DE50212773D1 - Verfahren zur herstellung builderhaltiger tensidgranulate - Google Patents
Verfahren zur herstellung builderhaltiger tensidgranulateInfo
- Publication number
- DE50212773D1 DE50212773D1 DE50212773T DE50212773T DE50212773D1 DE 50212773 D1 DE50212773 D1 DE 50212773D1 DE 50212773 T DE50212773 T DE 50212773T DE 50212773 T DE50212773 T DE 50212773T DE 50212773 D1 DE50212773 D1 DE 50212773D1
- Authority
- DE
- Germany
- Prior art keywords
- acid
- builder
- acids
- producing
- surfactant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000008187 granular material Substances 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 239000002253 acid Substances 0.000 abstract 5
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 abstract 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 abstract 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 abstract 3
- RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 abstract 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 abstract 2
- 150000007513 acids Chemical class 0.000 abstract 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000004094 surface-active agent Substances 0.000 abstract 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 abstract 2
- RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 abstract 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 abstract 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 abstract 1
- DBVJJBKOTRCVKF-UHFFFAOYSA-N Etidronic acid Chemical compound OP(=O)(O)C(O)(C)P(O)(O)=O DBVJJBKOTRCVKF-UHFFFAOYSA-N 0.000 abstract 1
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 abstract 1
- 229920002845 Poly(methacrylic acid) Polymers 0.000 abstract 1
- 229920000805 Polyaspartic acid Polymers 0.000 abstract 1
- 229920002125 Sokalan® Polymers 0.000 abstract 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 abstract 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 abstract 1
- YDONNITUKPKTIG-UHFFFAOYSA-N [Nitrilotris(methylene)]trisphosphonic acid Chemical compound OP(O)(=O)CN(CP(O)(O)=O)CP(O)(O)=O YDONNITUKPKTIG-UHFFFAOYSA-N 0.000 abstract 1
- 239000001361 adipic acid Substances 0.000 abstract 1
- 235000011037 adipic acid Nutrition 0.000 abstract 1
- 239000003945 anionic surfactant Substances 0.000 abstract 1
- 235000003704 aspartic acid Nutrition 0.000 abstract 1
- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 abstract 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 229920001577 copolymer Polymers 0.000 abstract 1
- 229960004585 etidronic acid Drugs 0.000 abstract 1
- 239000001530 fumaric acid Substances 0.000 abstract 1
- 235000011087 fumaric acid Nutrition 0.000 abstract 1
- 239000000174 gluconic acid Substances 0.000 abstract 1
- 235000012208 gluconic acid Nutrition 0.000 abstract 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 abstract 1
- 239000011976 maleic acid Substances 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical compound OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 abstract 1
- 235000006408 oxalic acid Nutrition 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000011975 tartaric acid Substances 0.000 abstract 1
- 235000002906 tartaric acid Nutrition 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10163603A DE10163603B4 (de) | 2001-12-21 | 2001-12-21 | Verfahren zur Herstellung builderhaltiger Tensidgranulate |
PCT/EP2002/014124 WO2003054131A1 (de) | 2001-12-21 | 2002-12-12 | Verfahren zur herstellung builderhaltiger tensidgranulate |
Publications (1)
Publication Number | Publication Date |
---|---|
DE50212773D1 true DE50212773D1 (de) | 2008-10-23 |
Family
ID=7710608
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE10163603A Expired - Fee Related DE10163603B4 (de) | 2001-12-21 | 2001-12-21 | Verfahren zur Herstellung builderhaltiger Tensidgranulate |
DE50212773T Expired - Lifetime DE50212773D1 (de) | 2001-12-21 | 2002-12-12 | Verfahren zur herstellung builderhaltiger tensidgranulate |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE10163603A Expired - Fee Related DE10163603B4 (de) | 2001-12-21 | 2001-12-21 | Verfahren zur Herstellung builderhaltiger Tensidgranulate |
Country Status (8)
Country | Link |
---|---|
US (1) | US7186677B2 (de) |
EP (1) | EP1456340B9 (de) |
JP (1) | JP4416508B2 (de) |
AT (1) | ATE408000T1 (de) |
AU (1) | AU2002361061A1 (de) |
DE (2) | DE10163603B4 (de) |
ES (1) | ES2309226T3 (de) |
WO (1) | WO2003054131A1 (de) |
Families Citing this family (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10258011A1 (de) * | 2002-12-12 | 2004-07-08 | Henkel Kgaa | Trockenneutralisationsverfahren |
DE102004011087A1 (de) * | 2004-03-06 | 2005-09-22 | Henkel Kgaa | Partikel umfassend diskrete, feinpartikuläre Tensidpartikel |
KR101392380B1 (ko) * | 2007-02-21 | 2014-05-07 | 주식회사 엘지생활건강 | 산성형태의 수용성 고분자를 함유하는 분말세제 입자 및그의 제조방법 |
US7763576B2 (en) * | 2008-01-04 | 2010-07-27 | Ecolab Inc. | Solidification matrix using a polycarboxylic acid polymer |
US8338352B2 (en) * | 2007-05-07 | 2012-12-25 | Ecolab Usa Inc. | Solidification matrix |
US8759269B2 (en) * | 2007-07-02 | 2014-06-24 | Ecolab Usa Inc. | Solidification matrix including a salt of a straight chain saturated mono-, di-, and tri- carboxylic acid |
US7759300B2 (en) * | 2007-07-02 | 2010-07-20 | Ecolab Inc. | Solidification matrix including a salt of a straight chain saturated mono-, di-, or tri- carboxylic acid |
GB0718944D0 (en) * | 2007-09-28 | 2007-11-07 | Reckitt Benckiser Nv | Detergent composition |
US8772221B2 (en) | 2008-01-04 | 2014-07-08 | Ecolab Usa Inc. | Solidification matrices using phosphonocarboxylic acid copolymers and phosphonopolyacrylic acid homopolymers |
US8198228B2 (en) * | 2008-01-04 | 2012-06-12 | Ecolab Usa Inc. | Solidification matrix using an aminocarboxylate |
US8138138B2 (en) * | 2008-01-04 | 2012-03-20 | Ecolab Usa Inc. | Solidification matrix using a polycarboxylic acid polymer |
EP2138568A1 (de) * | 2008-06-25 | 2009-12-30 | The Procter and Gamble Company | Neutralisierungsverfahren zur Herstellung einer Waschmittelzusammensetzung mit reinigungstensidhaltigem und polymerischem Material |
EP2350249B1 (de) * | 2008-10-31 | 2014-04-16 | Henkel AG & Co. KGaA | Maschinelles geschirrspülmittel |
DE102008063801A1 (de) * | 2008-12-19 | 2010-06-24 | Henkel Ag & Co. Kgaa | Maschinelles Geschirrspülmittel |
US20100197545A1 (en) * | 2009-01-30 | 2010-08-05 | Ecolab USA | High alkaline detergent composition with enhanced scale control |
DE102009027164A1 (de) * | 2009-06-24 | 2010-12-30 | Henkel Ag & Co. Kgaa | Maschinelles Geschirrspülmittel |
MX342487B (es) * | 2009-07-09 | 2016-09-29 | The Procter & Gamble Company * | Composicion detergente solida para tratamiento de tela con bajo contenido de aditivo. ligeramente alcalina, que comprende acido ftalimido peroxicaproico. |
US8530403B2 (en) * | 2009-11-20 | 2013-09-10 | Ecolab Usa Inc. | Solidification matrix using a maleic-containing terpolymer binding agent |
US20110124547A1 (en) * | 2009-11-23 | 2011-05-26 | Ecolab Inc. | Solidification matrix using a sulfonated/carboxylated polymer binding agent |
US8754026B2 (en) * | 2010-09-27 | 2014-06-17 | Basf Se | Process for producing granules comprising one or more complexing agent salts |
JP2012255145A (ja) * | 2011-05-18 | 2012-12-27 | Kao Corp | 洗剤粒子群の製造方法 |
AU2014346509B2 (en) * | 2013-11-11 | 2017-02-02 | Ecolab Usa Inc. | High alkaline warewash detergent with enhanced scale control and soil dispersion |
USD762486S1 (en) | 2015-02-18 | 2016-08-02 | Henkel Ag & Co. Kgaa | Solid state detergent in a transparent container |
USD784819S1 (en) | 2015-02-18 | 2017-04-25 | Henkel Us Iv Corporation | Container for a solid state detergent |
US9512388B2 (en) | 2015-02-18 | 2016-12-06 | Henkel Ag & Co. Kgaa | Solid state detergent in a transparent container |
WO2019173688A1 (en) * | 2018-03-08 | 2019-09-12 | Ecolab Usa Inc. | Solid enzymatic detergent compositions and methods of use and manufacture |
CN109517673B (zh) * | 2018-11-16 | 2021-03-19 | 太原理工大学 | 一种加酶无磷衣物用粉末洗涤剂及其制备方法 |
Family Cites Families (30)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3425948A (en) * | 1966-01-03 | 1969-02-04 | Wyandotte Chemicals Corp | Composition and process for light-weight surfactant products |
CA1276852C (en) | 1985-06-21 | 1990-11-27 | Francis John Leng | Liquid detergent composition |
GB8625104D0 (en) | 1986-10-20 | 1986-11-26 | Unilever Plc | Detergent compositions |
US5108642A (en) * | 1986-10-30 | 1992-04-28 | Colgate-Palmolive Company | Solid detergent cleaning composition, and method of manufacturing |
CA2017922C (en) | 1989-06-09 | 1995-07-11 | Frank Joseph Mueller | Formation of discrete, high active detergent granules using a continuous neutralization system |
GB9001285D0 (en) | 1990-01-19 | 1990-03-21 | Unilever Plc | Detergent compositions and process for preparing them |
US5066425A (en) * | 1990-07-16 | 1991-11-19 | The Procter & Gamble Company | Formation of high active detergent particles |
CA2027518A1 (en) * | 1990-10-03 | 1992-04-04 | Richard L. Tadsen | Process for preparing high density detergent compositions containing particulate ph sensitive surfactant |
GB9107092D0 (en) | 1991-04-04 | 1991-05-22 | Unilever Plc | Process for preparing detergent compositions |
DE69221357T2 (de) | 1991-04-12 | 1998-03-12 | Procter & Gamble | Chemische Strukturierung von oberflächenaktiven Pasten zwecks Herstellung hochwirksamer Tensidgranulate |
GB9120657D0 (en) * | 1991-09-27 | 1991-11-06 | Unilever Plc | Detergent powders and process for preparing them |
EP0555622B1 (de) * | 1992-02-14 | 1997-07-09 | The Procter & Gamble Company | Verfahren zur Herstellung von Detergenskörnchen durch Neutralisation von Sulfonsäuren |
DE4216629A1 (de) * | 1992-05-20 | 1993-11-25 | Henkel Kgaa | Verfahren zur Herstellung aniontensidhaltiger Wasch- und Reinigungsmittel |
DE4216774A1 (de) | 1992-05-21 | 1993-11-25 | Henkel Kgaa | Verfahren zur kontinuierlichen Herstellung eines granularen Wasch und/oder Reinigungsmittels |
ZA936554B (en) * | 1992-09-08 | 1995-03-06 | Unilever Plc | Detergent composition and process for its production. |
DE4232874A1 (de) * | 1992-09-30 | 1994-03-31 | Henkel Kgaa | Verfahren zur Herstellung von Tensidgranulaten |
DE4314885A1 (de) | 1993-05-05 | 1994-11-10 | Sued Chemie Ag | Verfahren zur Neutralisation der Säureform von anionischen Tensiden, danach erhaltene Agglomerate und Waschmittel |
ATE197811T1 (de) | 1994-04-20 | 2000-12-15 | Procter & Gamble | Verfahren zur herstellung von rieselfähigen waschmittelgranulaten |
DE4425968A1 (de) | 1994-07-25 | 1996-02-01 | Henkel Kgaa | Verfahren zur Herstellung von Tensidgranulaten |
JPH09241698A (ja) * | 1996-03-13 | 1997-09-16 | Lion Corp | 高嵩密度粒状洗剤組成物の製造方法 |
TW397862B (en) * | 1996-09-06 | 2000-07-11 | Kao Corp | Detergent granules and method for producing the same, and high-bulk density detergent composition |
CN1242800A (zh) | 1996-11-06 | 2000-01-26 | 普罗格特-甘布尔公司 | 中和法制造附聚洗涤剂颗粒 |
GB9713748D0 (en) * | 1997-06-27 | 1997-09-03 | Unilever Plc | Production of detergent granulates |
DE19735788A1 (de) * | 1997-08-18 | 1999-02-25 | Henkel Kgaa | Verfahren zur Herstellung hochtensidhaltiger Granulate |
DE19844522A1 (de) * | 1998-09-29 | 2000-03-30 | Henkel Kgaa | Granulationsverfahren |
DE19844523A1 (de) * | 1998-09-29 | 2000-03-30 | Henkel Kgaa | Granulationsverfahren |
DE19855380A1 (de) * | 1998-12-01 | 2000-06-08 | Henkel Kgaa | Granulationsverfahren |
GB2344597A (en) * | 1998-12-08 | 2000-06-14 | Procter & Gamble | Effervescence components |
DE19858859A1 (de) * | 1998-12-19 | 2000-06-21 | Henkel Kgaa | Verfahren zur Herstellung wasch- oder reinigungsaktiver Granulate |
BR0016209B1 (pt) * | 1999-12-08 | 2011-12-27 | processo de preparaÇço de uma composiÇço detergente em barra. |
-
2001
- 2001-12-21 DE DE10163603A patent/DE10163603B4/de not_active Expired - Fee Related
-
2002
- 2002-12-12 DE DE50212773T patent/DE50212773D1/de not_active Expired - Lifetime
- 2002-12-12 AU AU2002361061A patent/AU2002361061A1/en not_active Abandoned
- 2002-12-12 ES ES02795170T patent/ES2309226T3/es not_active Expired - Lifetime
- 2002-12-12 WO PCT/EP2002/014124 patent/WO2003054131A1/de active IP Right Grant
- 2002-12-12 EP EP02795170A patent/EP1456340B9/de not_active Expired - Lifetime
- 2002-12-12 JP JP2003554838A patent/JP4416508B2/ja not_active Expired - Fee Related
- 2002-12-12 AT AT02795170T patent/ATE408000T1/de not_active IP Right Cessation
-
2004
- 2004-06-21 US US10/872,813 patent/US7186677B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
ES2309226T3 (es) | 2008-12-16 |
EP1456340B1 (de) | 2008-09-10 |
US20050020469A1 (en) | 2005-01-27 |
DE10163603B4 (de) | 2006-05-04 |
AU2002361061A1 (en) | 2003-07-09 |
JP2005534721A (ja) | 2005-11-17 |
WO2003054131A1 (de) | 2003-07-03 |
EP1456340A1 (de) | 2004-09-15 |
DE10163603A1 (de) | 2003-07-10 |
JP4416508B2 (ja) | 2010-02-17 |
ATE408000T1 (de) | 2008-09-15 |
EP1456340B9 (de) | 2009-03-04 |
US7186677B2 (en) | 2007-03-06 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition |