DE69002719T2 - Silizium enthaltender umweltschützender wirkstoff, welcher radioaktive metallisotopen und giftige schwere metalle adsorbiert sowie denselben enthaltende pharmazeutische zusammensetzung. - Google Patents
Silizium enthaltender umweltschützender wirkstoff, welcher radioaktive metallisotopen und giftige schwere metalle adsorbiert sowie denselben enthaltende pharmazeutische zusammensetzung.Info
- Publication number
- DE69002719T2 DE69002719T2 DE90904923T DE69002719T DE69002719T2 DE 69002719 T2 DE69002719 T2 DE 69002719T2 DE 90904923 T DE90904923 T DE 90904923T DE 69002719 T DE69002719 T DE 69002719T DE 69002719 T2 DE69002719 T2 DE 69002719T2
- Authority
- DE
- Germany
- Prior art keywords
- weight
- diatomaceous earth
- agent
- minerals
- mxo
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 230000002285 radioactive effect Effects 0.000 title claims description 15
- 229910001385 heavy metal Inorganic materials 0.000 title claims description 8
- 229910052751 metal Inorganic materials 0.000 title claims description 7
- 239000002184 metal Substances 0.000 title claims description 7
- 231100000331 toxic Toxicity 0.000 title claims description 6
- 230000002588 toxic effect Effects 0.000 title claims description 6
- 239000008194 pharmaceutical composition Substances 0.000 title description 5
- 239000013543 active substance Substances 0.000 title description 2
- 230000001681 protective effect Effects 0.000 title 1
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 48
- 239000011707 mineral Substances 0.000 claims description 48
- 239000003795 chemical substances by application Substances 0.000 claims description 33
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 24
- 239000005909 Kieselgur Substances 0.000 claims description 22
- 239000010457 zeolite Substances 0.000 claims description 22
- 241001465754 Metazoa Species 0.000 claims description 18
- 229910021536 Zeolite Inorganic materials 0.000 claims description 18
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 17
- 239000002245 particle Substances 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 9
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 8
- 229910052593 corundum Inorganic materials 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 229910001845 yogo sapphire Inorganic materials 0.000 claims description 8
- 239000004480 active ingredient Substances 0.000 claims description 6
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 5
- 239000011575 calcium Substances 0.000 claims description 5
- 229910052791 calcium Inorganic materials 0.000 claims description 5
- 150000002739 metals Chemical class 0.000 claims description 5
- 229910052700 potassium Inorganic materials 0.000 claims description 5
- 239000011591 potassium Substances 0.000 claims description 5
- 229910052708 sodium Inorganic materials 0.000 claims description 5
- 239000011734 sodium Substances 0.000 claims description 5
- 238000001179 sorption measurement Methods 0.000 claims description 5
- 239000003937 drug carrier Substances 0.000 claims description 3
- 239000008203 oral pharmaceutical composition Substances 0.000 claims description 3
- 230000007613 environmental effect Effects 0.000 claims 1
- 239000011814 protection agent Substances 0.000 claims 1
- 239000003223 protective agent Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 description 16
- 239000004615 ingredient Substances 0.000 description 9
- 230000037213 diet Effects 0.000 description 7
- 235000005911 diet Nutrition 0.000 description 7
- 239000002689 soil Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- 150000002500 ions Chemical class 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- AIYUHDOJVYHVIT-UHFFFAOYSA-M caesium chloride Chemical compound [Cl-].[Cs+] AIYUHDOJVYHVIT-UHFFFAOYSA-M 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 241000700159 Rattus Species 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
- 238000011109 contamination Methods 0.000 description 3
- 239000008367 deionised water Substances 0.000 description 3
- 229910021641 deionized water Inorganic materials 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 239000010703 silicon Substances 0.000 description 3
- 241000699670 Mus sp. Species 0.000 description 2
- 238000010306 acid treatment Methods 0.000 description 2
- 239000003463 adsorbent Substances 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 229910052793 cadmium Inorganic materials 0.000 description 2
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 2
- UNYSKUBLZGJSLV-UHFFFAOYSA-L calcium;1,3,5,2,4,6$l^{2}-trioxadisilaluminane 2,4-dioxide;dihydroxide;hexahydrate Chemical compound O.O.O.O.O.O.[OH-].[OH-].[Ca+2].O=[Si]1O[Al]O[Si](=O)O1.O=[Si]1O[Al]O[Si](=O)O1 UNYSKUBLZGJSLV-UHFFFAOYSA-L 0.000 description 2
- 229910052676 chabazite Inorganic materials 0.000 description 2
- 238000004880 explosion Methods 0.000 description 2
- 230000035876 healing Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- 206010000372 Accident at work Diseases 0.000 description 1
- 229910052684 Cerium Inorganic materials 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000011260 aqueous acid Substances 0.000 description 1
- 230000037396 body weight Effects 0.000 description 1
- WLZRMCYVCSSEQC-UHFFFAOYSA-N cadmium(2+) Chemical compound [Cd+2] WLZRMCYVCSSEQC-UHFFFAOYSA-N 0.000 description 1
- 229910052792 caesium Inorganic materials 0.000 description 1
- NCMHKCKGHRPLCM-UHFFFAOYSA-N caesium(1+) Chemical compound [Cs+] NCMHKCKGHRPLCM-UHFFFAOYSA-N 0.000 description 1
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000003631 expected effect Effects 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000002496 gastric effect Effects 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 229910052901 montmorillonite Inorganic materials 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000012857 radioactive material Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000012488 sample solution Substances 0.000 description 1
- 239000010801 sewage sludge Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 230000002123 temporal effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21F—PROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR
- G21F9/00—Treating radioactively contaminated material; Decontamination arrangements therefor
- G21F9/04—Treating liquids
- G21F9/06—Processing
- G21F9/12—Processing by absorption; by adsorption; by ion-exchange
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P3/00—Drugs for disorders of the metabolism
- A61P3/12—Drugs for disorders of the metabolism for electrolyte homeostasis
- A61P3/14—Drugs for disorders of the metabolism for electrolyte homeostasis for calcium homeostasis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P39/00—General protective or antinoxious agents
- A61P39/02—Antidotes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
- B01J39/08—Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
- B01J39/14—Base exchange silicates, e.g. zeolites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
- B09B3/10—Destroying solid waste or transforming solid waste into something useful or harmless involving an adsorption step
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09C—RECLAMATION OF CONTAMINATED SOIL
- B09C1/00—Reclamation of contaminated soil
- B09C1/08—Reclamation of contaminated soil chemically
Landscapes
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Medicinal Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Epidemiology (AREA)
- Soil Sciences (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- General Engineering & Computer Science (AREA)
- High Energy & Nuclear Physics (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- General Chemical & Material Sciences (AREA)
- Rheumatology (AREA)
- Obesity (AREA)
- Diabetes (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Endocrinology (AREA)
- Toxicology (AREA)
- Hematology (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Processing Of Solid Wastes (AREA)
- Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| HU891511A HU206484B (en) | 1989-03-24 | 1989-03-24 | Silicium-containing environment-protecting composition adsorbing radioactive metal-isotopes and toxic heavy metals and process for producing pharmaceutical compositions containing this active component |
| PCT/HU1990/000020 WO1990011143A1 (en) | 1989-03-24 | 1990-03-21 | Silicon-containing environment-protective agent adsorbing radioactive metal isotopes and toxic heavy metals and a pharmaceutical composition containing same |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69002719D1 DE69002719D1 (de) | 1993-09-16 |
| DE69002719T2 true DE69002719T2 (de) | 1994-03-24 |
Family
ID=10954805
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE90904923T Expired - Fee Related DE69002719T2 (de) | 1989-03-24 | 1990-03-21 | Silizium enthaltender umweltschützender wirkstoff, welcher radioaktive metallisotopen und giftige schwere metalle adsorbiert sowie denselben enthaltende pharmazeutische zusammensetzung. |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US5264225A (enExample) |
