DE69230569D1 - Verfahren zur Herstellung von Terephthalsäure - Google Patents

Verfahren zur Herstellung von Terephthalsäure

Info

Publication number
DE69230569D1
DE69230569D1 DE69230569T DE69230569T DE69230569D1 DE 69230569 D1 DE69230569 D1 DE 69230569D1 DE 69230569 T DE69230569 T DE 69230569T DE 69230569 T DE69230569 T DE 69230569T DE 69230569 D1 DE69230569 D1 DE 69230569D1
Authority
DE
Germany
Prior art keywords
preparation
terephthalic acid
terephthalic
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69230569T
Other languages
English (en)
Other versions
DE69230569T2 (de
Inventor
Eric Hindmarsh
John Arthur Turner
Alan Macpherson Ure
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
La Seda de Barcelona SA
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of DE69230569D1 publication Critical patent/DE69230569D1/de
Application granted granted Critical
Publication of DE69230569T2 publication Critical patent/DE69230569T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C63/00Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
    • C07C63/14Monocyclic dicarboxylic acids
    • C07C63/15Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
    • C07C63/261,4 - Benzenedicarboxylic acid
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/487Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69230569T 1991-03-07 1992-02-02 Verfahren zur Herstellung von Terephthalsäure Expired - Lifetime DE69230569T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB919104776A GB9104776D0 (en) 1991-03-07 1991-03-07 Process for the production of terephthalic acid
IDP97064092A ID19108A (id) 1991-03-07 1992-06-08 Proses produksi asam tereftalat (pecahan dari p-002451)

Publications (2)

Publication Number Publication Date
DE69230569D1 true DE69230569D1 (de) 2000-02-17
DE69230569T2 DE69230569T2 (de) 2000-07-27

Family

ID=32599058

Family Applications (2)

Application Number Title Priority Date Filing Date
DE69230569T Expired - Lifetime DE69230569T2 (de) 1991-03-07 1992-02-02 Verfahren zur Herstellung von Terephthalsäure
DE69214859T Expired - Lifetime DE69214859T2 (de) 1991-03-07 1992-02-20 Verfahren zur Herstellung von Terephthalsäure

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE69214859T Expired - Lifetime DE69214859T2 (de) 1991-03-07 1992-02-20 Verfahren zur Herstellung von Terephthalsäure

Country Status (15)

Country Link
US (4) US5527957A (de)
EP (3) EP0502628B1 (de)
JP (1) JPH0565246A (de)
KR (1) KR100225371B1 (de)
CN (2) CN1038409C (de)
CA (1) CA2062063C (de)
DE (2) DE69230569T2 (de)
EG (1) EG19876A (de)
ES (2) ES2142006T3 (de)
GB (2) GB9104776D0 (de)
ID (1) ID19108A (de)
MX (1) MX9200997A (de)
RU (1) RU2106337C1 (de)
SG (1) SG66231A1 (de)
ZA (1) ZA921380B (de)

Families Citing this family (103)

* Cited by examiner, † Cited by third party
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GB9310070D0 (en) * 1992-05-29 1993-06-30 Ici Plc Process for the production of purified terephthalic acid
GB9400570D0 (en) * 1994-01-13 1994-03-09 Ici Plc Handling of materials at elevated pressure
TW299318B (de) * 1994-11-15 1997-03-01 Mitsubishi Chem Corp
CN1163693C (zh) * 1995-06-05 2004-08-25 纳幕尔杜邦公司 废气处理方法
US5961942A (en) * 1995-06-05 1999-10-05 E. I. Du Pont De Nemours And Company Effluent gas treatment
US5929274A (en) 1995-06-07 1999-07-27 Hfm International, Inc. Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid
US5767311A (en) 1995-06-07 1998-06-16 Glitsch International, Inc. Method and apparatus for preparing purified terephtalic acid
US6054610A (en) 1995-06-07 2000-04-25 Hfm International, Inc. Method and apparatus for preparing purified terephthalic acid and isophthalic acid from mixed xylenes
US6013835A (en) * 1995-06-07 2000-01-11 Hfm International, Inc. Method and apparatus for preparing purified terephthalic acid
TW442461B (en) * 1996-02-22 2001-06-23 Du Pont Process for the production of an aromatic carboxylic acid
TR199801626T2 (xx) * 1996-02-22 1999-08-23 E.I. Du Pont De Nemours And Company Aromatik polikarboksilik asitlerin �retilmesi.
GB9705349D0 (en) 1997-03-14 1997-04-30 Ici Plc Treatment of effluent streams
AU729150B2 (en) * 1997-12-12 2001-01-25 Mitsubishi Heavy Industries, Ltd. Rolling system and rolling method
JP2002508343A (ja) * 1997-12-15 2002-03-19 シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー 芳香族カルボン酸の製造方法
TW483886B (en) * 1998-08-11 2002-04-21 Du Pont Method for recovering methyl acetate and residual acetic acid in the production of pure terephtalic acid
IT1311976B1 (it) * 1999-03-25 2002-03-22 Franco Codignola Procedimento per la produzione di acidi aromatici.
IT1319169B1 (it) 2000-07-14 2003-09-26 Eurotecnica Dev & Licensing Sr Procedimento per la purificazione di acidi carbossilici aromatici.
US6765113B2 (en) 2000-07-19 2004-07-20 E.I. Du Pont De Nemours And Company Production of aromatic carboxylic acids
US6521777B2 (en) 2000-12-14 2003-02-18 General Electric Company Process for the production of diaryl carbonates
US6420589B1 (en) 2000-12-14 2002-07-16 General Electric Company Process for the production of diaryl carbonates
US6384262B1 (en) 2000-12-14 2002-05-07 General Electric Company Process for the production of diaryl carbonates
WO2004005235A1 (en) * 2002-07-09 2004-01-15 Invista Technologies S.À.R.L. Process for producing aromatic dicarboxylic acids under supercritical conditions
US7276625B2 (en) * 2002-10-15 2007-10-02 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
BR0316462A (pt) * 2002-12-09 2005-10-11 Eastman Chem Co Processos para reduzir uma suspensão de ácido carboxìlico purificado, para purificar um produto de oxidação em estágios, para produzir um produto de ácido carboxìlico purificado, e, suspensão de ácido carboxìlico purificado
US7161027B2 (en) 2002-12-09 2007-01-09 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7132566B2 (en) * 2003-09-22 2006-11-07 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
KR100498490B1 (ko) * 2003-02-28 2005-07-01 삼성전자주식회사 인페이스 신호와 쿼드러쳐 신호 간의 위상차를 가변시킬수 있는 쿼드러쳐 전압제어 발진기
US7193109B2 (en) 2003-03-06 2007-03-20 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
US20050059709A1 (en) * 2003-09-15 2005-03-17 Meythaler Jay M. Treatment of a neuropathy with rapid release aminopyridine
US7214760B2 (en) * 2004-01-15 2007-05-08 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
US7546747B2 (en) * 2004-01-15 2009-06-16 Eastman Chemical Company Process for production of a dried carboxylic acid cake suitable for use in polyester production
US20050283022A1 (en) * 2004-06-18 2005-12-22 Sheppard Ronald B Filtrate preparation process for terephthalic acid filtrate treatment
US7692037B2 (en) 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7582793B2 (en) 2004-09-02 2009-09-01 Eastman Chemical Company Optimized liquid-phase oxidation
US7504535B2 (en) 2004-09-02 2009-03-17 Eastman Chemical Company Optimized liquid-phase oxidation
US7399882B2 (en) * 2004-09-02 2008-07-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7683210B2 (en) * 2004-09-02 2010-03-23 Eastman Chemical Company Optimized liquid-phase oxidation
US7692036B2 (en) * 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7586000B2 (en) * 2004-09-02 2009-09-08 Eastman Chemical Company Optimized liquid-phase oxidation
US20060047153A1 (en) * 2004-09-02 2006-03-02 Wonders Alan G Optimized liquid-phase oxidation
US7741515B2 (en) 2004-09-02 2010-06-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7390921B2 (en) * 2004-09-02 2008-06-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7910769B2 (en) * 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7495125B2 (en) * 2004-09-02 2009-02-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7608732B2 (en) * 2005-03-08 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7507857B2 (en) 2004-09-02 2009-03-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7568361B2 (en) * 2004-09-02 2009-08-04 Eastman Chemical Company Optimized liquid-phase oxidation
US7608733B2 (en) * 2004-09-02 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7361784B2 (en) * 2004-09-02 2008-04-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7371894B2 (en) * 2004-09-02 2008-05-13 Eastman Chemical Company Optimized liquid-phase oxidation
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US7572932B2 (en) * 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
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US7381836B2 (en) * 2004-09-02 2008-06-03 Eastman Chemical Company Optimized liquid-phase oxidation
US7482482B2 (en) * 2004-09-02 2009-01-27 Eastman Chemical Company Optimized liquid-phase oxidation
UA96569C2 (ru) 2005-03-21 2011-11-25 Бипи Корпорейшн Норт Америка Инк. Процесс и устройство для изготовления ароматических карбоновых кислот
US7884231B2 (en) 2005-05-19 2011-02-08 Eastman Chemical Company Process to produce an enriched composition
US7741516B2 (en) 2005-05-19 2010-06-22 Eastman Chemical Company Process to enrich a carboxylic acid composition
US7304178B2 (en) 2005-05-19 2007-12-04 Eastman Chemical Company Enriched isophthalic acid composition
US20060264662A1 (en) * 2005-05-19 2006-11-23 Gibson Philip E Esterification of an enriched composition
US7897809B2 (en) 2005-05-19 2011-03-01 Eastman Chemical Company Process to produce an enrichment feed
US7880031B2 (en) 2005-05-19 2011-02-01 Eastman Chemical Company Process to produce an enrichment feed
US20060264656A1 (en) * 2005-05-19 2006-11-23 Fujitsu Limited Enrichment process using compounds useful in a polyester process
US7557243B2 (en) 2005-05-19 2009-07-07 Eastman Chemical Company Enriched terephthalic acid composition
US20060264664A1 (en) * 2005-05-19 2006-11-23 Parker Kenny R Esterification of an exchange solvent enriched composition
US7919652B2 (en) 2005-05-19 2011-04-05 Eastman Chemical Company Process to produce an enriched composition through the use of a catalyst removal zone and an enrichment zone
US7432395B2 (en) 2005-05-19 2008-10-07 Eastman Chemical Company Enriched carboxylic acid composition
US7834208B2 (en) 2005-05-19 2010-11-16 Eastman Chemical Company Process to produce a post catalyst removal composition
KR100708919B1 (ko) * 2005-05-30 2007-04-17 삼성석유화학(주) 테레프탈산의 회수 방법
US7884232B2 (en) * 2005-06-16 2011-02-08 Eastman Chemical Company Optimized liquid-phase oxidation
KR20080091453A (ko) 2005-12-29 2008-10-13 비피 코포레이션 노쓰 아메리카 인코포레이티드 Det를 형성하기 위한 pet의 가에탄올분해 및 그의산화
US7358389B2 (en) * 2006-01-04 2008-04-15 Eastman Chemical Company Oxidation system employing internal structure for enhanced hydrodynamics
US7355068B2 (en) * 2006-01-04 2008-04-08 Eastman Chemical Company Oxidation system with internal secondary reactor
US20070179312A1 (en) * 2006-02-02 2007-08-02 O'meadhra Ruairi Seosamh Process for the purification of a crude carboxylic axid slurry
US8697906B2 (en) * 2006-03-01 2014-04-15 Grupo Petrotemex, S.A. De C.V. Methods and apparatus for producing a low-moisture carboxylic acid wet cake
US8173836B2 (en) * 2006-03-01 2012-05-08 Grupo Petrotemex, S.A. De C.V. Method and apparatus for drying carboxylic acid
US7847121B2 (en) * 2006-03-01 2010-12-07 Eastman Chemical Company Carboxylic acid production process
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US7888529B2 (en) 2006-03-01 2011-02-15 Eastman Chemical Company Process to produce a post catalyst removal composition
US7462736B2 (en) * 2006-03-01 2008-12-09 Eastman Chemical Company Methods and apparatus for isolating carboxylic acid
CN100368370C (zh) * 2006-03-29 2008-02-13 中国石化仪征化纤股份有限公司 对二甲苯氧化母液中悬浮物的回收系统装置
US8115029B2 (en) 2006-11-02 2012-02-14 University Of Kansas Cobalt-catalyzed oxidations in volumetrically expanded liquids by compressed gases
RU2463096C2 (ru) * 2007-12-20 2012-10-10 Хитачи Плант Текнолоджиз, Лтд. Способ фильтрации кристаллической суспензии
US8614350B2 (en) 2008-01-15 2013-12-24 Eastman Chemical Company Carboxylic acid production process employing solvent from esterification of lignocellulosic material
US8455680B2 (en) 2008-01-15 2013-06-04 Eastman Chemical Company Carboxylic acid production process employing solvent from esterification of lignocellulosic material
CN101417943B (zh) * 2008-12-08 2010-11-10 中国纺织工业设计院 高效回收利用pta装置精制母液的简易方法和系统
US8636898B2 (en) * 2010-04-30 2014-01-28 Antonio Perez Site drainer
CN101914013B (zh) * 2010-07-30 2015-03-18 浙江大学 一种节水的对苯二甲酸生产方法
US8466312B2 (en) * 2010-08-20 2013-06-18 Grupo Petrotemex, S.A. De C.V. Terephthalic acid purge filtration rate by controlling % water in filter feed slurry
EP2691378B1 (de) * 2011-03-28 2015-04-22 DSM IP Assets B.V. Verfahren zur herstellung von kondensationsprodukten von melamin
US20140175025A1 (en) * 2012-12-21 2014-06-26 Eastman Chemical Company Generation of low-solids second mother liquor from terephthalic acid production filter
CN104338499B (zh) * 2013-07-31 2016-01-20 沅江华龙催化科技有限公司 一种液固多相反应分离同步反应器
CN104338500B (zh) * 2013-07-31 2015-12-02 沅江华龙催化科技有限公司 一种气液固多相反应分离同步反应器
CA2933721A1 (en) 2013-12-18 2015-06-25 Bp Corporation North America Inc. Improved process and apparatus for manufacturing aromatic carboxylic acids
CA2934789C (en) 2013-12-30 2021-03-02 Thomas M. Bartos Pressurized crude aromatic carboxylic acid feed mixes
CN103772182B (zh) * 2014-01-26 2015-06-17 沅江华龙催化科技有限公司 基于气液固多相反应分离同步反应器的利用空气氧化对二甲苯生产对苯二甲酸的方法
JP2015140342A (ja) * 2014-01-30 2015-08-03 株式会社日立製作所 精製テレフタル酸の製造方法
CN103936581A (zh) 2014-04-24 2014-07-23 天华化工机械及自动化研究设计院有限公司 一种提高cta溶剂交换效率的方法
CN105085231A (zh) 2014-05-20 2015-11-25 天华化工机械及自动化研究设计院有限公司 一种pta工业装置氧化单元中醋酸溶剂的处理方法
CN115867683A (zh) 2020-08-14 2023-03-28 科氏技术英国有限公司 从氧化剂清洗流中回收金属催化剂
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Also Published As

Publication number Publication date
RU2106337C1 (ru) 1998-03-10
ID19108A (id) 1998-06-18
EP0722927A1 (de) 1996-07-24
GB9104776D0 (en) 1991-04-17
ES2142006T3 (es) 2000-04-01
ZA921380B (en) 1993-08-25
US5877346A (en) 1999-03-02
CN1067977C (zh) 2001-07-04
DE69214859D1 (de) 1996-12-05
CN1038409C (zh) 1998-05-20
EG19876A (en) 1996-06-30
EP0502628A3 (en) 1993-01-27
CN1064676A (zh) 1992-09-23
EP0754673B1 (de) 2000-01-12
US5527957A (en) 1996-06-18
CN1150945A (zh) 1997-06-04
JPH0565246A (ja) 1993-03-19
CA2062063C (en) 2002-07-09
GB9203674D0 (en) 1992-04-08
MX9200997A (es) 1992-10-01
ES2093189T3 (es) 1996-12-16
US5563293A (en) 1996-10-08
DE69230569T2 (de) 2000-07-27
EP0754673A1 (de) 1997-01-22
US5679846A (en) 1997-10-21
DE69214859T2 (de) 1997-02-27
KR100225371B1 (ko) 1999-10-15
EP0502628A2 (de) 1992-09-09
EP0502628B1 (de) 1996-10-30
KR920018005A (ko) 1992-10-21
CA2062063A1 (en) 1992-09-08
SG66231A1 (en) 1999-10-19

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