DE60002285D1 - Verfahren zur Herstellung von zeolithischen Katalysatoren - Google Patents

Verfahren zur Herstellung von zeolithischen Katalysatoren

Info

Publication number
DE60002285D1
DE60002285D1 DE60002285T DE60002285T DE60002285D1 DE 60002285 D1 DE60002285 D1 DE 60002285D1 DE 60002285 T DE60002285 T DE 60002285T DE 60002285 T DE60002285 T DE 60002285T DE 60002285 D1 DE60002285 D1 DE 60002285D1
Authority
DE
Germany
Prior art keywords
preparation
zeolitic catalysts
zeolite
oligomeric silica
tetra
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60002285T
Other languages
English (en)
Other versions
DE60002285T2 (de
Inventor
Giuseppe Botti
Angela Carati
Leonardo Dalloro
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Eni Tecnologie SpA
Versalis SpA
Original Assignee
Eni Tecnologie SpA
Polimeri Europa SpA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eni Tecnologie SpA, Polimeri Europa SpA filed Critical Eni Tecnologie SpA
Publication of DE60002285D1 publication Critical patent/DE60002285D1/de
Application granted granted Critical
Publication of DE60002285T2 publication Critical patent/DE60002285T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/51—Spheres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0072—Preparation of particles, e.g. dispersion of droplets in an oil bath
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0219—Coating the coating containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/10—Preparation of carboxylic acid amides from compounds not provided for in groups C07C231/02 - C07C231/08

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Catalysts (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
DE60002285T 1999-12-03 2000-11-28 Verfahren zur Herstellung von zeolithischen Katalysatoren Expired - Lifetime DE60002285T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ITMI992538 1999-12-03
IT1999MI002538A IT1314263B1 (it) 1999-12-03 1999-12-03 Processo per la preparazione di catalizzatori zeolitici.

Publications (2)

Publication Number Publication Date
DE60002285D1 true DE60002285D1 (de) 2003-05-28
DE60002285T2 DE60002285T2 (de) 2004-04-01

Family

ID=11384072

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60002285T Expired - Lifetime DE60002285T2 (de) 1999-12-03 2000-11-28 Verfahren zur Herstellung von zeolithischen Katalysatoren

Country Status (11)

Country Link
US (1) US6734323B2 (de)
EP (1) EP1106576B1 (de)
JP (1) JP4969722B2 (de)
KR (1) KR100373898B1 (de)
CN (1) CN1150061C (de)
AT (1) ATE238237T1 (de)
DE (1) DE60002285T2 (de)
DK (1) DK1106576T3 (de)
IT (1) IT1314263B1 (de)
SG (1) SG93913A1 (de)
TW (1) TW548135B (de)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1295267B1 (it) 1997-10-03 1999-05-04 Enichem Spa Processo per preparare zeoliti legate
DE19939416A1 (de) * 1999-08-20 2001-02-22 Basf Ag Verfahren zur Herstellung eines kristallinen, zeolithischen Feststoffs
ATE356102T1 (de) 2001-07-02 2007-03-15 Exxonmobil Chem Patents Inc Inhibierung der katalysatorverkokung bei der herstellung eines olefins
ITMI20012470A1 (it) 2001-11-23 2003-05-23 Enichem Spa Procediemnto per la preparazione di vitalizzatori zeolitici di tipo mfi
US6872680B2 (en) 2002-03-20 2005-03-29 Exxonmobil Chemical Patents Inc. Molecular sieve catalyst composition, its making and use in conversion processes
US7271123B2 (en) 2002-03-20 2007-09-18 Exxonmobil Chemical Patents Inc. Molecular sieve catalyst composition, its making and use in conversion process
JP4025228B2 (ja) * 2003-03-28 2007-12-19 カウンスィル オブ サイエンティフィック アンド インダストリアル リサーチ 空気のサイズ／形態的選択分離用モレキュラーシーブ吸着剤の調製法
FR2872152B1 (fr) * 2004-06-24 2006-08-11 Inst Francais Du Petrole Materiau a porosite hierarchisee comprenant du silicium
CN101121148B (zh) * 2006-08-08 2010-05-12 中国科学院大连化学物理研究所 一种含分子筛的流化反应催化剂直接成型方法
FR2920758B1 (fr) * 2007-09-07 2009-11-13 Inst Francais Du Petrole Materiau cristallise a porosite hierarchisee et comprenant du silicium
KR100925851B1 (ko) * 2007-11-14 2009-11-06 한국화학연구원 높은 실리카/알루미늄 비를 갖는 제올라이트의 제조방법
ITMI20072342A1 (it) * 2007-12-14 2009-06-15 Polimeri Europa Spa Processo per preparare zeoliti ts-1
JP2012066977A (ja) * 2010-09-27 2012-04-05 Sumitomo Chemical Co Ltd ゼオライトの製造方法及びε−カプロラクタムの製造方法
CN102145300B (zh) * 2011-03-08 2012-11-28 华东师范大学 一种微球ts-1催化剂及其制备方法
TWI480100B (zh) * 2011-04-27 2015-04-11 China Petrochemical Dev Corp Taipei Taiwan Titanium-silicon molecular sieve and its preparation method and method for producing cyclohexanone oxime using the molecular sieve
US8772476B2 (en) 2011-10-28 2014-07-08 Honeywell International Inc. Gas and liquid phase catalytic Beckmann rearrangement of oximes to produce lactams
CN103143390A (zh) * 2013-03-15 2013-06-12 华东师范大学 一种微球钛硅分子筛催化剂的改性方法
CN104098106B (zh) * 2014-07-08 2016-05-04 黄河三角洲京博化工研究院有限公司 一种一步合成中空式多级孔Fe-Silicalite-1的方法
US10995008B2 (en) * 2016-03-30 2021-05-04 Basf Se Process for the flash calcination of a zeolitic material
CN108658087B (zh) * 2017-03-31 2021-03-12 中国石油化工股份有限公司 一种多级孔道ts-1沸石材料及其制备方法
CN107321301A (zh) * 2017-06-22 2017-11-07 北京化学试剂研究所 一种新型分子筛及其制备方法与应用
CN109046446A (zh) * 2018-08-30 2018-12-21 河北科技大学 一种金属氧化物/hts-1钛硅分子筛催化剂及其制备方法和应用
CN109731608B (zh) * 2019-01-30 2021-05-25 中国科学院过程工程研究所 一种封装金属纳米颗粒的无钠硅铝分子筛的双功能催化剂及其制备方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4452909A (en) * 1982-09-13 1984-06-05 E. I. Du Pont De Nemours And Company Process for coating crystalline silica polymorphs
JPS60218307A (ja) * 1984-04-13 1985-11-01 Nippon Chem Ind Co Ltd:The 化粧料
IT1213504B (it) * 1986-10-22 1989-12-20 Eniricerche Spa Zeoliti legate e procedimenye per la loro prosuzione.
IT1219692B (it) * 1988-05-06 1990-05-24 Eniricerche Spa Gel di silice e allumina cataliticamente attivo e procedimento per la sua preparazione
JP3254752B2 (ja) * 1991-11-27 2002-02-12 住友化学工業株式会社 ε−カプロラクタムの製法
DK0791558T3 (da) * 1996-02-22 2002-03-18 Enichem Spa Silica/zeolit-kompositmaterialer på sfærisk form og fremgangsmåde til deres fremstilling
IT1284007B1 (it) * 1996-06-13 1998-05-08 Eniricerche Spa Procedimento per la preparazione di un materiale micro-meso poroso ad alta area superficiale con distribuzione controllata della
IT1283773B1 (it) * 1996-08-07 1998-04-30 Enichem Spa Procedimento per la perparazione di ammidi da ossime
IT1295267B1 (it) * 1997-10-03 1999-05-04 Enichem Spa Processo per preparare zeoliti legate

Also Published As

Publication number Publication date
JP2001212463A (ja) 2001-08-07
TW548135B (en) 2003-08-21
EP1106576B1 (de) 2003-04-23
KR100373898B1 (ko) 2003-02-26
DK1106576T3 (da) 2003-06-30
CN1150061C (zh) 2004-05-19
US6734323B2 (en) 2004-05-11
ATE238237T1 (de) 2003-05-15
ITMI992538A1 (it) 2001-06-03
CN1316301A (zh) 2001-10-10
ITMI992538A0 (it) 1999-12-03
US20010002991A1 (en) 2001-06-07
JP4969722B2 (ja) 2012-07-04
IT1314263B1 (it) 2002-12-06
SG93913A1 (en) 2003-01-21
DE60002285T2 (de) 2004-04-01
KR20010062071A (ko) 2001-07-07
EP1106576A1 (de) 2001-06-13

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