DE3000727A1 - Verfahren zur herstellung von konzentriertem natuerlichen essig und essigsaeureestern - Google Patents
Verfahren zur herstellung von konzentriertem natuerlichen essig und essigsaeureesternInfo
- Publication number
- DE3000727A1 DE3000727A1 DE19803000727 DE3000727A DE3000727A1 DE 3000727 A1 DE3000727 A1 DE 3000727A1 DE 19803000727 DE19803000727 DE 19803000727 DE 3000727 A DE3000727 A DE 3000727A DE 3000727 A1 DE3000727 A1 DE 3000727A1
- Authority
- DE
- Germany
- Prior art keywords
- alcohol
- vinegar
- natural
- acetic acid
- concentrated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 150000002168 ethanoic acid esters Chemical class 0.000 title claims description 11
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 89
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 58
- 235000021419 vinegar Nutrition 0.000 claims description 53
- 239000000052 vinegar Substances 0.000 claims description 53
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 48
- 238000000034 method Methods 0.000 claims description 26
- 238000000855 fermentation Methods 0.000 claims description 21
- 230000004151 fermentation Effects 0.000 claims description 21
- 239000000203 mixture Substances 0.000 claims description 18
- 230000008014 freezing Effects 0.000 claims description 16
- 238000007710 freezing Methods 0.000 claims description 16
- 230000002378 acidificating effect Effects 0.000 claims description 12
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 10
- 239000003456 ion exchange resin Substances 0.000 claims description 9
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 9
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 229960000583 acetic acid Drugs 0.000 description 29
- 239000007788 liquid Substances 0.000 description 7
- 239000000243 solution Substances 0.000 description 6
- 229930014626 natural product Natural products 0.000 description 5
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 4
- 235000013399 edible fruits Nutrition 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- -1 0-296 or 1-696) Chemical compound 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- 235000006085 Vigna mungo var mungo Nutrition 0.000 description 2
- 240000005616 Vigna mungo var. mungo Species 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000001476 alcoholic effect Effects 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 235000015203 fruit juice Nutrition 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241000589220 Acetobacter Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 241000193403 Clostridium Species 0.000 description 1
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 1
- 238000006887 Ullmann reaction Methods 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000003729 cation exchange resin Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 239000001963 growth medium Substances 0.000 description 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 235000021440 light beer Nutrition 0.000 description 1
- 235000021430 malt vinegar Nutrition 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 229920001592 potato starch Polymers 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 235000015067 sauces Nutrition 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000000859 sublimation Methods 0.000 description 1
- 230000008022 sublimation Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- CYRMSUTZVYGINF-UHFFFAOYSA-N trichlorofluoromethane Chemical compound FC(Cl)(Cl)Cl CYRMSUTZVYGINF-UHFFFAOYSA-N 0.000 description 1
- 229940029284 trichlorofluoromethane Drugs 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
- C12J1/00—Vinegar; Preparation or purification thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7900196A NL7900196A (nl) | 1979-01-10 | 1979-01-10 | Werkwijze voor de bereiding van geconcentreerde natuurazijn en werkwijze voor de bereiding van azijnzuuresters. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3000727A1 true DE3000727A1 (de) | 1980-07-24 |
Family
ID=19832420
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19803000727 Withdrawn DE3000727A1 (de) | 1979-01-10 | 1980-01-08 | Verfahren zur herstellung von konzentriertem natuerlichen essig und essigsaeureestern |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4313960A (enExample) |
| BE (1) | BE881082A (enExample) |
| DE (1) | DE3000727A1 (enExample) |
| FR (1) | FR2446316A1 (enExample) |
| GB (1) | GB2040155B (enExample) |
| NL (1) | NL7900196A (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4897272A (en) * | 1987-11-20 | 1990-01-30 | Tamanoi Vinegar Corporation Limited | Process for producing rice vinegar |
| US5770761A (en) * | 1996-11-08 | 1998-06-23 | Chinese Petroleum Corporation | Process for ethyl acetate production |
| FR2757539B1 (fr) * | 1996-12-24 | 1999-03-05 | Bioconversion | Esters d'origine vegetale utilises comme substituts de carburants ou combustibles et leur procede de production |
| US6517822B1 (en) * | 1998-02-13 | 2003-02-11 | Carol J. Buck | Formulations and methods for straightening hair |
| US20040180016A1 (en) * | 1998-02-13 | 2004-09-16 | Buck Carol J. | Formulations and methods for straightening hair |
| US5993853A (en) * | 1998-06-22 | 1999-11-30 | Manning; Bethany M. | Dietary supplement |
| US6399812B1 (en) | 2000-04-27 | 2002-06-04 | Tsoung Y. Yan | Production of aliphatic esters |
| EP1231257A1 (en) * | 2001-02-12 | 2002-08-14 | Davide Maletti | A process for the production of aromatic vinegar |
| EP1325952A1 (en) * | 2001-12-31 | 2003-07-09 | Monari Federzoni S.p.A. | Food products based on fruits and a process for their production |
| CN104178408B (zh) * | 2013-05-21 | 2018-02-02 | 石小和 | 食醋的冷冻浓缩工艺 |
| EP3122865B1 (en) | 2014-03-24 | 2019-12-11 | Purac Biochem B.V. | Neutralized vinegar concentrates and liquid food grade blends containing said neutralized vinegar concentrates |
| BR112016022076B1 (pt) | 2014-03-24 | 2022-05-31 | Purac Biochem B.V. | Processo de produção de concentrado de vinagre neutralizado, processo de produção de um produto de conservação de alimento líquido, produtos obtidos de tais processos, método de tratamento de um produto alimentício com tais produtos e uso de tais produtos em um produto alimentício |
| GB202117110D0 (en) * | 2021-11-26 | 2022-01-12 | Ripcell Ltd | Apparatus & method |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3404006A (en) * | 1964-08-31 | 1968-10-01 | Phillips Petroleum Co | Wine preparation by fermenting a juice, concentrating the fermented product, and optionally fortifying the concentrate |
| US4076844A (en) * | 1975-12-22 | 1978-02-28 | Firma Heinrich Frings | Two stage process for the production of vinegar with high acetic acid concentration |
-
1979
- 1979-01-10 NL NL7900196A patent/NL7900196A/nl not_active Application Discontinuation
-
1980
- 1980-01-08 DE DE19803000727 patent/DE3000727A1/de not_active Withdrawn
- 1980-01-09 US US06/110,746 patent/US4313960A/en not_active Expired - Lifetime
- 1980-01-10 BE BE0/198910A patent/BE881082A/nl not_active IP Right Cessation
- 1980-01-10 FR FR8000527A patent/FR2446316A1/fr active Granted
- 1980-01-10 GB GB8000893A patent/GB2040155B/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US4313960A (en) | 1982-02-02 |
| NL7900196A (nl) | 1980-07-14 |
| GB2040155A (en) | 1980-08-28 |
| BE881082A (nl) | 1980-07-10 |
| FR2446316A1 (fr) | 1980-08-08 |
| GB2040155B (en) | 1983-04-13 |
| FR2446316B1 (enExample) | 1983-07-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8139 | Disposal/non-payment of the annual fee |