JPS62282601A - 無重力の状態で液体中に溶けている物質を晶出させるための方法とその装置 - Google Patents
無重力の状態で液体中に溶けている物質を晶出させるための方法とその装置Info
- Publication number
- JPS62282601A JPS62282601A JP62109934A JP10993487A JPS62282601A JP S62282601 A JPS62282601 A JP S62282601A JP 62109934 A JP62109934 A JP 62109934A JP 10993487 A JP10993487 A JP 10993487A JP S62282601 A JPS62282601 A JP S62282601A
- Authority
- JP
- Japan
- Prior art keywords
- liquid
- chamber
- chamber area
- crystallization
- sphere
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007788 liquid Substances 0.000 title claims description 86
- 239000000126 substance Substances 0.000 title claims description 26
- 238000000034 method Methods 0.000 title claims description 21
- 238000002425 crystallisation Methods 0.000 claims description 20
- 239000013078 crystal Substances 0.000 claims description 19
- 230000008025 crystallization Effects 0.000 claims description 17
- 239000002904 solvent Substances 0.000 claims description 10
- 230000005484 gravity Effects 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 238000005192 partition Methods 0.000 claims description 4
- 238000011049 filling Methods 0.000 claims description 3
- 238000000638 solvent extraction Methods 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 10
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 6
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 6
- 235000011130 ammonium sulphate Nutrition 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 229930195733 hydrocarbon Natural products 0.000 description 5
- 150000002430 hydrocarbons Chemical class 0.000 description 5
- 239000012071 phase Substances 0.000 description 5
- 102000004169 proteins and genes Human genes 0.000 description 5
- 108090000623 proteins and genes Proteins 0.000 description 5
- 239000000243 solution Substances 0.000 description 4
- 230000001133 acceleration Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 239000012808 vapor phase Substances 0.000 description 3
- 230000002209 hydrophobic effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000005486 microgravity Effects 0.000 description 2
- 239000012460 protein solution Substances 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 235000011148 calcium chloride Nutrition 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 239000011538 cleaning material Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000002178 crystalline material Substances 0.000 description 1
- 238000012866 crystallographic experiment Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229930182830 galactose Natural products 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 102000039446 nucleic acids Human genes 0.000 description 1
- 108020004707 nucleic acids Proteins 0.000 description 1
- 150000007523 nucleic acids Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 230000007847 structural defect Effects 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B30/00—Production of single crystals or homogeneous polycrystalline material with defined structure characterised by the action of electric or magnetic fields, wave energy or other specific physical conditions
- C30B30/08—Production of single crystals or homogeneous polycrystalline material with defined structure characterised by the action of electric or magnetic fields, wave energy or other specific physical conditions in conditions of zero-gravity or low gravity
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
- Y10S117/901—Levitation, reduced gravity, microgravity, space
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
- Y10T117/10—Apparatus
- Y10T117/1024—Apparatus for crystallization from liquid or supercritical state
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Peptides Or Proteins (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863615541 DE3615541A1 (de) | 1986-05-07 | 1986-05-07 | Verfahren und vorrichtung zur auskristallisation einer in einer fluessigkeit geloesten substanz im zustand der schwerelosigkeit |
| DE3615541.1 | 1986-05-07 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62282601A true JPS62282601A (ja) | 1987-12-08 |
| JPH0443880B2 JPH0443880B2 (enExample) | 1992-07-17 |
Family
ID=6300394
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP62109934A Granted JPS62282601A (ja) | 1986-05-07 | 1987-05-07 | 無重力の状態で液体中に溶けている物質を晶出させるための方法とその装置 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4960572A (enExample) |
| EP (1) | EP0244867B1 (enExample) |
| JP (1) | JPS62282601A (enExample) |
| CA (1) | CA1329359C (enExample) |
| DE (2) | DE3615541A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5558837A (en) * | 1994-04-05 | 1996-09-24 | Mitsubishi Denki Kabushiki Kaisha | Droplet floating apparatus |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3806635A1 (de) * | 1988-03-02 | 1989-09-14 | Battelle Institut E V | Verfahren zum zuechten eines einkristalls |
| DE3806634A1 (de) * | 1988-03-02 | 1989-09-14 | Battelle Institut E V | Verfahren zum zuechten eines einkristalls |
| DE3941099A1 (de) * | 1989-12-13 | 1991-06-20 | Dornier Gmbh | Handhabung von fluessigkeiten unter schwerelosigkeit |
| DE4007943C1 (en) * | 1990-03-13 | 1991-03-07 | Erno Raumfahrttechnik Gmbh, 2800 Bremen, De | Appts. for weightless crystallisation - has sprung piston spray ejector forming droplet at tip |
| US5427335A (en) * | 1992-07-13 | 1995-06-27 | The University Of Tennessee Research Corporation | Method for producing extreme microgravity in extended volumes |
| JPH0834699A (ja) * | 1994-07-25 | 1996-02-06 | Fujitsu Ltd | 生体高分子結晶化装置 |
| US5643540A (en) * | 1995-02-27 | 1997-07-01 | The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration | Protein crystal growth apparatus for microgravitiy |
| US7479859B2 (en) * | 2006-03-08 | 2009-01-20 | Jack Gerber | Apparatus and method for processing material in a magnetic vortex |
| DE102007020671A1 (de) | 2007-05-01 | 2008-11-06 | Justus-Liebig-Universität Giessen | Verfahren und Vorrichtung zum kontaktfreien Materialwachstum in einer strömenden Lösung (FLow suspended solution growth (FSSG)) |
| ES2310131B1 (es) | 2007-06-04 | 2009-12-04 | INSTITUTO NACIONAL DE TECNICA AEROESPACIAL "ESTEBAN TERRADAS" | Procedimiento de cristalizacion a partir de solucion. |
| KR102797400B1 (ko) * | 2024-04-26 | 2025-04-21 | 주식회사 스페이스린텍 | 미세 중력 환경에서의 단백질 결정화 장치 및 이를 이용하여 단백질을 결정화하는 방법 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59217692A (ja) * | 1983-05-25 | 1984-12-07 | Rikagaku Kenkyusho | 薄膜単結晶の製造方法 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1095208A (en) * | 1912-07-10 | 1914-05-05 | Alfred H Humphrey | Gas-lamp. |
| US1736437A (en) * | 1927-09-22 | 1929-11-19 | Visible Night And Day Street N | Street sign |
| US1746340A (en) * | 1928-04-14 | 1930-02-11 | Miller Co | Dustproof cover for reflectors |
| US1854020A (en) * | 1930-11-24 | 1932-04-12 | Gen Electric | Adjustable support |
| US3425584A (en) * | 1966-10-19 | 1969-02-04 | California Texas Oil Corp | Shipboard mounting liquefied gas tanks |
| US3713560A (en) * | 1971-04-19 | 1973-01-30 | Gen Dynamics Corp | Spaced wall container |
| US4046617A (en) * | 1975-09-05 | 1977-09-06 | Nasa | Method of crystallization |
| DE3024127C2 (de) * | 1980-06-27 | 1983-09-29 | Deutsche Forschungs- und Versuchsanstalt für Luft- und Raumfahrt e.V., 5000 Köln | Vorrichtung zur beschleunigungsfreien Anbringung eines Körpers in einem Raumfahrzeug |
| FR2509637A1 (fr) * | 1981-07-17 | 1983-01-21 | Commissariat Energie Atomique | Procede de sustentation, de positionnement et de moulage sans contact de masses liquides permettant la solidification en forme de materiaux et application de ce procede a la mise en forme de materiaux en microgravite |
-
1986
- 1986-05-07 DE DE19863615541 patent/DE3615541A1/de active Granted
-
1987
- 1987-05-06 CA CA000536474A patent/CA1329359C/en not_active Expired - Fee Related
- 1987-05-07 JP JP62109934A patent/JPS62282601A/ja active Granted
- 1987-05-07 DE DE8787106664T patent/DE3772835D1/de not_active Expired - Fee Related
- 1987-05-07 EP EP87106664A patent/EP0244867B1/de not_active Expired - Lifetime
-
1988
- 1988-09-19 US US07/248,234 patent/US4960572A/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59217692A (ja) * | 1983-05-25 | 1984-12-07 | Rikagaku Kenkyusho | 薄膜単結晶の製造方法 |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5558837A (en) * | 1994-04-05 | 1996-09-24 | Mitsubishi Denki Kabushiki Kaisha | Droplet floating apparatus |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3615541A1 (de) | 1987-11-12 |
| CA1329359C (en) | 1994-05-10 |
| EP0244867A2 (de) | 1987-11-11 |
| DE3615541C2 (enExample) | 1988-11-17 |
| US4960572A (en) | 1990-10-02 |
| EP0244867B1 (de) | 1991-09-11 |
| DE3772835D1 (de) | 1991-10-17 |
| EP0244867A3 (en) | 1989-07-19 |
| JPH0443880B2 (enExample) | 1992-07-17 |
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