DE60229389D1 - Verfahren zur herstellung schwefelhaltiger organosiliziumverbindungen - Google Patents
Verfahren zur herstellung schwefelhaltiger organosiliziumverbindungenInfo
- Publication number
- DE60229389D1 DE60229389D1 DE60229389T DE60229389T DE60229389D1 DE 60229389 D1 DE60229389 D1 DE 60229389D1 DE 60229389 T DE60229389 T DE 60229389T DE 60229389 T DE60229389 T DE 60229389T DE 60229389 D1 DE60229389 D1 DE 60229389D1
- Authority
- DE
- Germany
- Prior art keywords
- formula
- reacting
- carbon atoms
- alkali metal
- compound
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 150000001875 compounds Chemical class 0.000 title 1
- 238000000034 method Methods 0.000 abstract 5
- -1 alkali metal hydroxide compound Chemical class 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- 239000004215 Carbon black (E152) Substances 0.000 abstract 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- 150000003961 organosilicon compounds Chemical class 0.000 abstract 2
- 229920001021 polysulfide Polymers 0.000 abstract 2
- 239000005077 polysulfide Substances 0.000 abstract 2
- 150000008117 polysulfides Polymers 0.000 abstract 2
- 229910052717 sulfur Inorganic materials 0.000 abstract 2
- 239000011593 sulfur Substances 0.000 abstract 2
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 abstract 1
- 229910052783 alkali metal Chemical group 0.000 abstract 1
- 150000001340 alkali metals Chemical group 0.000 abstract 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 239000012467 final product Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 abstract 1
- 238000003408 phase transfer catalysis Methods 0.000 abstract 1
- 239000003444 phase transfer catalyst Substances 0.000 abstract 1
- 229910000077 silane Inorganic materials 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
- C07F7/1872—Preparation; Treatments not provided for in C07F7/20
- C07F7/1892—Preparation; Treatments not provided for in C07F7/20 by reactions not provided for in C07F7/1876 - C07F7/1888
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/895,720 US6384256B1 (en) | 2001-06-29 | 2001-06-29 | Process for the preparation of sulfur-containing organosilicon compounds |
| PCT/US2002/015194 WO2003002577A1 (en) | 2001-06-29 | 2002-05-13 | Process for the preparation of sulfur-containing organosilicon compounds |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE60229389D1 true DE60229389D1 (de) | 2008-11-27 |
Family
ID=25404953
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE60229389T Expired - Lifetime DE60229389D1 (de) | 2001-06-29 | 2002-05-13 | Verfahren zur herstellung schwefelhaltiger organosiliziumverbindungen |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6384256B1 (de) |
| EP (1) | EP1401843B1 (de) |
| JP (1) | JP4372542B2 (de) |
| KR (1) | KR100886096B1 (de) |
| CN (2) | CN100339381C (de) |
| AT (1) | ATE411327T1 (de) |
| DE (1) | DE60229389D1 (de) |
| TW (1) | TWI238825B (de) |
| WO (1) | WO2003002577A1 (de) |
Families Citing this family (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6465670B2 (en) * | 2000-08-01 | 2002-10-15 | The Goodyear Tire & Rubber Company | Preparation of surface modified silica |
| US6534668B2 (en) * | 2001-06-29 | 2003-03-18 | Dow Corning Corporation | Preparation of sulfur-containing organosilicon compounds using a buffered phase transfer catalysis process |
