DE69800995D1 - Verfahren und vorrichtung zur direkten umsetzung von uranhexafluorid in uranoxid - Google Patents

Verfahren und vorrichtung zur direkten umsetzung von uranhexafluorid in uranoxid

Info

Publication number
DE69800995D1
DE69800995D1 DE69800995T DE69800995T DE69800995D1 DE 69800995 D1 DE69800995 D1 DE 69800995D1 DE 69800995 T DE69800995 T DE 69800995T DE 69800995 T DE69800995 T DE 69800995T DE 69800995 D1 DE69800995 D1 DE 69800995D1
Authority
DE
Germany
Prior art keywords
uranoxide
uranhexafluoride
conversing
directly
directly conversing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69800995T
Other languages
English (en)
Other versions
DE69800995T2 (de
Inventor
Andre Feugier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Areva NP SAS
Original Assignee
Franco Belge de Fabrication de Combustible FBFC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Franco Belge de Fabrication de Combustible FBFC filed Critical Franco Belge de Fabrication de Combustible FBFC
Application granted granted Critical
Publication of DE69800995D1 publication Critical patent/DE69800995D1/de
Publication of DE69800995T2 publication Critical patent/DE69800995T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G43/00Compounds of uranium
    • C01G43/01Oxides; Hydroxides
    • C01G43/025Uranium dioxide
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/0084Filters or filtering processes specially modified for separating dispersed particles from gases or vapours provided with safety means
    • B01D46/0091Including arrangements for environmental or personal protection
    • B01D46/0094Including arrangements for environmental or personal protection against radiation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/0084Filters or filtering processes specially modified for separating dispersed particles from gases or vapours provided with safety means
    • B01D46/0095Means acting upon failure of the filtering system, e.g. in case of damage of the filter elements; Failsafes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/24Particle separators, e.g. dust precipitators, using rigid hollow filter bodies
    • B01D46/2403Particle separators, e.g. dust precipitators, using rigid hollow filter bodies characterised by the physical shape or structure of the filtering element
    • B01D46/2407Filter candles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/56Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with multiple filtering elements, characterised by their mutual disposition
    • B01D46/62Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with multiple filtering elements, characterised by their mutual disposition connected in series
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/66Regeneration of the filtering material or filter elements inside the filter
    • B01D46/70Regeneration of the filtering material or filter elements inside the filter by acting counter-currently on the filtering surface, e.g. by flushing on the non-cake side of the filter
    • B01D46/71Regeneration of the filtering material or filter elements inside the filter by acting counter-currently on the filtering surface, e.g. by flushing on the non-cake side of the filter with pressurised gas, e.g. pulsed air
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/28Moving reactors, e.g. rotary drums
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005Separating solid material from the gas/liquid stream
    • B01J8/006Separating solid material from the gas/liquid stream by filtration
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G43/00Compounds of uranium
    • C01G43/01Oxides; Hydroxides
    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21CNUCLEAR REACTORS
    • G21C19/00Arrangements for treating, for handling, or for facilitating the handling of, fuel or other materials which are used within the reactor, e.g. within its pressure vessel
    • G21C19/42Reprocessing of irradiated fuel
    • G21C19/44Reprocessing of irradiated fuel of irradiated solid fuel
    • G21C19/48Non-aqueous processes
    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21CNUCLEAR REACTORS
    • G21C21/00Apparatus or processes specially adapted to the manufacture of reactors or parts thereof
    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21CNUCLEAR REACTORS
    • G21C3/00Reactor fuel elements and their assemblies; Selection of substances for use as reactor fuel elements
    • G21C3/42Selection of substances for use as reactor fuel
    • G21C3/58Solid reactor fuel Pellets made of fissile material
    • G21C3/62Ceramic fuel
    • G21C3/623Oxide fuels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058Temperature measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00065Pressure measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00132Controlling the temperature using electric heating or cooling elements
    • B01J2219/00135Electric resistance heaters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/0015Controlling the temperature by thermal insulation means
    • B01J2219/00155Controlling the temperature by thermal insulation means using insulating materials or refractories
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/187Details relating to the spatial orientation of the reactor inclined at an angle to the horizontal or to the vertical plane
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G43/00Compounds of uranium
    • C01G43/04Halides of uranium
    • C01G43/06Fluorides
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E30/00Energy generation of nuclear origin
    • Y02E30/30Nuclear fission reactors
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • General Engineering & Computer Science (AREA)
  • Plasma & Fusion (AREA)
  • High Energy & Nuclear Physics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Geometry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Ceramic Engineering (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
DE69800995T 1997-11-28 1998-11-25 Verfahren und vorrichtung zur direkten umsetzung von uranhexafluorid in uranoxid Expired - Lifetime DE69800995T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9715016A FR2771725B1 (fr) 1997-11-28 1997-11-28 Procede et dispositif de conversion directe d'hexafluorure d'uranium en oxyde d'uranium
PCT/FR1998/002522 WO1999028236A1 (fr) 1997-11-28 1998-11-25 Procede et dispositif de conversion directe d'hexafluorure d'uranium en oxyde d'uranium

Publications (2)

Publication Number Publication Date
DE69800995D1 true DE69800995D1 (de) 2001-08-02
DE69800995T2 DE69800995T2 (de) 2002-01-17

Family

ID=9513946

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69800995T Expired - Lifetime DE69800995T2 (de) 1997-11-28 1998-11-25 Verfahren und vorrichtung zur direkten umsetzung von uranhexafluorid in uranoxid

Country Status (14)

Country Link
US (1) US6136285A (de)
EP (1) EP0960070B1 (de)
JP (1) JP4206448B2 (de)
KR (1) KR100567454B1 (de)
CN (1) CN1143824C (de)
AU (1) AU1340099A (de)
BR (1) BR9807115A (de)
DE (1) DE69800995T2 (de)
ES (1) ES2159193T3 (de)
FR (1) FR2771725B1 (de)
RU (1) RU2162058C1 (de)
TW (1) TW362217B (de)
WO (1) WO1999028236A1 (de)
ZA (1) ZA9810827B (de)

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FR2805044B1 (fr) * 2000-02-11 2002-05-17 Franco Belge Combustibles Procede et dispositif de determination de l'evolution d'une reaction chimique dans un four et de reglage de la reaction
FR2818159B1 (fr) 2000-12-15 2003-10-03 Franco Belge Combustibles Procede et dispositif de decolmatage d'un filtre d'une installation de production d'oxyde d'uranium a partir d'hexafluorure d'uranium
DK1214970T3 (da) * 2000-12-15 2002-12-30 Cleanaway Deutschland Ag & Co Indretning til oprensning og/eller dekontaminering af polyester
US7824640B1 (en) * 2006-07-25 2010-11-02 Westinghouse Electric Co. Llc Two step dry UO2 production process utilizing a positive sealing valve means between steps
EP2277831B1 (de) 2009-07-20 2012-05-23 Westinghouse Electric Company LLC Zweistufiges Verfahren zur Herstellung von trockenem UO2 mittels positivem Dichtungsventil zwischen den Schritten
EP2459486B1 (de) * 2009-07-29 2013-08-28 The South African Nuclear Energy Corporation Limited Behandlung von material auf zirkonoxidbasis mit ammonium-bifluorid
US8329109B2 (en) * 2009-11-12 2012-12-11 Areva Np Segmented reactors for capacity and enrichment changes in conversion of uranium hexafluoride to uranium dioxide
CN102476080A (zh) * 2010-11-29 2012-05-30 中核建中核燃料元件有限公司 一种转化还原炉喷嘴及其加工用刀具
FR2972811B1 (fr) 2011-03-14 2014-02-07 Soc Franco Belge De Fabrication De Combustibles Fbfc Dispositif et procede de spectrometrie photonique, procede de calibrage du dispositif et utilisation du dispositif
RU2498941C2 (ru) * 2012-02-28 2013-11-20 Открытое акционерное общество "Машиностроительный завод" Реакционная камера для получения порошка диоксида урана методом пирогидролиза из гексафторида урана (варианты)
RU2548443C2 (ru) * 2013-06-05 2015-04-20 Открытое акционерное общество "Машиностроительный завод" Аппарат для гидролиза гексафторида урана
RU2567633C1 (ru) * 2014-09-24 2015-11-10 Акционерное общество "Высокотехнологический научно-исследовательский институт неорганических материалов имени академика А.А. Бочвара" ( АО "ВНИИНМ") Способ получения порошка диоксида урана из гексафторида урана и установка для его осуществления
CN106924989B (zh) * 2015-12-29 2019-05-17 中核四○四有限公司 天然六氟化铀气相转移方法
KR101856467B1 (ko) * 2017-06-01 2018-05-11 한전원자력연료 주식회사 기상반응을 통한 6불화우라늄 실린더 내부 잔여물 처리방법 및 처리장치
US10457558B2 (en) 2017-06-22 2019-10-29 Westinghouse Electric Company Llc Method to produce uranium silicides
CN109954475A (zh) * 2017-12-25 2019-07-02 中核建中核燃料元件有限公司 一种干法制备uo2粉末工艺过程中的喷嘴
KR102065771B1 (ko) * 2018-06-26 2020-01-13 한전원자력연료 주식회사 핵연료 제조공정에서의 uf6 가스 누출 감지 시스템
JP7142157B2 (ja) * 2018-10-09 2022-09-26 フラマトム 核燃料粉末の生産設備
EA202190742A1 (ru) * 2018-10-09 2021-08-13 Фраматом Способ и установка конверсии гексафторида урана в диоксид урана
WO2020074794A1 (fr) 2018-10-09 2020-04-16 Framatome Installation et procédé de conversion d'hexafluorure d'uranium en dioxyde d'uranium
WO2020074791A1 (fr) * 2018-10-09 2020-04-16 Framatome Procédé et installation de conversion d'hexafluorure d'uranium en dioxyde d'uranium
CN109399745A (zh) * 2018-12-17 2019-03-01 广东上典环境保护工程有限公司 一种自除垢蒸发器及其运行方法
KR20220062220A (ko) 2019-09-05 2022-05-16 퍼블리크노에 악트시오네르노에 옵스체스트보 "노보시비르스키 자보드 힘콘트센트라토브" (파오 엔제트에이치케이) 육불화우라늄의 열가수분해로 이산화우라늄 분말을 제조하는 반응 챔버
FR3103118B1 (fr) 2019-11-15 2022-03-25 Framatome Sa Réacteur d’hydrolyse d’hexafluorure d’uranium
CN112811470A (zh) * 2020-11-20 2021-05-18 中核北方核燃料元件有限公司 一种六氟化铀干法制备高纯氟化铀酰粉末的方法
CN113023782B (zh) * 2021-03-10 2023-05-05 哈尔滨工程大学 一种重铀酸钠(Na2U2O7)直接制备UO2的方法

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Also Published As

Publication number Publication date
EP0960070B1 (de) 2001-06-27
KR20000070530A (ko) 2000-11-25
US6136285A (en) 2000-10-24
JP2001511109A (ja) 2001-08-07
FR2771725B1 (fr) 2000-02-04
CN1244178A (zh) 2000-02-09
TW362217B (en) 1999-06-21
DE69800995T2 (de) 2002-01-17
EP0960070A1 (de) 1999-12-01
BR9807115A (pt) 2000-04-25
AU1340099A (en) 1999-06-16
RU2162058C1 (ru) 2001-01-20
WO1999028236A1 (fr) 1999-06-10
ES2159193T3 (es) 2001-09-16
KR100567454B1 (ko) 2006-04-04
CN1143824C (zh) 2004-03-31
ZA9810827B (en) 1999-05-28
JP4206448B2 (ja) 2009-01-14
FR2771725A1 (fr) 1999-06-04

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