DE60036613D1 - Massenfertigung von langen nanoröhrchen aus übergangsmetallchalcogeniden - Google Patents

Massenfertigung von langen nanoröhrchen aus übergangsmetallchalcogeniden

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Publication number
DE60036613D1
DE60036613D1 DE60036613T DE60036613T DE60036613D1 DE 60036613 D1 DE60036613 D1 DE 60036613D1 DE 60036613 T DE60036613 T DE 60036613T DE 60036613 T DE60036613 T DE 60036613T DE 60036613 D1 DE60036613 D1 DE 60036613D1
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DE
Germany
Prior art keywords
transition metal
sub
long
nanotones
mass production
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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DE60036613T
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English (en)
Other versions
DE60036613T2 (de
Inventor
Reshef Tenne
Aude Rothschild
Moshe Homyonfer
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Yeda Research and Development Co Ltd
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Yeda Research and Development Co Ltd
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Publication of DE60036613T2 publication Critical patent/DE60036613T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01Q—SCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q70/00—General aspects of SPM probes, their manufacture or their related instrumentation, insofar as they are not specially adapted to a single SPM technique covered by group G01Q60/00
    • G01Q70/08—Probe characteristics
    • G01Q70/10—Shape or taper
    • G01Q70/12—Nanotube tips
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/20—Methods for preparing sulfides or polysulfides, in general
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B19/00—Selenium; Tellurium; Compounds thereof
    • C01B19/02—Elemental selenium or tellurium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00—Compounds of tungsten
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00—Compounds of tungsten
    • C01G41/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B25/00—Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/005—Growth of whiskers or needles
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C30B29/46—Sulfur-, selenium- or tellurium-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/60—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape characterised by shape
    • C30B29/605—Products containing multiple oriented crystallites, e.g. columnar crystallites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/74—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by peak-intensities or a ratio thereof only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/82—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/10—Particle morphology extending in one dimension, e.g. needle-like
    • C01P2004/13—Nanotubes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/84—Manufacture, treatment, or detection of nanostructure
    • Y10S977/842—Manufacture, treatment, or detection of nanostructure for carbon nanotubes or fullerenes
    • Y10S977/844—Growth by vaporization or dissociation of carbon source using a high-energy heat source, e.g. electric arc, laser, plasma, e-beam

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Metallurgy (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Radiology & Medical Imaging (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • General Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Nanotechnology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
DE60036613T 1999-05-02 2000-05-02 Massenfertigung von langen nanoröhrchen aus übergangsmetallchalcogeniden Expired - Lifetime DE60036613T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IL12971899A IL129718A0 (en) 1999-05-02 1999-05-02 Synthesis of nanotubes of transition metal chalcogenides
IL12971899 1999-05-02
PCT/IL2000/000251 WO2000066485A1 (en) 1999-05-02 2000-05-02 Bulk synthesis of long nanotubes of transition metal chalcogenides

Publications (2)

Publication Number Publication Date
DE60036613D1 true DE60036613D1 (de) 2007-11-15
DE60036613T2 DE60036613T2 (de) 2008-07-10

Family

ID=11072753

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60036613T Expired - Lifetime DE60036613T2 (de) 1999-05-02 2000-05-02 Massenfertigung von langen nanoröhrchen aus übergangsmetallchalcogeniden

Country Status (7)

Country Link
US (3) US6841142B1 (de)
EP (1) EP1177153B1 (de)
AT (1) ATE374729T1 (de)
DE (1) DE60036613T2 (de)
ES (1) ES2293897T3 (de)
IL (1) IL129718A0 (de)
WO (1) WO2000066485A1 (de)