| DE10132939C1 (de) * | 2001-07-06 | 2003-01-30 | Degussa | Verfahren zur Herstellung von gelben Bis(3-[trialkoxysilyl]alkyl)polysulfanen |
| US6680398B1 (en) * | 2002-08-16 | 2004-01-20 | Dow Corning Corporation | Method of making mercaptoalkylalkoxysilanes |
| US8097743B2 (en) * | 2002-11-04 | 2012-01-17 | Momentive Performance Materials Inc. | Process for manufacture of blocked mercaptosilane coupling agents |
| US6740767B1 (en) * | 2002-11-12 | 2004-05-25 | Dow Corning Corporation | Method of making sulfur containing organosilicon compounds |
| US8008520B2 (en) * | 2003-07-03 | 2011-08-30 | Momentive Performance Materials Inc. | Process for the preparation of thiocarboxylate silane |
| JP4885857B2 (ja) * | 2004-06-09 | 2012-02-29 | ダウ・コーニング・コーポレイション | 電気ケーブル修復液用防食添加剤 |
| US6998452B1 (en) | 2005-01-14 | 2006-02-14 | The Goodyear Tire & Rubber Company | Controlled free radical agent for nanocomposite synthesis |
| DE102005037690A1 (de) * | 2005-08-10 | 2007-02-15 | Degussa Ag | Verfahren zur Herstellung von Organosiliciumverbindungen |
| WO2007061550A1 (en) | 2005-11-16 | 2007-05-31 | Dow Corning Corporation | Organosilanes and their preparation and use in elastomer compositions |
| FR2900151A1 (fr) * | 2006-04-24 | 2007-10-26 | Univ Grenoble 1 | Procede pour l'obtention de disulfures et thiosulfinates et composes obtenus |
| US8236945B2 (en) | 2006-04-24 | 2012-08-07 | Universite Joseph Fourier (Grenoble1) | Process for preparing disulfides and thiosulphinates and compounds prepared |
| DE102006041356A1 (de) * | 2006-09-01 | 2008-03-20 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Organosilanen |
| CN102037001A (zh) * | 2008-05-20 | 2011-04-27 | 大曹株式会社 | 新型含硫有机硅化合物的制备方法 |
| EP2290011A1 (de) | 2009-08-18 | 2011-03-02 | Heritage Environmental Services, Llc. | Verfahren zur Herstellung von Silizium-Schwefel-Verbindungen und ihre Verwendung in Bitumen-Zusammensetzungen |
| CN103772427B (zh) * | 2014-01-28 | 2016-03-02 | 南京曙光硅烷化工有限公司 | 双[丙基三乙氧基硅烷]二硫化物的制备方法 |
| CN103788121B (zh) * | 2014-01-28 | 2016-08-17 | 南京曙光硅烷化工有限公司 | 无缓冲剂生产浅色多硫化物硅烷偶联剂的方法 |
| CN105713032B (zh) * | 2016-01-21 | 2018-06-15 | 杭州硅畅科技有限公司 | 一种一锅法制备含硫硅烷偶联剂的方法 |
| EP3838905A1 (de) | 2019-12-18 | 2021-06-23 | Evonik Operations GmbH | Verfahren zur herstellung von polysulfansilanen mittels phasentransferkatalyse |
| DE102020211042A1 (de) | 2020-09-02 | 2022-03-03 | Evonik Operations Gmbh | Verfahren zur Herstellung von Polysulfansilanen mittels Phasentransferkatalyse |
| CN112920216A (zh) * | 2021-02-02 | 2021-06-08 | 山东阳谷华泰化工股份有限公司 | 双-[3-(三乙氧基硅)-丙基]-二硫化物的制备方法 |
| WO2023208772A1 (en) | 2022-04-26 | 2023-11-02 | Momentive Performance Materials Gmbh | Stabilized compositions of sulfur silanes with high mercapto content |
Family Cites Families (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3590065A (en) | 1969-07-18 | 1971-06-29 | Dow Corning | Method of preparing mercaptoalkylalkoxy silanes |
| US4082790A (en) | 1974-12-11 | 1978-04-04 | Dow Corning Corporation | Method of preparing mercaptans |
| US4401826A (en) | 1982-09-10 | 1983-08-30 | General Electric Company | Method for production of mercapto functional silanes |
| DE3346910C1 (de) | 1983-12-24 | 1985-05-02 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur Herstellung von Mercaptoalkylsilanen |
| DE4025866A1 (de) | 1990-08-16 | 1992-02-20 | Huels Chemische Werke Ag | Verfahren zur herstellung von mercaptosilanen |
| US5399739A (en) | 1994-04-18 | 1995-03-21 | Wright Chemical Corporation | Method of making sulfur-containing organosilanes |
