DE60304214D1 - Verfahren zur herstellung von mercaptoalkylalkoxysilanen - Google Patents

Verfahren zur herstellung von mercaptoalkylalkoxysilanen

Info

Publication number
DE60304214D1
DE60304214D1 DE60304214T DE60304214T DE60304214D1 DE 60304214 D1 DE60304214 D1 DE 60304214D1 DE 60304214 T DE60304214 T DE 60304214T DE 60304214 T DE60304214 T DE 60304214T DE 60304214 D1 DE60304214 D1 DE 60304214D1
Authority
DE
Germany
Prior art keywords
mercaptoalkylalkoxysilanes
water soluble
added
soluble byproducts
aqueous phase
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60304214T
Other languages
English (en)
Other versions
DE60304214T2 (de
Inventor
Marie Boswell
Charles Maki
Kumar Tomar
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Silicones Corp
Original Assignee
Dow Corning Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Corning Corp filed Critical Dow Corning Corp
Application granted granted Critical
Publication of DE60304214D1 publication Critical patent/DE60304214D1/de
Publication of DE60304214T2 publication Critical patent/DE60304214T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic System
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic System
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C07F7/1804—Compounds having Si-O-C linkages
    • C07F7/1872—Preparation; Treatments not provided for in C07F7/20
    • C07F7/1892—Preparation; Treatments not provided for in C07F7/20 by reactions not provided for in C07F7/1876 - C07F7/1888
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic System
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
DE60304214T 2002-08-16 2003-08-11 Verfahren zur herstellung von marcaptoalkylalkoxysilanen Expired - Lifetime DE60304214T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US219080 1980-12-22
US10/219,080 US6680398B1 (en) 2002-08-16 2002-08-16 Method of making mercaptoalkylalkoxysilanes
PCT/US2003/025101 WO2004016629A1 (en) 2002-08-16 2003-08-11 Method of making mercaptoalkylalkoxysilanes

Publications (2)

Publication Number Publication Date
DE60304214D1 true DE60304214D1 (de) 2006-05-11
DE60304214T2 DE60304214T2 (de) 2007-03-29

Family

ID=30000163

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60304214T Expired - Lifetime DE60304214T2 (de) 2002-08-16 2003-08-11 Verfahren zur herstellung von marcaptoalkylalkoxysilanen

Country Status (9)