| EP (1) | EP0417238B1 (enExample) |
| JP (1) | JPH03504827A (enExample) |
| KR (1) | KR920700073A (enExample) |
| AU (1) | AU622306B2 (enExample) |
| CA (1) | CA2030542A1 (enExample) |
| CS (1) | CS276789B6 (enExample) |
| DE (1) | DE69002719T2 (enExample) |
| HU (1) | HU206484B (enExample) |
| IN (1) | IN170317B (enExample) |
| WO (1) | WO1990011143A1 (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3259853B2 (ja) * | 1991-10-21 | 2002-02-25 | 尚明 山本 | 害虫駆除材 |
| AU6141196A (en) * | 1995-06-14 | 1997-01-15 | Envirosil Limited | Treatment of contaminated soils |
| ITMI20021246A1 (it) * | 2002-06-07 | 2003-12-09 | Geomedical S R L | Composizioni minerali detossinanti a base di zeoliti ad elevata capacita' di scambio cationico |
| KR20050108370A (ko) * | 2003-03-03 | 2005-11-16 | 닛폰 이타가라스 가부시키가이샤 | 토양 개량제 |
| US20050031708A1 (en) * | 2003-08-06 | 2005-02-10 | Portney Micah S. | Composition comprising a zeolite compound for treatment of diseases |
| EP1679962B1 (en) | 2003-10-20 | 2021-01-13 | Framework Therapeutics, L.L.C. | Zeolite molecular sieves for the removal of toxins |
| JP6032633B2 (ja) * | 2011-07-05 | 2016-11-30 | 国立大学法人北海道大学 | 放射能汚染水中の放射性物質の除去方法及び装置 |
| JP2013088422A (ja) * | 2011-10-14 | 2013-05-13 | Yoichiro Yamanobe | 放射能汚染土壌の除洗方法 |
| JP6376428B2 (ja) * | 2012-03-19 | 2018-08-22 | 東京電力ホールディングス株式会社 | セシウム汚染土壌の除染方法 |
| RU2625497C1 (ru) * | 2016-10-18 | 2017-07-14 | Федеральное государственное бюджетное образовательное учреждение высшего образования Горский государственный аграрный университет | Способ производства пищевой добавки из дикорастущего растения люпина |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3449492A (en) * | 1964-10-05 | 1969-06-10 | Upjohn Co | Water reconstitutable kaolin-pectin powders |
| US3687680A (en) * | 1970-08-04 | 1972-08-29 | Bio Med Research Corp | Animal feed containing mortmorillonite clay |
| JPS5116491B2 (enExample) * | 1971-10-08 | 1976-05-25 | ||
| JPS5320437A (en) * | 1976-08-05 | 1978-02-24 | Katsuo Makita | Prevention and treatment method for pig gastric ulcer |
| FR2397189A1 (fr) * | 1977-07-13 | 1979-02-09 | Siran De Cavanac Raymond | Composition de boues thermales, de produits medicaux-thermaux, de sante, de beaute et de toilette |
| HU180443B (en) * | 1979-04-02 | 1983-03-28 | Chinoin Gyogyszer Es Vegyeszet | Process for preparing a pharmaceutical preparation with synergetic action against radiation |
| US4610883A (en) * | 1983-03-14 | 1986-09-09 | Ethyl Corporation | Method of improving liveability of poultry |
| DE3337335C2 (de) * | 1983-10-13 | 1987-01-08 | Technischer Überwachungs-Verein Bayern e.V., 8000 München | Jodpräparat und Verfahren zu dessen Herstellung |
| US4698335A (en) * | 1984-09-27 | 1987-10-06 | University Of Medicine & Dentistry Of New Jersey | Process for treating a warm-blooded animal to be subjected to radiotherapy |
-
1989
- 1989-03-24 HU HU891511A patent/HU206484B/hu unknown
-
1990
- 1990-03-21 AU AU52892/90A patent/AU622306B2/en not_active Ceased
- 1990-03-21 DE DE90904923T patent/DE69002719T2/de not_active Expired - Fee Related
- 1990-03-21 CA CA002030542A patent/CA2030542A1/en not_active Abandoned
- 1990-03-21 WO PCT/HU1990/000020 patent/WO1990011143A1/en not_active Ceased
- 1990-03-21 JP JP2504983A patent/JPH03504827A/ja active Pending
- 1990-03-21 US US07/635,635 patent/US5264225A/en not_active Expired - Fee Related
- 1990-03-21 EP EP90904923A patent/EP0417238B1/en not_active Expired - Lifetime
- 1990-03-23 IN IN215/MAS/90A patent/IN170317B/en unknown
- 1990-03-23 CS CS901428A patent/CS276789B6/cs unknown
- 1990-11-24 KR KR1019900702509A patent/KR920700073A/ko not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| CS9001428A2 (en) | 1991-08-13 |
| CS276789B6 (en) | 1992-08-12 |
| CA2030542A1 (en) | 1990-09-25 |
| AU622306B2 (en) | 1992-04-02 |
| US5264225A (en) | 1993-11-23 |
| AU5289290A (en) | 1990-10-22 |
| EP0417238A1 (en) | 1991-03-20 |
| KR920700073A (ko) | 1992-02-19 |
| EP0417238B1 (en) | 1993-08-11 |
| WO1990011143A1 (en) | 1990-10-04 |
| HU206484B (en) | 1992-11-30 |
| JPH03504827A (ja) | 1991-10-24 |
| DE69002719D1 (de) | 1993-09-16 |
| IN170317B (enExample) | 1992-03-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8380 | Miscellaneous part iii |
Free format text: DER PATENTINHABER LAUTET RICHTIG: AGROMEN AGRARMENEDZSERI RESZVENYTARSASAG, SZOLNOK, HU ORSZAGOS "FREDERIC JOLIOT-CURIE" SUGARBIOLOGIA ES SUGAREGESZSEGUGYI KUTATO INTEZET, BUDAPEST, HU MAGYAR KUELKERESKEDELMI BANK RT, BUDAPEST, HU |
|
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |