injection moldable polymers
PCT/US1999/029494 WO2000039042A1 (en) 1998-12-23 1999-12-13 Nonaqueous sizing system for glass fibers and injection moldable polymers

Publications (2)

Publication Number Publication Date
DE69911068D1 DE69911068D1 (de) 2003-10-09
DE69911068T2 true DE69911068T2 (de) 2004-07-15

Family

ID=22822610

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69911068T Expired - Lifetime DE69911068T2 (de) 1998-12-23 1999-12-13 Nichtwässriges schlichtesystem für glasfasern und spritzgussfähige polymere

Country Status (17)

Country Link
US (1) US6399198B1 (enExample)
EP (1) EP1152991B1 (enExample)
JP (1) JP4739528B2 (enExample)
KR (1) KR20010099938A (enExample)
CN (1) CN1333734A (enExample)
AT (1) ATE248784T1 (enExample)
AU (1) AU2177600A (enExample)
BR (1) BR9916487B1 (enExample)
CA (1) CA2354127C (enExample)
CZ (1) CZ299979B6 (enExample)
DE (1) DE69911068T2 (enExample)
ES (1) ES2207331T3 (enExample)
HU (1) HUP0202933A2 (enExample)
NO (1) NO332885B1 (enExample)
NZ (1) NZ512538A (enExample)
WO (1) WO2000039042A1 (enExample)
ZA (1) ZA200105123B (enExample)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6562257B1 (en) * 2000-04-25 2003-05-13 Owens Corning Fiberglas Technology, Inc. Loose-fill insulation with improved recoverability
US6607186B2 (en) * 2000-05-01 2003-08-19 Bret Voelkel Shock absorber
FR2826359B1 (fr) * 2001-06-21 2004-05-07 Saint Gobain Vetrotex Fils de verre ensimes, composition d'ensimage et composites comprenant lesdits fils
US6844374B2 (en) 2001-10-03 2005-01-18 Lord Corporation Enhanced scratch resistant coatings using inorganic fillers
US7414780B2 (en) * 2003-06-30 2008-08-19 Imra America, Inc. All-fiber chirped pulse amplification systems
FR2864073B1 (fr) * 2003-12-17 2006-03-31 Saint Gobain Vetrotex Fils de verre ensimes a impregnation rapide pour le renforcement de matieres polymeres
US20060177657A1 (en) * 2005-02-08 2006-08-10 Keith Weller Sizing compositions for fibers utilizing low VOC silanes
EP2219839B1 (en) * 2007-12-21 2011-10-26 Saudi Basic Industries Corporation Process for producing long glass fibre-reinforced thermoplastic compositions
US20140228486A1 (en) * 2011-08-01 2014-08-14 Ocv Intellectual Capital, Llc Sizing compositions and methods of their use
US20130143025A1 (en) * 2011-12-06 2013-06-06 Makoto Kibayashi Thermoplastic resin impregnated tape
US9718956B2 (en) 2014-01-14 2017-08-01 Sabic Global Technologies B.V. Interior aircraft components and methods of manufacture
US9365720B2 (en) * 2014-01-14 2016-06-14 Sabic Global Technologies B.V. Interior train components having low smoke and low heat release, and methods of their manufacture
CN104045244B (zh) * 2014-05-29 2017-02-01 巨石集团有限公司 连续纤维增强聚烯烃用无碱直接纱浸润剂
TWI719982B (zh) 2015-05-15 2021-03-01 美商西凱渥資訊處理科技公司 半導體裝置中之空腔形成
CN105568694B (zh) * 2016-03-09 2017-10-27 广东工业大学 一种热塑性上浆剂及其制备方法与应用
KR101999900B1 (ko) * 2017-10-24 2019-07-12 주식회사 케이씨씨 사이징 조성물 및 이를 이용한 유리섬유

Family Cites Families (39)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2272588A (en) 1937-07-31 1942-02-10 Owens Corning Fiberglass Corp Coating for fibrous glass strands
US3066383A (en) 1957-02-14 1962-12-04 Owens Corning Fiberglass Corp Finish for staple glass fibers and yarns manufactured thereof
US3644245A (en) 1969-06-25 1972-02-22 Nat Starch Chem Corp Hot melt adhesives containing silane compounds
US3676287A (en) * 1970-09-08 1972-07-11 Owens Corning Fiberglass Corp Glass fiber-reinforced elastomers
US3837892A (en) 1972-01-28 1974-09-24 Owens Corning Fiberglass Corp Glass fiber reinforced elastomers
US3997306A (en) 1975-03-31 1976-12-14 Ppg Industries, Inc. Glass fiber sizing composition for the reinforcement of resin matrices and method of using same
US4136069A (en) 1975-07-18 1979-01-23 Eastman Kodak Company Hot melt sizing compositions and fibrous articles sized therewith
US4173680A (en) 1975-07-18 1979-11-06 Eastman Kodak Company Hot melt sizing compositions and fibrous articles sized therewith
US4088468A (en) 1976-12-16 1978-05-09 Owens-Corning Fiberglas Corporation Method and apparatus for applying size to glass strands
US4500600A (en) 1977-04-25 1985-02-19 Owens-Corning Fiberglas Corporation Size composition for glass fibers
JPS54106626A (en) 1978-02-01 1979-08-21 Asahi Glass Co Ltd Sizing agent
JPS54120737A (en) 1978-03-13 1979-09-19 Kanebo Ltd Manufacture of alkali-resistant glass fibers withstanding high-temperatur cure
US4298653A (en) 1978-12-15 1981-11-03 Ppg Industries, Inc. Method for producing an improved bundle of a plurality of fiber glass strands
US4248936A (en) 1979-05-29 1981-02-03 Owens-Corning Fiberglas Corporation Asphalt-coated glass fibers
JPS5678455A (en) 1979-09-04 1981-06-27 Owens Corning Fiberglass Corp Glass fiber sizing agent composition
US4530860A (en) 1980-06-25 1985-07-23 Owens-Corning Fiberglas Corporation Migration-free size for glass fibers
AU541503B2 (en) 1981-11-27 1985-01-10 Nitto Boseki Co. Ltd. Producing compacted chopped strands
US4524040A (en) 1983-08-04 1985-06-18 The Firestone Tire & Rubber Company Process for making coated glass fiber reinforced composites
US4567102A (en) 1984-05-24 1986-01-28 Owens-Corning Fiberglas Corporation Hot melt size
US4581392A (en) 1984-05-24 1986-04-08 Owens-Corning Fiberglas Corporation Hot melt glass fiber coating
US4537917A (en) 1984-10-01 1985-08-27 The Firestone Tire & Rubber Company Composites and size coated glass fibers used therein
US4604325A (en) 1985-05-10 1986-08-05 Owens-Corning Fiberglas Corporation Non-aqueous coating for glass fibers and glass fibers coated therewith
US4609591A (en) 1985-05-10 1986-09-02 Owens-Corning Fiberglas Corporation Non-aqueous coating for glass fibers and glass fibers coated therewith
US5071914A (en) 1986-01-29 1991-12-10 H. B. Fuller Company Thermoplastic hot melt adhesive containing epoxy adduct
US4774135A (en) 1986-05-16 1988-09-27 Bgf Industries, Inc. Process for coating yarn with hot melt thermoplastic
FR2607801B1 (fr) 1986-12-04 1989-03-03 Saint Gobain Vetrotex Procede et dispositif de fabrication d'un fil de verre simple obtenu directement sous filiere
US5026410A (en) * 1987-03-12 1991-06-25 Owens-Corning Fiberglas Corporation Process for impregnating filament strands
US5387468A (en) 1987-03-12 1995-02-07 Owens-Corning Fiberglas Technology Inc. Size composition for impregnating filament strands
US5024890A (en) * 1987-03-12 1991-06-18 Owens-Corning Fiberglass Corporation Size composition for impregnating filament strands and glass fibers coated therein
FR2638467B1 (enExample) 1988-10-28 1991-11-08 Saint Gobain Vetrotex
US5071675A (en) 1989-03-20 1991-12-10 Weyerhaeuser Company Method of applying liquid sizing of alkyl ketene dimer in ethanol to cellulose fibers entrained in a gas stream
US5156913A (en) 1989-12-11 1992-10-20 Hoechst Celanese Corp. Glass reinforced acetal polymer products
FR2691112B1 (fr) 1992-05-14 1995-07-21 Saint Gobain Vitrage Int Procede d'encapsulation d'un vitrage et vitrage ainsi obtenu.
FR2691171B1 (fr) 1992-05-15 1994-12-23 Vetrotex France Sa Procédé de fabrication d'un fil continu par étirage mécanique et produits en résultant.
US5405895A (en) * 1992-07-30 1995-04-11 Industrial Technology Research Institute Surface treating compositions and methods of preparation and use in treating long glass fibers
FR2702778B1 (fr) 1993-03-18 1995-05-05 Vetrotex France Sa Procédé et dispositif de formation d'un fil composite.
JPH09324136A (ja) 1996-06-07 1997-12-16 Japan Synthetic Rubber Co Ltd 光ファイバー被覆用液状硬化性樹脂組成物
US6020064A (en) 1997-05-13 2000-02-01 Owens Corning Fiberglas Technology, Inc. Nonaqueous sizing for glass and carbon fibers
US5998029A (en) 1997-06-30 1999-12-07 Owens Corning Fiberglas Technology, Inc. Nonaqueous sizing system for glass fibers and injection moldable polymers

Also Published As

Publication number Publication date
DE69911068D1 (de) 2003-10-09
BR9916487A (pt) 2001-12-11
ES2207331T3 (es) 2004-05-16
EP1152991A1 (en) 2001-11-14
CN1333734A (zh) 2002-01-30
CA2354127A1 (en) 2000-07-06
ZA200105123B (en) 2002-06-21
CZ299979B6 (cs) 2009-01-14
NO20013137L (no) 2001-06-22
HUP0202933A2 (en) 2002-12-28
CA2354127C (en) 2008-08-12
US6399198B1 (en) 2002-06-04
ATE248784T1 (de) 2003-09-15
BR9916487B1 (pt) 2009-08-11
EP1152991B1 (en) 2003-09-03
US20020054985A1 (en) 2002-05-09
NO20013137D0 (no) 2001-06-22
NZ512538A (en) 2003-03-28
JP2002533296A (ja) 2002-10-08
WO2000039042A1 (en) 2000-07-06
NO332885B1 (no) 2013-01-28
KR20010099938A (ko) 2001-11-09
CZ20012347A3 (cs) 2004-03-17
AU2177600A (en) 2000-07-31
JP4739528B2 (ja) 2011-08-03

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