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WO2002022499A1 (en) 2000-09-18 2002-03-21 President And Fellows Of Harvard College Fabrication of nanotube microscopy tips
WO2002026624A1 (en) 2000-09-29 2002-04-04 President And Fellows Of Harvard College Direct growth of nanotubes, and their use in nanotweezers
IL139266A0 (en) 2000-10-25 2001-11-25 Yeda Res & Dev A method and apparatus for producing inorganic fullerene-like nanoparticles
JP2003265962A (ja) * 2002-03-18 2003-09-24 Nittetsu Mining Co Ltd 光触媒およびその製造方法
JP4357801B2 (ja) * 2002-06-25 2009-11-04 日鉄鉱業株式会社 高活性光触媒およびその製造方法
EP1394115B1 (de) 2002-08-24 2009-10-21 Haldor Topsoe A/S Rheniumsulfid Nanoröhrenmaterial und Verfahren zur Herstellung
US7708974B2 (en) * 2002-12-10 2010-05-04 Ppg Industries Ohio, Inc. Tungsten comprising nanomaterials and related nanotechnology
JP4125638B2 (ja) * 2003-06-02 2008-07-30 独立行政法人科学技術振興機構 Ｖ族遷移金属ダイカルコゲナイド結晶からなるナノファイバー又はナノチューブ並びにその製造方法
FR2863265B1 (fr) 2003-12-04 2006-12-08 Centre Nat Rech Scient Procede de synthese de nanoparticules de chalcogenures ayant une structure lamellaire
US7208094B2 (en) * 2003-12-17 2007-04-24 Hewlett-Packard Development Company, L.P. Methods of bridging lateral nanowires and device using same
JP4418300B2 (ja) * 2004-05-25 2010-02-17 株式会社日立製作所 記録媒体作製方法とこれを用いた記録媒体及び情報記録再生装置
CN1328157C (zh) * 2006-03-02 2007-07-25 浙江大学 一种制备非层状硫化物纳米管的方法
SI22445A (sl) 2007-02-26 2008-08-31 Institut "Jožef Stefan" Postopek za sintezo nitkastega volframovega oksida w5o14
CN101641292B (zh) * 2007-03-23 2012-10-17 株式会社东芝 生产用于光催化剂的三氧化钨粉末的方法，用于光催化剂的三氧化钨粉末，及光催化剂产品
EP2132142B1 (de) * 2007-03-30 2015-08-05 Institut "Jozef Stefan" Verfahren zur synthese von nanoröhren und fulleren-ähnlichen nanostrukturen aus übergangsmetallen und dichalcogeniden, quasi eindimensionalen strukturen aus übergangsmetallen und oxiden aus übergangsmetallen
US8329138B2 (en) 2007-09-10 2012-12-11 Yeda Research And Development Company Ltd. Fullerene-like nanostructures, their use and process for their production
DE102008034452B4 (de) * 2008-07-24 2010-09-09 Johannes Gutenberg-Universität Mainz Verfahren zur Herstellung von Nanostrukturen aus Metalldisulfiden, danach hergestellte Nanostrukturen und ihre Verwendung
RU2506284C2 (ru) 2009-01-20 2014-02-10 Ппг Индастриз Огайо, Инк. Прозрачные, бесцветные, поглощающие инфракрасное излучение композиции, содержащие наночастицы нестехиометрического оксида вольфрама
US7955588B2 (en) * 2009-05-26 2011-06-07 Conocophillips Company Metal sulfide catalysts and methods of making same
US9255853B2 (en) * 2012-05-04 2016-02-09 William Marsh Rice University Non-contact strain sensing of objects by use of single-walled carbon nanotubes
EP2958979A4 (de) 2013-02-19 2016-10-26 Nanotech Ind Solutions Inc Anorganische fullerenartige und röhrenartige teilchen in flüssigkeiten und schmiermitteln sowie anwendungen für unterirdische bohrungen
US9446965B2 (en) 2013-02-19 2016-09-20 Nanotech Industrial Solutions, Inc. Applications for inorganic fullerene-like particles
CN105378982A (zh) 2013-06-18 2016-03-02 耶达研究及发展有限公司 作为用于钠/镁离子电池的主体电极材料的类富勒烯纳米粒子和无机纳米管
US9896340B2 (en) * 2013-07-18 2018-02-20 William Marsh Rice University Rebar hybrid materials and methods of making the same
US11158502B2 (en) 2014-09-25 2021-10-26 Purdue Research Foundation Methods of forming nano-scale and micro-scale structured materials and materials formed thereby
TWI532892B (zh) 2015-02-16 2016-05-11 炬力奈米科技有限公司 二維層狀硫族化合物的合成方法及製程設備
US9840764B2 (en) * 2015-09-30 2017-12-12 National Tsing Hua University Method of fabricating transition metal dichalcogenide
WO2017136660A1 (en) * 2016-02-04 2017-08-10 Nanotech Industrial Solutions, Inc. Nanolog and nanoparticles and method of formation
IL249804A0 (en) * 2016-12-27 2017-04-02 Yeda Res & Dev Electromechanical devices are based on metal chalcogenide nanotubes
CN111372894A (zh) * 2017-11-21 2020-07-03 住友金属矿山株式会社 三氧化钨
CA3089149C (en) 2018-01-23 2024-02-27 Evonik Operations Gmbh Polymeric-inorganic nanoparticle compositions, manufacturing process thereof and their use as lubricant additives
WO2019145287A1 (en) 2018-01-23 2019-08-01 Evonik Oil Additives Gmbh Polymeric-inorganic nanoparticle compositions, manufacturing process thereof and their use as lubricant additives
KR102587269B1 (ko) 2018-01-23 2023-10-11 에보닉 오퍼레이션스 게엠베하 중합체성-무기 나노입자 조성물, 이의 제조 방법 및 윤활제 첨가제로서의 이들의 용도
CN109201084B (zh) * 2018-11-06 2021-03-19 中国科学院东北地理与农业生态研究所 一种三氧化钨@二硫化钼中空管复合催化剂的制备方法及其应用
CN113666341A (zh) * 2021-08-24 2021-11-19 昆明理工大学 一种硫属化合物管状材料的制备方法

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IL118378A0 (en) 1996-05-22 1996-09-12 Yeda Res & Dev Method and apparatus for preparing inorganic fullerene-like nanoparticles of transition metal chalcogenides having predetermined size and shape
IL119719A0 (en) * 1996-11-29 1997-02-18 Yeda Res & Dev Inorganic fullerene-like structures of metal chalcogenides
US6346189B1 (en) * 1998-08-14 2002-02-12 The Board Of Trustees Of The Leland Stanford Junior University Carbon nanotube structures made using catalyst islands
US6146227A (en) * 1998-09-28 2000-11-14 Xidex Corporation Method for manufacturing carbon nanotubes as functional elements of MEMS devices
AU2001245786A1 (en) * 2000-03-17 2001-10-03 Hyperion Catalysis International Inc. Carbon nanotubes in fuels and lubricants
US7276283B2 (en) * 2004-03-24 2007-10-02 Wisconsin Alumni Research Foundation Plasma-enhanced functionalization of carbon-containing substrates

Also Published As

Publication number Publication date
WO2000066485A1 (en) 2000-11-09
EP1177153B1 (de) 2007-10-03
US20060071165A1 (en) 2006-04-06
IL129718A0 (en) 2000-02-29
US20040089410A1 (en) 2004-05-13
ES2293897T3 (es) 2008-04-01
DE60036613T2 (de) 2008-07-10
ATE374729T1 (de) 2007-10-15
US6841142B1 (en) 2005-01-11
EP1177153A1 (de) 2002-02-06

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