DE69710901T2 - Verfahren und vorrichtung zur rückextraktion von metallchelaten - Google Patents

Verfahren und vorrichtung zur rückextraktion von metallchelaten

Info

Publication number
DE69710901T2
DE69710901T2 DE69710901T DE69710901T DE69710901T2 DE 69710901 T2 DE69710901 T2 DE 69710901T2 DE 69710901 T DE69710901 T DE 69710901T DE 69710901 T DE69710901 T DE 69710901T DE 69710901 T2 DE69710901 T2 DE 69710901T2
Authority
DE
Germany
Prior art keywords
extracing
metal chelates
chelates
metal
extracing metal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69710901T
Other languages
English (en)
Other versions
DE69710901D1 (de
Inventor
Chien M Wai
Neil G Smart
Lin Yuehe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Idaho Research Foundation Inc
Original Assignee
Idaho Research Foundation Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Idaho Research Foundation Inc filed Critical Idaho Research Foundation Inc
Application granted granted Critical
Publication of DE69710901D1 publication Critical patent/DE69710901D1/de
Publication of DE69710901T2 publication Critical patent/DE69710901T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B59/00—Obtaining rare earth metals
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/16—Extraction of metal compounds from ores or concentrates by wet processes by leaching in organic solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0203—Solvent extraction of solids with a supercritical fluid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0403—Solvent extraction of solutions which are liquid with a supercritical fluid
    • B01D11/0407—Solvent extraction of solutions which are liquid with a supercritical fluid the supercritical fluid acting as solvent for the solute
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/02—Apparatus therefor
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/302—Ethers or epoxides
    • C22B3/304—Crown ethers
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
    • C22B60/02—Obtaining thorium, uranium, or other actinides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S210/00—Liquid purification or separation
    • Y10S210/902—Materials removed
    • Y10S210/911—Cumulative poison
    • Y10S210/912—Heavy metal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Environmental & Geological Engineering (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Manufacture And Refinement Of Metals (AREA)
DE69710901T 1996-07-26 1997-07-18 Verfahren und vorrichtung zur rückextraktion von metallchelaten Expired - Fee Related DE69710901T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/692,894 US5792357A (en) 1996-07-26 1996-07-26 Method and apparatus for back-extracting metal chelates
PCT/US1997/013777 WO1998004754A1 (en) 1996-07-26 1997-07-18 Method and apparatus for back-extracting metal chelates

Publications (2)

Publication Number Publication Date
DE69710901D1 DE69710901D1 (de) 2002-04-11
DE69710901T2 true DE69710901T2 (de) 2002-11-28

Family

ID=24782487

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69710901T Expired - Fee Related DE69710901T2 (de) 1996-07-26 1997-07-18 Verfahren und vorrichtung zur rückextraktion von metallchelaten

Country Status (10)

Country Link
US (1) US5792357A (de)
EP (1) EP0914482B1 (de)
JP (1) JP2000515932A (de)
KR (1) KR20000029570A (de)
CN (1) CN1061383C (de)
AU (1) AU4052497A (de)
CA (1) CA2260831A1 (de)
DE (1) DE69710901T2 (de)
ES (1) ES2173472T3 (de)
WO (1) WO1998004754A1 (de)

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US5965025A (en) * 1991-06-12 1999-10-12 Idaho Research Foundation, Inc. Fluid extraction
ES2202591T3 (es) * 1997-08-20 2004-04-01 Idaho Research Foundation, Inc. Metodo para disociar metales o para disociar compuestos metalicos.
US6187911B1 (en) * 1998-05-08 2001-02-13 Idaho Research Foundation, Inc. Method for separating metal chelates from other materials based on solubilities in supercritical fluids
RU2153203C2 (ru) * 1998-05-22 2000-07-20 Научно-производственное объединение "Радиевый институт им.В.Г.Хлопина" Способ удаления неорганических, в том числе радиоактивных, загрязнений с поверхностей твердых тел
US6180069B1 (en) * 1999-02-18 2001-01-30 Leco Corporation Cleaning system and method for cleaning a flow restrictor in a supercritical fluid extraction system
US6322702B1 (en) * 1999-09-23 2001-11-27 U.T. Battlle, Llc Solvent and process for recovery of hydroxide from aqueous mixtures
US6416682B1 (en) 1999-11-04 2002-07-09 Ceramic Oxides International B.V. Method of producing minerals under near-critical, critical and supercritical conditions
US7128840B2 (en) 2002-03-26 2006-10-31 Idaho Research Foundation, Inc. Ultrasound enhanced process for extracting metal species in supercritical fluids
WO2005069955A2 (en) * 2004-01-21 2005-08-04 Idaho Research Foundation, Inc. Supercritical fluids in the formation and modification of nanostructures and nanocomposites
US20080115627A1 (en) * 2004-08-20 2008-05-22 Wang Joanna S Metal Extraction In Liquid Or Supercritical-Fluid Solvents
WO2007084116A2 (en) 2005-01-18 2007-07-26 Idaho Research Foundation, Inc. Method and system for recovering metal from metal-containing materials
JP4452837B2 (ja) * 2005-09-26 2010-04-21 国立大学法人静岡大学 抽出分離方法
US8669344B2 (en) 2006-04-07 2014-03-11 Lg Chem, Ltd. Method of deashing from polymer solutions
US7244403B1 (en) * 2006-04-19 2007-07-17 Iso-Tex Diagnostics, Inc. Purification of Lutetium 177
GB0804055D0 (en) * 2008-03-04 2008-04-09 Univ Nottingham Trent Cleaning method
JP5889060B2 (ja) * 2011-04-04 2016-03-22 アークレイ株式会社 金属の回収方法
US9597775B2 (en) 2013-10-30 2017-03-21 Us Synthetic Corporation Methods of at least partially removing at least one interstitial constituent from a polycrystalline diamond body using a removing agent including a supercritical fluid component
FR3025115B1 (fr) 2014-09-03 2018-12-07 Commissariat A L'energie Atomique Et Aux Energies Alternatives Procede d'extraction selectif de platinoides, a partir d'un support les contenant, avec un milieu d'extraction comprenant un fluide supercritique et un ligand organique.
US10141079B2 (en) 2014-12-29 2018-11-27 Terrapower, Llc Targetry coupled separations
US10867710B2 (en) 2015-09-30 2020-12-15 Terrapower, Llc Molten fuel nuclear reactor with neutron reflecting coolant
KR101699926B1 (ko) * 2015-09-30 2017-01-25 한국지질자원연구원 왕수용액으로부터 질산 및 금의 회수 방법
US10665356B2 (en) 2015-09-30 2020-05-26 Terrapower, Llc Molten fuel nuclear reactor with neutron reflecting coolant
EP3357068B1 (de) 2015-09-30 2020-06-17 TerraPower LLC Schneller kernreaktor mit neutronenreflektoranordnung für dynamische spektralverschiebung
CN106653134B (zh) * 2017-01-22 2018-04-27 中国核动力研究设计院 无载体磷32的制备方法
CN114651311A (zh) 2019-12-23 2022-06-21 泰拉能源公司 熔融燃料反应堆和用于熔融燃料反应堆的孔环板
US11937438B2 (en) 2020-04-17 2024-03-19 Peking University Shenzhen Graduate School Organic field-effect transistor and fabrication method therefor
CN111477743B (zh) * 2020-04-17 2022-11-22 北京大学深圳研究生院 一种有机场效应晶体管及其制备方法
WO2022039893A1 (en) 2020-08-17 2022-02-24 Terrapower, Llc Designs for fast spectrum molten chloride test reactors
CN113889336B (zh) * 2021-12-08 2022-03-11 天津三环乐喜新材料有限公司 一种高性能钕铁硼永磁体的制备方法

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US4206132A (en) * 1971-09-24 1980-06-03 The United States Of America As Represented By The Secretary Of The Air Force Lanthanide chelate of a fluorinated ligand
US4015980A (en) * 1975-08-04 1977-04-05 General Mills Chemicals, Inc. Use of fluorinated β-diketones in the solvent extraction of zinc
US4051223A (en) * 1975-11-10 1977-09-27 General Mills Chemicals, Inc. Process for the recovery of magnesium
US4069273A (en) * 1977-01-24 1978-01-17 Chevron Research Company Dimerization of linear alpha-olefins
DE2855191C2 (de) * 1978-12-21 1982-12-23 Fried. Krupp Gmbh, 4300 Essen Trennung von Isotopen
US4275039A (en) * 1980-01-17 1981-06-23 Interox Chemicals Limited Separation of tungsten and molybdenum by solvent extraction
JPS5920406A (ja) * 1982-07-26 1984-02-02 Nippon Sanso Kk 超微粉末金属の製造方法
US4529503A (en) * 1982-08-05 1985-07-16 Phillips Petroleum Company Demetallization of hydrocarbon containing feed streams with phosphorous compounds
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US4528100A (en) * 1983-10-31 1985-07-09 General Electric Company Process for producing high yield of gas turbine fuel from residual oil
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US5169968A (en) * 1985-09-10 1992-12-08 Vitamins, Inc. Mass separation of liquid or soluble components from solid materials utilizing supercritical fluids
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DE3704307A1 (de) * 1987-02-12 1988-08-25 Dow Chemical Gmbh Komplexbildendes harz des geltyps und seine verwendung zur verringerung der konzentration mehrwertiger erdalkali- und/oder schwermetallionen in loesungen
FR2614725B1 (fr) * 1987-04-28 1992-10-30 Rhone Poulenc Chimie Procede d'elimination de la radioactivite d'effluents par extraction liquide-liquide
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JP2584498B2 (ja) * 1988-09-05 1997-02-26 工業技術院長 新規なクラウンエーテル化合物及び分離剤
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US5730874A (en) * 1991-06-12 1998-03-24 Idaho Research Foundation, Inc. Extraction of metals using supercritical fluid and chelate forming legand
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US5641887A (en) * 1994-04-01 1997-06-24 University Of Pittsburgh Extraction of metals in carbon dioxide and chelating agents therefor
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Also Published As

Publication number Publication date
AU4052497A (en) 1998-02-20
CA2260831A1 (en) 1998-02-05
WO1998004754A1 (en) 1998-02-05
EP0914482A1 (de) 1999-05-12
DE69710901D1 (de) 2002-04-11
US5792357A (en) 1998-08-11
ES2173472T3 (es) 2002-10-16
JP2000515932A (ja) 2000-11-28
KR20000029570A (ko) 2000-05-25
EP0914482B1 (de) 2002-03-06
CN1061383C (zh) 2001-01-31
CN1226286A (zh) 1999-08-18

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Legal Events

Date Code Title Description
8339 Ceased/non-payment of the annual fee