DE60229787D1 - Herstellung von schwefelhaltigen organosiliconverbindungen durch ein verfahren mit einem gepufferten phasentransferkatalysator - Google Patents

Herstellung von schwefelhaltigen organosiliconverbindungen durch ein verfahren mit einem gepufferten phasentransferkatalysator

Info

Publication number
DE60229787D1
DE60229787D1 DE60229787T DE60229787T DE60229787D1 DE 60229787 D1 DE60229787 D1 DE 60229787D1 DE 60229787 T DE60229787 T DE 60229787T DE 60229787 T DE60229787 T DE 60229787T DE 60229787 D1 DE60229787 D1 DE 60229787D1
Authority
DE
Germany
Prior art keywords
phase transfer
sulfur
transfer catalyst
formula
organosilicon compounds
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60229787T
Other languages
English (en)
Inventor
Michael Wolfgang Backer
Howard Marvin Bank
John Michael Gohndrone
William Charles Maki
Charles Edmund Skinner
Anil Kumar Tomar
Honggjun Yue
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Silicones Corp
Original Assignee
Dow Corning Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Corning Corp filed Critical Dow Corning Corp
Application granted granted Critical
Publication of DE60229787D1 publication Critical patent/DE60229787D1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C07F7/1804—Compounds having Si-O-C linkages
    • C07F7/1872—Preparation; Treatments not provided for in C07F7/20
    • C07F7/1892—Preparation; Treatments not provided for in C07F7/20 by reactions not provided for in C07F7/1876 - C07F7/1888

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE60229787T 2001-06-29 2002-05-13 Herstellung von schwefelhaltigen organosiliconverbindungen durch ein verfahren mit einem gepufferten phasentransferkatalysator Expired - Lifetime DE60229787D1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/895,719 US6534668B2 (en) 2001-06-29 2001-06-29 Preparation of sulfur-containing organosilicon compounds using a buffered phase transfer catalysis process
PCT/US2002/015162 WO2003002573A2 (en) 2001-06-29 2002-05-13 Preparation of sulfur-containing organosilicon compounds using a buffered phase transfer catalysis process

Publications (1)

Publication Number Publication Date
DE60229787D1 true DE60229787D1 (de) 2008-12-18

Family

ID=25404951

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60229787T Expired - Lifetime DE60229787D1 (de) 2001-06-29 2002-05-13 Herstellung von schwefelhaltigen organosiliconverbindungen durch ein verfahren mit einem gepufferten phasentransferkatalysator

Country Status (10)

Country Link
US (1) US6534668B2 (de)
EP (1) EP1480989B1 (de)
JP (1) JP4268039B2 (de)
KR (1) KR100835875B1 (de)
CN (1) CN1283644C (de)
AT (1) ATE413408T1 (de)
AU (1) AU2002308708A1 (de)
DE (1) DE60229787D1 (de)
TW (1) TW593326B (de)
WO (1) WO2003002573A2 (de)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4035690B2 (ja) * 2001-04-06 2008-01-23 信越化学工業株式会社 有機珪素化合物の製造方法
US6740767B1 (en) * 2002-11-12 2004-05-25 Dow Corning Corporation Method of making sulfur containing organosilicon compounds
US7125497B1 (en) * 2003-05-22 2006-10-24 Sandia Corporation Reactive formulations for a neutralization of toxic industrial chemicals
US8008520B2 (en) * 2003-07-03 2011-08-30 Momentive Performance Materials Inc. Process for the preparation of thiocarboxylate silane
CN1305879C (zh) * 2004-06-09 2007-03-21 上海人怡精细化工有限公司 一种相转移催化剂制造硅－69的工艺
EP1769512A1 (de) * 2004-06-09 2007-04-04 Dow Corning Corporation Antikorrosionszusatzstoff für restaurationsflüssigkeiten für elektrische kabel
US6998452B1 (en) 2005-01-14 2006-02-14 The Goodyear Tire & Rubber Company Controlled free radical agent for nanocomposite synthesis
DE102005037690A1 (de) * 2005-08-10 2007-02-15 Degussa Ag Verfahren zur Herstellung von Organosiliciumverbindungen
JP2007091678A (ja) * 2005-09-30 2007-04-12 Shin Etsu Chem Co Ltd スルフィド鎖含有有機珪素化合物の製造方法
JP2007091677A (ja) * 2005-09-30 2007-04-12 Shin Etsu Chem Co Ltd スルフィド鎖含有有機珪素化合物の製造方法
EP1948668A1 (de) * 2005-11-16 2008-07-30 Dow Corning Corporation Organosilane und ihre herstellung und verwendung in elastomerzusammensetzungen
DE102006041356A1 (de) 2006-09-01 2008-03-20 Evonik Degussa Gmbh Verfahren zur Herstellung von Organosilanen
DE102007062282A1 (de) * 2007-12-21 2009-06-25 Saltigo Gmbh Verfahren zur Herstellung von Thiodiglycolsäuredialkylestern
US9475998B2 (en) 2008-10-09 2016-10-25 Ceramatec, Inc. Process for recovering alkali metals and sulfur from alkali metal sulfides and polysulfides
US8728295B2 (en) * 2008-10-09 2014-05-20 Ceramatec, Inc. Apparatus and method for reducing an alkali metal electrochemically at a temperature below the metal's melting temperature
US8551339B2 (en) * 2009-03-06 2013-10-08 Heritage Environmental Services Llc Use of silica for the removal of organosilanes
CN102286017B (zh) * 2011-07-12 2014-06-18 泰山医学院 一种双-[丙基三乙氧基硅烷]-二硫化物的合成方法
CN102993228A (zh) * 2012-12-06 2013-03-27 青岛晟科材料有限公司 一种双-[丙基三甲氧基硅烷]-二硫化物硅烷偶联剂的合成方法
CN103772427B (zh) * 2014-01-28 2016-03-02 南京曙光硅烷化工有限公司 双[丙基三乙氧基硅烷]二硫化物的制备方法
JP6378100B2 (ja) * 2015-01-28 2018-08-22 住友ゴム工業株式会社 タイヤ用ゴム組成物およびタイヤ
EP3838905A1 (de) 2019-12-18 2021-06-23 Evonik Operations GmbH Verfahren zur herstellung von polysulfansilanen mittels phasentransferkatalyse
CN111269258B (zh) * 2020-03-19 2022-08-19 厦门威亮光学涂层技术有限公司 一种含硫有机硅化合物及其制备方法和用途
DE102020211042A1 (de) 2020-09-02 2022-03-03 Evonik Operations Gmbh Verfahren zur Herstellung von Polysulfansilanen mittels Phasentransferkatalyse
CN114478616B (zh) * 2022-01-12 2024-05-10 湖北江瀚新材料股份有限公司 一种3-(n-咪唑)丙基三乙氧基硅烷及其合成方法

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3590065A (en) 1969-07-18 1971-06-29 Dow Corning Method of preparing mercaptoalkylalkoxy silanes
US4082790A (en) 1974-12-11 1978-04-04 Dow Corning Corporation Method of preparing mercaptans
US4401826A (en) 1982-09-10 1983-08-30 General Electric Company Method for production of mercapto functional silanes
DE3346910C1 (de) 1983-12-24 1985-05-02 Dynamit Nobel Ag, 5210 Troisdorf Verfahren zur Herstellung von Mercaptoalkylsilanen
DE4025866A1 (de) 1990-08-16 1992-02-20 Huels Chemische Werke Ag Verfahren zur herstellung von mercaptosilanen
US5399739A (en) 1994-04-18 1995-03-21 Wright Chemical Corporation Method of making sulfur-containing organosilanes
US5468893A (en) 1994-07-08 1995-11-21 The Goodyear Tire & Rubber Company Preparation of sulfur-containing organosilicon compounds
US5405985A (en) 1994-07-08 1995-04-11 The Goodyear Tire & Rubber Company Preparation of sulfur-containing organosilicon compounds
US5489701A (en) 1994-09-28 1996-02-06 Osi Specialties, Inc. Process for the preparation of silane polysulfides
US5466848A (en) 1994-09-28 1995-11-14 Osi Specialties, Inc. Process for the preparation of silane polysulfides
US5596116A (en) 1995-09-11 1997-01-21 Osi Specialties, Inc. Process for the preparation of silane polysulfides
US5840952A (en) 1995-11-02 1998-11-24 Shin-Etsu Chemical Co., Ltd. Method of manufacturing 3-mercaptopropylalkoxy silane
US5583245A (en) 1996-03-06 1996-12-10 The Goodyear Tire & Rubber Company Preparation of sulfur-containing organosilicon compounds
US5663396A (en) 1996-10-31 1997-09-02 The Goodyear Tire & Rubber Company Preparation of sulfur-containing organosilicon compounds
DE19651849A1 (de) 1996-12-13 1998-06-18 Degussa Verfahren zur Herstellung von Bis(silylorganyl)-polysulfanen
DE19732725A1 (de) 1997-07-30 1999-02-04 Degussa Mischungen, bestehend aus Bis(silylorganyl)polysulfanen und Silylorganylthiocyanaten, ihre Herstellung und Verwendung
DE19734295C1 (de) 1997-08-08 1999-02-25 Degussa Verfahren zur Herstellung von Organosiliciumdisulfanen hoher Reinheit
JP3498559B2 (ja) 1997-12-01 2004-02-16 信越化学工業株式会社 短鎖ポリスルフィドシラン混合物の製造方法
JP3501008B2 (ja) 1998-04-10 2004-02-23 ダイソー株式会社 含硫黄有機珪素化合物の製造方法およびその合成中間体の製造方法
US6172251B1 (en) * 1998-07-24 2001-01-09 The Goodyear Tire & Rubber Company Solid/liquid phase transfer system
US6384256B1 (en) * 2001-06-29 2002-05-07 Dow Corning Corporation Process for the preparation of sulfur-containing organosilicon compounds

Also Published As

Publication number Publication date
CN1283644C (zh) 2006-11-08
WO2003002573A3 (en) 2004-09-02
CN1639173A (zh) 2005-07-13
WO2003002573A2 (en) 2003-01-09
TW593326B (en) 2004-06-21
AU2002308708A1 (en) 2003-03-03
EP1480989A2 (de) 2004-12-01
JP2005505512A (ja) 2005-02-24
US20030013901A1 (en) 2003-01-16
KR100835875B1 (ko) 2008-06-09
ATE413408T1 (de) 2008-11-15
US6534668B2 (en) 2003-03-18
KR20040015304A (ko) 2004-02-18
EP1480989B1 (de) 2008-11-05
JP4268039B2 (ja) 2009-05-27

Similar Documents

Publication Publication Date Title
DE60229787D1 (de) Herstellung von schwefelhaltigen organosiliconverbindungen durch ein verfahren mit einem gepufferten phasentransferkatalysator
ATE411327T1 (de) Verfahren zur herstellung schwefelhaltiger organosiliziumverbindungen
ATE314382T1 (de) Verfahren zur bereitung von organosilikonverbindungen die schwefel enthalten
KR960010660A (ko) 실란 폴리설파이드의 제조방법
GB1518560A (en) Process for the production of sulphur-containing organosilicon compounds
JPH11158192A (ja) 短鎖ポリスルフィドシラン混合物の製造方法
DE69406513T2 (de) Methode zur wiedergewinnung der schwefel-bindenden komponente aus dem reaktionsprodukt einer entschwefelungsreaktion
DE60018483D1 (de) Polysulfid-silane mit niedrigem schwefel-gehalt und ein verfahren zu deren herstellung
KR900012942A (ko) 아미노 프로필 알콕시 실란의 제조법
RU2008123798A (ru) Способ получения меркаптоалкилалкоксисиланов
EP0913401A3 (de) Fluor-enthaltende Siloxane und Verfahren zu deren Herstellung
ATE207055T1 (de) Verfahren zur herstellung von 4-aryl-3- hydroxymethyl-piperidinen
ATE40815T1 (de) Verfahren zur herstellung von siliciumwasserstoff-verbindungen, insbesondere des silans.
CA2022221C (en) N-n'-disubstituted and n,n,n'-or n,n',n'-trisubstituted thioureas
KR950008490A (ko) 히드록시옥사알킬멜라민류의 제조방법
ATE356134T1 (de) Verfahren zur herstellung von organosilanen
CN1218053A (zh) 降低双(甲硅烷基有机基)聚硫烷中硫烷链长的方法
ATE325159T1 (de) Verfahren zur herstellung von synergistischen stabilisatorgemischen
ATE202080T1 (de) Verfahren zur herstellung von 2-cyanobiphenyl verbindungen
JPS5910559A (ja) ジアルキルトリスルフイド類の製造法
MX9701413A (es) La preparacion de compuestos de organosilicio que contienen azufre.
EP1484311A4 (de) Verfahren zur herstellung von kettenoligomilchsäureester
KR970701180A (ko) 3-이속사졸카복실산의 제조 방법(process for producing 3-isoxazole-carboxylic acid)
GB0316268D0 (en) Process for preparing cyclic organohydrogensiloxanes
RU2021134459A (ru) Силан, каучуковая смесь, содержащая силан, и шина транспортного средства, которая содержит каучуковую смесь в по меньшей мере одном компоненте, а также способ получения силана

Legal Events

Date Code Title Description
8364 No opposition during term of opposition