Country Link
US (1) US6680398B1 (de)
EP (1) EP1534719B1 (de)
JP (1) JP4443408B2 (de)
KR (1) KR100953282B1 (de)
CN (1) CN1319977C (de)
AT (1) ATE321056T1 (de)
AU (1) AU2003264043A1 (de)
DE (1) DE60304214T2 (de)
WO (1) WO2004016629A1 (de)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7388087B2 (en) * 2000-11-09 2008-06-17 The Board Of Trustees Of The University Of Illinois Enhancement of immune response to vaccine by interferon alpha
US20040227127A1 (en) * 2003-01-31 2004-11-18 Boswell Lisa Marie Hydrophobing silica with organosilicon compounds and blends thereof
US8008520B2 (en) * 2003-07-03 2011-08-30 Momentive Performance Materials Inc. Process for the preparation of thiocarboxylate silane
DE102005020534B4 (de) 2004-09-07 2006-07-06 Degussa Ag Verfahren zur Herstellung von Mercaptoorganyl(alkoxysilanen)
CN1746175B (zh) * 2004-09-11 2010-06-23 张家港市国泰华荣化工新材料有限公司 巯基烷基烷氧基硅烷的制备方法
US6998452B1 (en) 2005-01-14 2006-02-14 The Goodyear Tire & Rubber Company Controlled free radical agent for nanocomposite synthesis
DE102005038791A1 (de) * 2005-08-17 2007-02-22 Degussa Ag Organosiliciumverbindungen, ihre Herstellung und ihre Verwendung
US7151188B1 (en) 2005-11-16 2006-12-19 General Electric Company Process for the production of mercaptoalkylalkoxysilanes
DE102005060122A1 (de) * 2005-12-16 2007-06-21 Degussa Gmbh Verfahren zur Herstellung von (Mercaptoorganyl)alkylpolyethersilanen
DE102006027235A1 (de) * 2006-06-09 2008-01-17 Evonik Degussa Gmbh Kautschukmischungen
DE102006041356A1 (de) * 2006-09-01 2008-03-20 Evonik Degussa Gmbh Verfahren zur Herstellung von Organosilanen
DE102007037556A1 (de) 2007-08-09 2009-02-12 Evonik Degussa Gmbh Verfahren zur Herstellung von alkylpolyethersubstituierten Mercaptosilanen
CN101423528B (zh) * 2007-11-02 2012-07-25 张家港市国泰华荣化工新材料有限公司 巯基烷基烷氧基硅烷的制备方法
DE102007062282A1 (de) * 2007-12-21 2009-06-25 Saltigo Gmbh Verfahren zur Herstellung von Thiodiglycolsäuredialkylestern
DE102008035623A1 (de) * 2008-07-31 2010-02-04 Evonik Degussa Gmbh Verfahren zur Herstellung von Organosilanen
CN102241701B (zh) * 2011-05-25 2014-03-12 泰山医学院 一种γ-巯丙基三乙氧基硅烷的合成方法
JP2013181029A (ja) * 2012-03-05 2013-09-12 Daiso Co Ltd 高純度のメルカプトシラン化合物の製造法。
JP2013199441A (ja) * 2012-03-23 2013-10-03 Sumitomo Seika Chem Co Ltd アルキルチオールの製造方法
JP2014108923A (ja) * 2012-11-30 2014-06-12 Daiso Co Ltd 有機珪素化合物
CN103408582B (zh) * 2013-09-04 2015-12-09 荆州市江汉精细化工有限公司 一种3-巯丙基三乙氧基硅烷偶联剂的制备方法
CN104926854B (zh) * 2014-03-23 2018-05-11 浙江新安化工集团股份有限公司 一种常压低温水相制备巯丙基三乙氧基硅烷的方法
JP6620142B2 (ja) * 2014-08-07 2019-12-11 アーケマ・インコーポレイテッド ２，２，２−トリフルオロエタンチオールの合成
CN104926857B (zh) * 2015-06-25 2017-10-31 嘉兴学院 3‑巯丙基三乙氧基硅烷的合成方法
CN109320542A (zh) * 2018-11-13 2019-02-12 江西宏柏新材料股份有限公司 含巯丙基的硅烷偶联剂的双釜串联合成方法
CN115215898A (zh) * 2022-07-29 2022-10-21 上海橡实化学有限公司 一种生产巯丙基三乙氧基硅烷的方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1102251A (en) 1964-02-04 1968-02-07 Union Carbide Corp Treatment of metal surfaces
US3590065A (en) 1969-07-18 1971-06-29 Dow Corning Method of preparing mercaptoalkylalkoxy silanes
US3849471A (en) 1972-12-14 1974-11-19 Union Carbide Corp Process for reacting weak acids with chloroalkyl substituted silicon compounds
US3890213A (en) 1973-08-28 1975-06-17 Phillips Petroleum Co Mercaptoalkyltrialkoxysilane production
US5405985A (en) 1994-07-08 1995-04-11 The Goodyear Tire & Rubber Company Preparation of sulfur-containing organosilicon compounds
US5840952A (en) 1995-11-02 1998-11-24 Shin-Etsu Chemical Co., Ltd. Method of manufacturing 3-mercaptopropylalkoxy silane
US5583245A (en) 1996-03-06 1996-12-10 The Goodyear Tire & Rubber Company Preparation of sulfur-containing organosilicon compounds
US6384256B1 (en) 2001-06-29 2002-05-07 Dow Corning Corporation Process for the preparation of sulfur-containing organosilicon compounds

Also Published As

Publication number Publication date
DE60304214T2 (de) 2007-03-29
WO2004016629A1 (en) 2004-02-26
JP2005535721A (ja) 2005-11-24
CN1319977C (zh) 2007-06-06
US6680398B1 (en) 2004-01-20
EP1534719A1 (de) 2005-06-01
AU2003264043A1 (en) 2004-03-03
KR20050044903A (ko) 2005-05-13
ATE321056T1 (de) 2006-04-15
KR100953282B1 (ko) 2010-04-16
JP4443408B2 (ja) 2010-03-31
EP1534719B1 (de) 2006-03-22
CN1675228A (zh) 2005-09-28

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