| US5405985A (en) | 1994-07-08 | 1995-04-11 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| US5468893A (en) | 1994-07-08 | 1995-11-21 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| US5489701A (en) | 1994-09-28 | 1996-02-06 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
| US5466848A (en) | 1994-09-28 | 1995-11-14 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
| US5596116A (en) | 1995-09-11 | 1997-01-21 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
| US5840952A (en) | 1995-11-02 | 1998-11-24 | Shin-Etsu Chemical Co., Ltd. | Method of manufacturing 3-mercaptopropylalkoxy silane |
| US5583245A (en) | 1996-03-06 | 1996-12-10 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| US5663396A (en) * | 1996-10-31 | 1997-09-02 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| DE19651849A1 (de) | 1996-12-13 | 1998-06-18 | Degussa | Verfahren zur Herstellung von Bis(silylorganyl)-polysulfanen |
| DE19732725A1 (de) | 1997-07-30 | 1999-02-04 | Degussa | Mischungen, bestehend aus Bis(silylorganyl)polysulfanen und Silylorganylthiocyanaten, ihre Herstellung und Verwendung |
| DE19734295C1 (de) | 1997-08-08 | 1999-02-25 | Degussa | Verfahren zur Herstellung von Organosiliciumdisulfanen hoher Reinheit |
| JP3498559B2 (ja) | 1997-12-01 | 2004-02-16 | 信越化学工業株式会社 | 短鎖ポリスルフィドシラン混合物の製造方法 |
| JP3501008B2 (ja) | 1998-04-10 | 2004-02-23 | ダイソー株式会社 | 含硫黄有機珪素化合物の製造方法およびその合成中間体の製造方法 |
| DE19819373A1 (de) * | 1998-04-30 | 1999-11-04 | Degussa | Verfahren zur Herstellung von Gemischen von Organosiliciumoligosulfanen mit einem hohen Anteil an Organanosiliciumdisulfanen |
| US6172251B1 (en) * | 1998-07-24 | 2001-01-09 | The Goodyear Tire & Rubber Company | Solid/liquid phase transfer system |
| US6294683B1 (en) * | 1999-01-19 | 2001-09-25 | The Goodyear Tire & Rubber Company | Solid/liquid phase transfer system |
| DE19930495C1 (de) * | 1999-07-01 | 2000-11-09 | Degussa | Verfahren zur Herstellung von polysulfidischen Silanverbindungen |
-
2001
- 2001-06-29 US US09/895,720 patent/US6384256B1/en not_active Expired - Lifetime
-
2002
- 2002-05-13 WO PCT/US2002/015194 patent/WO2003002577A1/en active Application Filing
- 2002-05-13 CN CNB2005100703008A patent/CN100339381C/zh not_active Expired - Lifetime
- 2002-05-13 DE DE60229389T patent/DE60229389D1/de not_active Expired - Lifetime
- 2002-05-13 AT AT02736814T patent/ATE411327T1/de not_active IP Right Cessation
- 2002-05-13 EP EP02736814A patent/EP1401843B1/de not_active Expired - Lifetime
- 2002-05-13 CN CNB02813124XA patent/CN1280296C/zh not_active Expired - Lifetime
- 2002-05-13 JP JP2003508958A patent/JP4372542B2/ja not_active Expired - Lifetime
- 2002-05-13 KR KR1020037017150A patent/KR100886096B1/ko active IP Right Grant
- 2002-05-31 TW TW091111715A patent/TWI238825B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| EP1401843A1 (de) | 2004-03-31 |
| US6384256B1 (en) | 2002-05-07 |
| CN1680396A (zh) | 2005-10-12 |
| WO2003002577A1 (en) | 2003-01-09 |
| TWI238825B (en) | 2005-09-01 |
| EP1401843B1 (de) | 2008-10-15 |
| ATE411327T1 (de) | 2008-10-15 |
| JP2004531581A (ja) | 2004-10-14 |
| JP4372542B2 (ja) | 2009-11-25 |
| KR20040018405A (ko) | 2004-03-03 |
| CN100339381C (zh) | 2007-09-26 |
| CN1522261A (zh) | 2004-08-18 |
| KR100886096B1 (ko) | 2009-02-27 |
| CN1280296C (zh) | 2006-10-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition |