DE3331136A1 - Verfahren zur aufnahme von ionen-zyklotron-resonanz-spektren und vorrichtung zur durchfuehrung des verfahrens - Google Patents
Verfahren zur aufnahme von ionen-zyklotron-resonanz-spektren und vorrichtung zur durchfuehrung des verfahrensInfo
- Publication number
- DE3331136A1 DE3331136A1 DE19833331136 DE3331136A DE3331136A1 DE 3331136 A1 DE3331136 A1 DE 3331136A1 DE 19833331136 DE19833331136 DE 19833331136 DE 3331136 A DE3331136 A DE 3331136A DE 3331136 A1 DE3331136 A1 DE 3331136A1
- Authority
- DE
- Germany
- Prior art keywords
- ions
- measuring cell
- sample substance
- primary ions
- primary
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims description 45
- 150000002500 ions Chemical class 0.000 claims description 103
- 239000000126 substance Substances 0.000 claims description 39
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 12
- 238000010894 electron beam technology Methods 0.000 claims description 10
- 238000001228 spectrum Methods 0.000 claims description 10
- 229910052786 argon Inorganic materials 0.000 claims description 6
- 238000005259 measurement Methods 0.000 claims description 6
- 238000005040 ion trap Methods 0.000 claims description 5
- 229910052756 noble gas Inorganic materials 0.000 claims description 5
- 239000007789 gas Substances 0.000 claims description 4
- 230000005684 electric field Effects 0.000 claims description 3
- 230000004936 stimulating effect Effects 0.000 claims 1
- 230000005284 excitation Effects 0.000 description 17
- 230000008569 process Effects 0.000 description 12
- 238000004611 spectroscopical analysis Methods 0.000 description 7
- 230000008901 benefit Effects 0.000 description 6
- 239000002245 particle Substances 0.000 description 5
- 238000000451 chemical ionisation Methods 0.000 description 4
- 238000004949 mass spectrometry Methods 0.000 description 4
- 230000008878 coupling Effects 0.000 description 3
- 238000010168 coupling process Methods 0.000 description 3
- 238000005859 coupling reaction Methods 0.000 description 3
- 238000010791 quenching Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 238000012935 Averaging Methods 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 238000003795 desorption Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000003993 interaction Effects 0.000 description 2
- 238000010884 ion-beam technique Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 241000276498 Pollachius virens Species 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000001793 charged compounds Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000010265 fast atom bombardment Methods 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 230000003116 impacting effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R33/00—Arrangements or instruments for measuring magnetic variables
- G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
- G01R33/64—Arrangements or instruments for measuring magnetic variables involving magnetic resonance using cyclotron resonance
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/26—Mass spectrometers or separator tubes
- H01J49/34—Dynamic spectrometers
- H01J49/36—Radio frequency spectrometers, e.g. Bennett-type spectrometers, Redhead-type spectrometers
- H01J49/38—Omegatrons ; using ion cyclotron resonance
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S505/00—Superconductor technology: apparatus, material, process
- Y10S505/825—Apparatus per se, device per se, or process of making or operating same
- Y10S505/842—Measuring and testing
Landscapes
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Electron Tubes For Measurement (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19833331136 DE3331136A1 (de) | 1983-08-30 | 1983-08-30 | Verfahren zur aufnahme von ionen-zyklotron-resonanz-spektren und vorrichtung zur durchfuehrung des verfahrens |
| DE8484108959T DE3480429D1 (en) | 1983-08-30 | 1984-07-28 | Method of recording ion cyclotron resonance spectra and apparatus for carrying out this method |
| EP84108959A EP0141059B1 (de) | 1983-08-30 | 1984-07-28 | Verfahren zur Aufnahme von Ionen-Zyklotron-Resonanz-Spektren und Vorrichtung zur Durchführung des Verfahrens |
| US06/645,051 US4563579A (en) | 1983-08-30 | 1984-08-28 | Procedure for recording ion-cyclotron-resonance spectra and apparatus for carrying out the procedure |
| JP59179510A JPS6084753A (ja) | 1983-08-30 | 1984-08-30 | イオンサイクロトロン共振スペクトルを記録する方法および装置 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19833331136 DE3331136A1 (de) | 1983-08-30 | 1983-08-30 | Verfahren zur aufnahme von ionen-zyklotron-resonanz-spektren und vorrichtung zur durchfuehrung des verfahrens |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3331136A1 true DE3331136A1 (de) | 1985-03-07 |
| DE3331136C2 DE3331136C2 (enExample) | 1990-06-07 |
Family
ID=6207728
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19833331136 Granted DE3331136A1 (de) | 1983-08-30 | 1983-08-30 | Verfahren zur aufnahme von ionen-zyklotron-resonanz-spektren und vorrichtung zur durchfuehrung des verfahrens |
| DE8484108959T Expired DE3480429D1 (en) | 1983-08-30 | 1984-07-28 | Method of recording ion cyclotron resonance spectra and apparatus for carrying out this method |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8484108959T Expired DE3480429D1 (en) | 1983-08-30 | 1984-07-28 | Method of recording ion cyclotron resonance spectra and apparatus for carrying out this method |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US4563579A (enExample) |
| EP (1) | EP0141059B1 (enExample) |
| JP (1) | JPS6084753A (enExample) |
| DE (2) | DE3331136A1 (enExample) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0221339A1 (de) * | 1985-10-29 | 1987-05-13 | Spectrospin AG | Ionen-Zyklotron-Resonanz-Spektrometer |
| EP0200027A3 (de) * | 1985-05-02 | 1987-10-21 | Spectrospin AG | Ionen-Zyklotron-Resonanz-Spektrometer |
| DE3627605A1 (de) * | 1986-08-14 | 1988-02-25 | Spectrospin Ag | Verfahren zum eliminieren unerwuenschter geladener teilchen aus der messzelle eines icr-spektrometers |
| DE3903322A1 (de) * | 1989-02-04 | 1990-08-16 | Nmi Naturwissenschaftl U Mediz | Verfahren zur erzeugung von ionen |
| US6555814B1 (en) | 1999-07-05 | 2003-04-29 | Brucker Daltonik Gmbh | Method and device for controlling the number of ions in ion cyclotron resonance mass spectrometers |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4668864A (en) * | 1984-08-22 | 1987-05-26 | Nicolet Instrument Corporation | Mass spectrometer |
| US4731584A (en) * | 1985-08-14 | 1988-03-15 | Picker International, Inc. | Magnetic resonance probe for operation at frequencies above self resonance |
| DE3733853A1 (de) * | 1987-10-07 | 1989-04-27 | Spectrospin Ag | Verfahren zum einbringen von ionen in die ionenfalle eines ionen-zyklotron-resonanz-spektrometers und zur durchfuehrung des verfahrens ausgebildetes ionen-zyklotron-resonanz-spektrometers |
| US4959543A (en) * | 1988-06-03 | 1990-09-25 | Ionspec Corporation | Method and apparatus for acceleration and detection of ions in an ion cyclotron resonance cell |
| WO1989012316A1 (en) * | 1988-06-06 | 1989-12-14 | University Of Delaware | Resolution improvement in an ion cyclotron resonance mass spectrometer |
| US4990775A (en) * | 1988-06-06 | 1991-02-05 | University Of Delaware | Resolution improvement in an ion cyclotron resonance mass spectrometer |
| GB2235086A (en) * | 1989-06-01 | 1991-02-20 | Ion Tech Ltd | Ion beam source |
| US5118950A (en) * | 1989-12-29 | 1992-06-02 | The United States Of America As Represented By The Secretary Of The Air Force | Cluster ion synthesis and confinement in hybrid ion trap arrays |
| US4982088A (en) * | 1990-02-02 | 1991-01-01 | California Institute Of Technology | Method and apparatus for highly sensitive spectroscopy of trapped ions |
| US5451781A (en) * | 1994-10-28 | 1995-09-19 | Regents Of The University Of California | Mini ion trap mass spectrometer |
| WO1999027559A1 (en) * | 1997-11-24 | 1999-06-03 | Gerasimos Daniel Danilatos | Radiofrequency gaseous detection device (rf-gdd) |
| DE10325582B4 (de) * | 2003-06-05 | 2009-01-15 | Bruker Daltonik Gmbh | Ionenfragmentierung durch Elektroneneinfang in Hochfrequenz-Ionenfallen mit magnetischer Führung der Elektronen |
| US7186972B2 (en) * | 2003-10-23 | 2007-03-06 | Beckman Coulter, Inc. | Time of flight mass analyzer having improved mass resolution and method of operating same |
| JP4275545B2 (ja) * | 2004-02-17 | 2009-06-10 | 株式会社日立ハイテクノロジーズ | 質量分析装置 |
| KR100874369B1 (ko) | 2007-04-17 | 2008-12-16 | 한국기초과학지원연구원 | 푸리에 변환 이온 싸이클로트론 공명 질량 분석기의 신호개선을 위한 장치 |
| US8362423B1 (en) * | 2011-09-20 | 2013-01-29 | The University Of Sussex | Ion trap |
| GB2517670B (en) * | 2013-03-15 | 2020-04-29 | Smiths Detection Watford Ltd | Ion modification |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3535512A (en) * | 1966-07-21 | 1970-10-20 | Varian Associates | Double resonance ion cyclotron mass spectrometer for studying ion-molecule reactions |
| DE3124465A1 (de) * | 1981-06-22 | 1983-01-05 | Spectrospin AG, 8117 Fällanden, Zürich | Verfahren zur ionen-zyklotron-resonanz-spektroskopie |
-
1983
- 1983-08-30 DE DE19833331136 patent/DE3331136A1/de active Granted
-
1984
- 1984-07-28 EP EP84108959A patent/EP0141059B1/de not_active Expired
- 1984-07-28 DE DE8484108959T patent/DE3480429D1/de not_active Expired
- 1984-08-28 US US06/645,051 patent/US4563579A/en not_active Expired - Lifetime
- 1984-08-30 JP JP59179510A patent/JPS6084753A/ja active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3535512A (en) * | 1966-07-21 | 1970-10-20 | Varian Associates | Double resonance ion cyclotron mass spectrometer for studying ion-molecule reactions |
| DE3124465A1 (de) * | 1981-06-22 | 1983-01-05 | Spectrospin AG, 8117 Fällanden, Zürich | Verfahren zur ionen-zyklotron-resonanz-spektroskopie |
Non-Patent Citations (3)
| Title |
|---|
| DE-Z.: Messtechnik, 78.Jg., Nr.6, 1970, S.109-115 * |
| Z.: Applied Physics, Bd.11, 1976, S.35-39 * |
| Z.: The Review of Scientific Instruments, Vol.36, Nr.4, 1965, S.466-475 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0200027A3 (de) * | 1985-05-02 | 1987-10-21 | Spectrospin AG | Ionen-Zyklotron-Resonanz-Spektrometer |
| EP0221339A1 (de) * | 1985-10-29 | 1987-05-13 | Spectrospin AG | Ionen-Zyklotron-Resonanz-Spektrometer |
| DE3627605A1 (de) * | 1986-08-14 | 1988-02-25 | Spectrospin Ag | Verfahren zum eliminieren unerwuenschter geladener teilchen aus der messzelle eines icr-spektrometers |
| DE3903322A1 (de) * | 1989-02-04 | 1990-08-16 | Nmi Naturwissenschaftl U Mediz | Verfahren zur erzeugung von ionen |
| US6555814B1 (en) | 1999-07-05 | 2003-04-29 | Brucker Daltonik Gmbh | Method and device for controlling the number of ions in ion cyclotron resonance mass spectrometers |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3331136C2 (enExample) | 1990-06-07 |
| EP0141059A2 (de) | 1985-05-15 |
| EP0141059A3 (en) | 1986-02-12 |
| EP0141059B1 (de) | 1989-11-08 |
| DE3480429D1 (en) | 1989-12-14 |
| JPS6084753A (ja) | 1985-05-14 |
| US4563579A (en) | 1986-01-07 |
| JPH0378743B2 (enExample) | 1991-12-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |