DE60304214D1 - Verfahren zur herstellung von mercaptoalkylalkoxysilanen - Google Patents
Verfahren zur herstellung von mercaptoalkylalkoxysilanenInfo
- Publication number
- DE60304214D1 DE60304214D1 DE60304214T DE60304214T DE60304214D1 DE 60304214 D1 DE60304214 D1 DE 60304214D1 DE 60304214 T DE60304214 T DE 60304214T DE 60304214 T DE60304214 T DE 60304214T DE 60304214 D1 DE60304214 D1 DE 60304214D1
- Authority
- DE
- Germany
- Prior art keywords
- mercaptoalkylalkoxysilanes
- water soluble
- added
- soluble byproducts
- aqueous phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000006227 byproduct Substances 0.000 abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
- 239000008346 aqueous phase Substances 0.000 abstract 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 2
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 abstract 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 239000003002 pH adjusting agent Substances 0.000 abstract 2
- 239000003444 phase transfer catalyst Substances 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 abstract 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 abstract 1
- 239000004327 boric acid Substances 0.000 abstract 1
- 239000001569 carbon dioxide Substances 0.000 abstract 1
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
- C07F7/1872—Preparation; Treatments not provided for in C07F7/20
- C07F7/1892—Preparation; Treatments not provided for in C07F7/20 by reactions not provided for in C07F7/1876 - C07F7/1888
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US219080 | 2002-08-16 | ||
| US10/219,080 US6680398B1 (en) | 2002-08-16 | 2002-08-16 | Method of making mercaptoalkylalkoxysilanes |
| PCT/US2003/025101 WO2004016629A1 (en) | 2002-08-16 | 2003-08-11 | Method of making mercaptoalkylalkoxysilanes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE60304214D1 true DE60304214D1 (de) | 2006-05-11 |
| DE60304214T2 DE60304214T2 (de) | 2007-03-29 |
Family
ID=30000163
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE60304214T Expired - Lifetime DE60304214T2 (de) | 2002-08-16 | 2003-08-11 | Verfahren zur herstellung von marcaptoalkylalkoxysilanen |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6680398B1 (de) |
| EP (1) | EP1534719B1 (de) |
| JP (1) | JP4443408B2 (de) |
| KR (1) | KR100953282B1 (de) |
| CN (1) | CN1319977C (de) |
| AT (1) | ATE321056T1 (de) |
| AU (1) | AU2003264043A1 (de) |
| DE (1) | DE60304214T2 (de) |
| WO (1) | WO2004016629A1 (de) |
Families Citing this family (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7388087B2 (en) * | 2000-11-09 | 2008-06-17 | The Board Of Trustees Of The University Of Illinois | Enhancement of immune response to vaccine by interferon alpha |
| US20040227127A1 (en) * | 2003-01-31 | 2004-11-18 | Boswell Lisa Marie | Hydrophobing silica with organosilicon compounds and blends thereof |
| US8008520B2 (en) * | 2003-07-03 | 2011-08-30 | Momentive Performance Materials Inc. | Process for the preparation of thiocarboxylate silane |
| DE102005020534B4 (de) | 2004-09-07 | 2006-07-06 | Degussa Ag | Verfahren zur Herstellung von Mercaptoorganyl(alkoxysilanen) |
| CN1746175B (zh) * | 2004-09-11 | 2010-06-23 | 张家港市国泰华荣化工新材料有限公司 | 巯基烷基烷氧基硅烷的制备方法 |
| US6998452B1 (en) | 2005-01-14 | 2006-02-14 | The Goodyear Tire & Rubber Company | Controlled free radical agent for nanocomposite synthesis |
| DE102005038791A1 (de) * | 2005-08-17 | 2007-02-22 | Degussa Ag | Organosiliciumverbindungen, ihre Herstellung und ihre Verwendung |
| US7151188B1 (en) | 2005-11-16 | 2006-12-19 | General Electric Company | Process for the production of mercaptoalkylalkoxysilanes |
| DE102005060122A1 (de) * | 2005-12-16 | 2007-06-21 | Degussa Gmbh | Verfahren zur Herstellung von (Mercaptoorganyl)alkylpolyethersilanen |
| DE102006027235A1 (de) * | 2006-06-09 | 2008-01-17 | Evonik Degussa Gmbh | Kautschukmischungen |
| DE102006041356A1 (de) * | 2006-09-01 | 2008-03-20 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Organosilanen |
| DE102007037556A1 (de) | 2007-08-09 | 2009-02-12 | Evonik Degussa Gmbh | Verfahren zur Herstellung von alkylpolyethersubstituierten Mercaptosilanen |
| CN101423528B (zh) * | 2007-11-02 | 2012-07-25 | 张家港市国泰华荣化工新材料有限公司 | 巯基烷基烷氧基硅烷的制备方法 |
| DE102007062282A1 (de) * | 2007-12-21 | 2009-06-25 | Saltigo Gmbh | Verfahren zur Herstellung von Thiodiglycolsäuredialkylestern |
| DE102008035623A1 (de) * | 2008-07-31 | 2010-02-04 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Organosilanen |
| CN102241701B (zh) * | 2011-05-25 | 2014-03-12 | 泰山医学院 | 一种γ-巯丙基三乙氧基硅烷的合成方法 |
| JP2013181029A (ja) * | 2012-03-05 | 2013-09-12 | Daiso Co Ltd | 高純度のメルカプトシラン化合物の製造法。 |
| JP2013199441A (ja) * | 2012-03-23 | 2013-10-03 | Sumitomo Seika Chem Co Ltd | アルキルチオールの製造方法 |
| JP2014108923A (ja) * | 2012-11-30 | 2014-06-12 | Daiso Co Ltd | 有機珪素化合物 |
| CN103408582B (zh) * | 2013-09-04 | 2015-12-09 | 荆州市江汉精细化工有限公司 | 一种3-巯丙基三乙氧基硅烷偶联剂的制备方法 |
| CN104926854B (zh) * | 2014-03-23 | 2018-05-11 | 浙江新安化工集团股份有限公司 | 一种常压低温水相制备巯丙基三乙氧基硅烷的方法 |
| US20170210706A1 (en) * | 2014-08-07 | 2017-07-27 | Arkema Inc. | Synthesis of 2,2,2-trifluoroethanethiol |
| CN104926857B (zh) * | 2015-06-25 | 2017-10-31 | 嘉兴学院 | 3‑巯丙基三乙氧基硅烷的合成方法 |
| CN109320542A (zh) * | 2018-11-13 | 2019-02-12 | 江西宏柏新材料股份有限公司 | 含巯丙基的硅烷偶联剂的双釜串联合成方法 |
| CN115215898A (zh) * | 2022-07-29 | 2022-10-21 | 上海橡实化学有限公司 | 一种生产巯丙基三乙氧基硅烷的方法 |
| CN115873234A (zh) * | 2022-11-25 | 2023-03-31 | 广西珀源新材料有限公司 | 一种用于量产多元硫醇的方法及其制备的多元硫醇 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1102251A (en) | 1964-02-04 | 1968-02-07 | Union Carbide Corp | Treatment of metal surfaces |
| US3590065A (en) | 1969-07-18 | 1971-06-29 | Dow Corning | Method of preparing mercaptoalkylalkoxy silanes |
| US3849471A (en) | 1972-12-14 | 1974-11-19 | Union Carbide Corp | Process for reacting weak acids with chloroalkyl substituted silicon compounds |
| US3890213A (en) | 1973-08-28 | 1975-06-17 | Phillips Petroleum Co | Mercaptoalkyltrialkoxysilane production |
| US5405985A (en) | 1994-07-08 | 1995-04-11 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| US5840952A (en) | 1995-11-02 | 1998-11-24 | Shin-Etsu Chemical Co., Ltd. | Method of manufacturing 3-mercaptopropylalkoxy silane |
| US5583245A (en) | 1996-03-06 | 1996-12-10 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| US6384256B1 (en) | 2001-06-29 | 2002-05-07 | Dow Corning Corporation | Process for the preparation of sulfur-containing organosilicon compounds |
-
2002
- 2002-08-16 US US10/219,080 patent/US6680398B1/en not_active Expired - Lifetime
-
2003
- 2003-08-11 DE DE60304214T patent/DE60304214T2/de not_active Expired - Lifetime
- 2003-08-11 KR KR1020057002542A patent/KR100953282B1/ko active IP Right Grant
- 2003-08-11 EP EP03788381A patent/EP1534719B1/de not_active Expired - Lifetime
- 2003-08-11 AU AU2003264043A patent/AU2003264043A1/en not_active Abandoned
- 2003-08-11 CN CNB03818799XA patent/CN1319977C/zh not_active Expired - Lifetime
- 2003-08-11 JP JP2004529301A patent/JP4443408B2/ja not_active Expired - Lifetime
- 2003-08-11 AT AT03788381T patent/ATE321056T1/de not_active IP Right Cessation
- 2003-08-11 WO PCT/US2003/025101 patent/WO2004016629A1/en active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| DE60304214T2 (de) | 2007-03-29 |
| ATE321056T1 (de) | 2006-04-15 |
| US6680398B1 (en) | 2004-01-20 |
| WO2004016629A1 (en) | 2004-02-26 |
| CN1319977C (zh) | 2007-06-06 |
| CN1675228A (zh) | 2005-09-28 |
| EP1534719A1 (de) | 2005-06-01 |
| JP4443408B2 (ja) | 2010-03-31 |
| JP2005535721A (ja) | 2005-11-24 |
| EP1534719B1 (de) | 2006-03-22 |
| KR20050044903A (ko) | 2005-05-13 |
| AU2003264043A1 (en) | 2004-03-03 |
| KR100953282B1 (ko) | 2010-04-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition |