DE287933C - - Google Patents
Info
- Publication number
- DE287933C DE287933C DENDAT287933D DE287933DA DE287933C DE 287933 C DE287933 C DE 287933C DE NDAT287933 D DENDAT287933 D DE NDAT287933D DE 287933D A DE287933D A DE 287933DA DE 287933 C DE287933 C DE 287933C
- Authority
- DE
- Germany
- Prior art keywords
- acetone
- sodium
- ether
- freer
- vol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims description 3
- 150000001408 amides Chemical class 0.000 claims description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 18
- GKHOLUJNLGYFHA-UHFFFAOYSA-N [Na].CC(C)=O Chemical compound [Na].CC(C)=O GKHOLUJNLGYFHA-UHFFFAOYSA-N 0.000 description 9
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- ODZPKZBBUMBTMG-UHFFFAOYSA-N sodium amide Chemical compound [NH2-].[Na+] ODZPKZBBUMBTMG-UHFFFAOYSA-N 0.000 description 5
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- -1 acetone sodium 3-methylbutynol Chemical compound 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- SWXVUIWOUIDPGS-UHFFFAOYSA-N diacetone alcohol Chemical compound CC(=O)CC(C)(C)O SWXVUIWOUIDPGS-UHFFFAOYSA-N 0.000 description 2
- 239000012442 inert solvent Chemical group 0.000 description 2
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- ZFFBIQMNKOJDJE-UHFFFAOYSA-N 2-bromo-1,2-diphenylethanone Chemical compound C=1C=CC=CC=1C(Br)C(=O)C1=CC=CC=C1 ZFFBIQMNKOJDJE-UHFFFAOYSA-N 0.000 description 1
- 238000005684 Liebig rearrangement reaction Methods 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 239000003701 inert diluent Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 150000003388 sodium compounds Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F1/00—Compounds containing elements of Groups 1 or 11 of the Periodic Table
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE289498T |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE287933C true DE287933C (enExample) |
Family
ID=32997327
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT289498D Active DE289498C (enExample) | |||
| DENDAT289497D Active DE289497C (enExample) | |||
| DENDAT287933D Active DE287933C (enExample) |
Family Applications Before (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT289498D Active DE289498C (enExample) | |||
| DENDAT289497D Active DE289497C (enExample) |
Country Status (1)
| Country | Link |
|---|---|
| DE (3) | DE287933C (enExample) |
-
0
- DE DENDAT289498D patent/DE289498C/de active Active
- DE DENDAT289497D patent/DE289497C/de active Active
- DE DENDAT287933D patent/DE287933C/de active Active
Also Published As
| Publication number | Publication date |
|---|---|
| DE289497C (enExample) | |
| DE289498C (enExample) |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE287933C (enExample) | ||
| EP0026847B1 (de) | Verfahren zur Herstellung von 4-Amino-5-chlor-1-phenyl-pyridazon-(6) | |
| DD144051A5 (de) | Verfahren zur herstellung von isocyanaten | |
| EP0012261B1 (de) | Substituierte Spiro-Derivate von 3-(3,5-Dichlorphenyl)-oxazolidin-2,4-dionen, Verfahren zu ihrer Herstellung sowie ihre Verwendung als Fungizide | |
| DE865739C (de) | Verfahren zur Herstellung von Monochloressigsaeure | |
| DE859456C (de) | Verfahren zur Herstellung von Thiolactonen | |
| DE808835C (de) | Verfahren zur Herstellung von Nitrilen | |
| DE691621C (de) | Verfahren zur Herstellung von Nitrilen mit 5 Kohlenstoffatomen | |
| DE1163800B (de) | Verfahren zur Herstellung von Methacrylsaeureamidsulfat durch Umsetzung von Acetoncyanhydrin mit Schwefelsaeure | |
| DE882702C (de) | Verfahren zur Herstellung von Imidazolderivaten | |
| DE953795C (de) | Verfahren zur Herstellung von Monothiono-pyrophorsaeure-tetraalkylestern | |
| DE840686C (de) | Verfahren zur Herstellung eines Gemisches von Diacetonalkohol und Hydracetylaceton | |
| DE338281C (de) | Verfahren zur Herstellung von Alkylaethern des Vinylalkohols und seiner Homologen | |
| DE767830C (de) | Verfahren zur Herstellung von N-substituierten Aminocyanphosphinsaeure- bzw. -thiophosphinsaeureestern | |
| EP0029495A1 (de) | Verfahren zur Herstellung von 3-Cyanopropionsäureamid | |
| DE1048586B (enExample) | ||
| EP0080106A1 (de) | Verfahren zur Herstellung von N-substituierten N-Isocyanatocarbonyl-carbamaten | |
| DE1543894C (de) | 2,3-Dimethy 1-5-tert-butylphenol, seine Verwendung und Verfahren zu seiner Herstellung | |
| DE882850C (de) | Verfahren zur Herstellung von mehrwertigen Alkoholen der Diacetylenreihe | |
| DE445524C (de) | Verfahren zur Darstellung von ªÏ-Chloracetobrenzcatechin | |
| DE1002359B (de) | Verfahren zur Herstellung von N,N'-Dioxyaethylpiperazin | |
| DE1103327B (de) | Verfahren zur Herstellung von substituierten Cyclopentadienen | |
| DE1041053B (de) | Verfahren zur Herstellung von Pentachloranilinen | |
| DE1175242B (de) | Verfahren zur Herstellung von AEthylenimin-N-aethylphosphonsaeure-dialkylestern | |
| DE1167833B (de) | Verfahren zur Herstellung substituierter N-Dialkylaluminylcarbonsaeureamide oder -thiocarbonsaeureamide |