DE3615541C2 - - Google Patents
Info
- Publication number
- DE3615541C2 DE3615541C2 DE3615541A DE3615541A DE3615541C2 DE 3615541 C2 DE3615541 C2 DE 3615541C2 DE 3615541 A DE3615541 A DE 3615541A DE 3615541 A DE3615541 A DE 3615541A DE 3615541 C2 DE3615541 C2 DE 3615541C2
- Authority
- DE
- Germany
- Prior art keywords
- liquid
- retaining elements
- ball
- container
- space
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007788 liquid Substances 0.000 claims description 75
- 239000000126 substance Substances 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 20
- 239000013078 crystal Substances 0.000 claims description 16
- 238000002425 crystallisation Methods 0.000 claims description 14
- 230000008025 crystallization Effects 0.000 claims description 13
- 239000002904 solvent Substances 0.000 claims description 10
- 238000007667 floating Methods 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 230000014759 maintenance of location Effects 0.000 claims description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 6
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 6
- 235000011130 ammonium sulphate Nutrition 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 238000002474 experimental method Methods 0.000 description 5
- 229930195733 hydrocarbon Natural products 0.000 description 5
- 150000002430 hydrocarbons Chemical class 0.000 description 5
- 102000004169 proteins and genes Human genes 0.000 description 5
- 108090000623 proteins and genes Proteins 0.000 description 5
- 239000004215 Carbon black (E152) Substances 0.000 description 4
- 239000012808 vapor phase Substances 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 3
- 239000007791 liquid phase Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000007847 structural defect Effects 0.000 description 3
- 230000001133 acceleration Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000008030 elimination Effects 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- 230000002209 hydrophobic effect Effects 0.000 description 2
- 230000005486 microgravity Effects 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 229910020366 ClO 4 Inorganic materials 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 102000016943 Muramidase Human genes 0.000 description 1
- 108010014251 Muramidase Proteins 0.000 description 1
- 108010062010 N-Acetylmuramoyl-L-alanine Amidase Proteins 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 102000005936 beta-Galactosidase Human genes 0.000 description 1
- 108010005774 beta-Galactosidase Proteins 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229940088598 enzyme Drugs 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 229960000274 lysozyme Drugs 0.000 description 1
- 235000010335 lysozyme Nutrition 0.000 description 1
- 239000004325 lysozyme Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 102000039446 nucleic acids Human genes 0.000 description 1
- 108020004707 nucleic acids Proteins 0.000 description 1
- 150000007523 nucleic acids Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 239000012460 protein solution Substances 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 238000005185 salting out Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B30/00—Production of single crystals or homogeneous polycrystalline material with defined structure characterised by the action of electric or magnetic fields, wave energy or other specific physical conditions
- C30B30/08—Production of single crystals or homogeneous polycrystalline material with defined structure characterised by the action of electric or magnetic fields, wave energy or other specific physical conditions in conditions of zero-gravity or low gravity
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
- Y10S117/901—Levitation, reduced gravity, microgravity, space
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
- Y10T117/10—Apparatus
- Y10T117/1024—Apparatus for crystallization from liquid or supercritical state
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Peptides Or Proteins (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863615541 DE3615541A1 (de) | 1986-05-07 | 1986-05-07 | Verfahren und vorrichtung zur auskristallisation einer in einer fluessigkeit geloesten substanz im zustand der schwerelosigkeit |
| CA000536474A CA1329359C (en) | 1986-05-07 | 1987-05-06 | Process and an apparatus for crystallizing a substance dissolved in a liquid in zero gravity |
| DE8787106664T DE3772835D1 (de) | 1986-05-07 | 1987-05-07 | Verfahren und vorrichtung zur auskristallisation einer in einer fluessigkeit geloesten substanz im zustand der schwerelosigkeit. |
| JP62109934A JPS62282601A (ja) | 1986-05-07 | 1987-05-07 | 無重力の状態で液体中に溶けている物質を晶出させるための方法とその装置 |
| EP87106664A EP0244867B1 (de) | 1986-05-07 | 1987-05-07 | Verfahren und Vorrichtung zur Auskristallisation einer in einer Flüssigkeit gelösten Substanz im Zustand der Schwerelosigkeit |
| US07/248,234 US4960572A (en) | 1986-05-07 | 1988-09-19 | Method and apparatus for crystallizing substances dissolved in a liquid at zero-gravity |
| US07/553,961 US5139605A (en) | 1986-05-07 | 1990-07-17 | Method and apparatus for crystallizing substances dissolved in a liquid at zero-gravity |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863615541 DE3615541A1 (de) | 1986-05-07 | 1986-05-07 | Verfahren und vorrichtung zur auskristallisation einer in einer fluessigkeit geloesten substanz im zustand der schwerelosigkeit |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3615541A1 DE3615541A1 (de) | 1987-11-12 |
| DE3615541C2 true DE3615541C2 (enExample) | 1988-11-17 |
Family
ID=6300394
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19863615541 Granted DE3615541A1 (de) | 1986-05-07 | 1986-05-07 | Verfahren und vorrichtung zur auskristallisation einer in einer fluessigkeit geloesten substanz im zustand der schwerelosigkeit |
| DE8787106664T Expired - Fee Related DE3772835D1 (de) | 1986-05-07 | 1987-05-07 | Verfahren und vorrichtung zur auskristallisation einer in einer fluessigkeit geloesten substanz im zustand der schwerelosigkeit. |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8787106664T Expired - Fee Related DE3772835D1 (de) | 1986-05-07 | 1987-05-07 | Verfahren und vorrichtung zur auskristallisation einer in einer fluessigkeit geloesten substanz im zustand der schwerelosigkeit. |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4960572A (enExample) |
| EP (1) | EP0244867B1 (enExample) |
| JP (1) | JPS62282601A (enExample) |
| CA (1) | CA1329359C (enExample) |
| DE (2) | DE3615541A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007020671A1 (de) | 2007-05-01 | 2008-11-06 | Justus-Liebig-Universität Giessen | Verfahren und Vorrichtung zum kontaktfreien Materialwachstum in einer strömenden Lösung (FLow suspended solution growth (FSSG)) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3806635A1 (de) * | 1988-03-02 | 1989-09-14 | Battelle Institut E V | Verfahren zum zuechten eines einkristalls |
| DE3806634A1 (de) * | 1988-03-02 | 1989-09-14 | Battelle Institut E V | Verfahren zum zuechten eines einkristalls |
| DE3941099A1 (de) * | 1989-12-13 | 1991-06-20 | Dornier Gmbh | Handhabung von fluessigkeiten unter schwerelosigkeit |
| DE4007943C1 (en) * | 1990-03-13 | 1991-03-07 | Erno Raumfahrttechnik Gmbh, 2800 Bremen, De | Appts. for weightless crystallisation - has sprung piston spray ejector forming droplet at tip |
| US5427335A (en) * | 1992-07-13 | 1995-06-27 | The University Of Tennessee Research Corporation | Method for producing extreme microgravity in extended volumes |
| JPH07275690A (ja) * | 1994-04-05 | 1995-10-24 | Mitsubishi Electric Corp | 浮遊装置 |
| JPH0834699A (ja) * | 1994-07-25 | 1996-02-06 | Fujitsu Ltd | 生体高分子結晶化装置 |
| US5643540A (en) * | 1995-02-27 | 1997-07-01 | The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration | Protein crystal growth apparatus for microgravitiy |
| US7479859B2 (en) * | 2006-03-08 | 2009-01-20 | Jack Gerber | Apparatus and method for processing material in a magnetic vortex |
| ES2310131B1 (es) | 2007-06-04 | 2009-12-04 | INSTITUTO NACIONAL DE TECNICA AEROESPACIAL "ESTEBAN TERRADAS" | Procedimiento de cristalizacion a partir de solucion. |
| KR102797400B1 (ko) * | 2024-04-26 | 2025-04-21 | 주식회사 스페이스린텍 | 미세 중력 환경에서의 단백질 결정화 장치 및 이를 이용하여 단백질을 결정화하는 방법 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1095208A (en) * | 1912-07-10 | 1914-05-05 | Alfred H Humphrey | Gas-lamp. |
| US1736437A (en) * | 1927-09-22 | 1929-11-19 | Visible Night And Day Street N | Street sign |
| US1746340A (en) * | 1928-04-14 | 1930-02-11 | Miller Co | Dustproof cover for reflectors |
| US1854020A (en) * | 1930-11-24 | 1932-04-12 | Gen Electric | Adjustable support |
| US3425584A (en) * | 1966-10-19 | 1969-02-04 | California Texas Oil Corp | Shipboard mounting liquefied gas tanks |
| US3713560A (en) * | 1971-04-19 | 1973-01-30 | Gen Dynamics Corp | Spaced wall container |
| US4046617A (en) * | 1975-09-05 | 1977-09-06 | Nasa | Method of crystallization |
| DE3024127C2 (de) * | 1980-06-27 | 1983-09-29 | Deutsche Forschungs- und Versuchsanstalt für Luft- und Raumfahrt e.V., 5000 Köln | Vorrichtung zur beschleunigungsfreien Anbringung eines Körpers in einem Raumfahrzeug |
| FR2509637A1 (fr) * | 1981-07-17 | 1983-01-21 | Commissariat Energie Atomique | Procede de sustentation, de positionnement et de moulage sans contact de masses liquides permettant la solidification en forme de materiaux et application de ce procede a la mise en forme de materiaux en microgravite |
| JPH089520B2 (ja) * | 1983-05-25 | 1996-01-31 | 理化学研究所 | 薄膜単結晶の製造方法 |
-
1986
- 1986-05-07 DE DE19863615541 patent/DE3615541A1/de active Granted
-
1987
- 1987-05-06 CA CA000536474A patent/CA1329359C/en not_active Expired - Fee Related
- 1987-05-07 JP JP62109934A patent/JPS62282601A/ja active Granted
- 1987-05-07 DE DE8787106664T patent/DE3772835D1/de not_active Expired - Fee Related
- 1987-05-07 EP EP87106664A patent/EP0244867B1/de not_active Expired - Lifetime
-
1988
- 1988-09-19 US US07/248,234 patent/US4960572A/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007020671A1 (de) | 2007-05-01 | 2008-11-06 | Justus-Liebig-Universität Giessen | Verfahren und Vorrichtung zum kontaktfreien Materialwachstum in einer strömenden Lösung (FLow suspended solution growth (FSSG)) |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3615541A1 (de) | 1987-11-12 |
| CA1329359C (en) | 1994-05-10 |
| EP0244867A2 (de) | 1987-11-11 |
| US4960572A (en) | 1990-10-02 |
| EP0244867B1 (de) | 1991-09-11 |
| DE3772835D1 (de) | 1991-10-17 |
| EP0244867A3 (en) | 1989-07-19 |
| JPH0443880B2 (enExample) | 1992-07-17 |
| JPS62282601A (ja) | 1987-12-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: DEUTSCHE AEROSPACE AG, 8000 MUENCHEN, DE |
|
| 8339 | Ceased/non-payment of the annual fee |