DE268646C - - Google Patents

Info

Publication number

DE268646C

DE268646C DENDAT268646D DE268646DA DE268646C DE 268646 C DE268646 C DE 268646C DE NDAT268646 D DENDAT268646 D DE NDAT268646D DE 268646D A DE268646D A DE 268646DA DE 268646 C DE268646 C DE 268646C

Authority

DE

Germany

Prior art keywords

violet

sulfuric acid

aryl

solution

concentrated sulfuric

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 claims description 4
• 125000001841 imino group Chemical group [H]N=* 0.000 claims description 4
• 150000004056 anthraquinones Chemical class 0.000 claims description 3
• 125000003118 aryl group Chemical group 0.000 claims description 2
• 150000005840 aryl radicals Chemical class 0.000 claims description 2
• 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 2
• 238000000034 method Methods 0.000 claims description 2
• 238000002360 preparation method Methods 0.000 claims description 2
• RZVHIXYEVGDQDX-UHFFFAOYSA-N 9,10-anthraquinone Chemical group C1=CC=C2C(=O)C3=CC=CC=C3C(=O)C2=C1 RZVHIXYEVGDQDX-UHFFFAOYSA-N 0.000 claims 1
• 239000007800 oxidant agent Substances 0.000 claims 1
• 238000006467 substitution reaction Methods 0.000 claims 1
• QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 9
• PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 8
• ZYECOAILUNWEAL-NUDFZHEQSA-N (4z)-4-[[2-methoxy-5-(phenylcarbamoyl)phenyl]hydrazinylidene]-n-(3-nitrophenyl)-3-oxonaphthalene-2-carboxamide Chemical compound COC1=CC=C(C(=O)NC=2C=CC=CC=2)C=C1N\N=C(C1=CC=CC=C1C=1)/C(=O)C=1C(=O)NC1=CC=CC([N+]([O-])=O)=C1 ZYECOAILUNWEAL-NUDFZHEQSA-N 0.000 description 5
• QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 5
• 230000003647 oxidation Effects 0.000 description 5
• 238000007254 oxidation reaction Methods 0.000 description 5
• 239000000984 vat dye Substances 0.000 description 5
• NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 4
• 229920000742 Cotton Polymers 0.000 description 3
• 239000000843 powder Substances 0.000 description 3
• 229910021529 ammonia Inorganic materials 0.000 description 2
• RWZYAGGXGHYGMB-UHFFFAOYSA-N anthranilic acid Chemical compound NC1=CC=CC=C1C(O)=O RWZYAGGXGHYGMB-UHFFFAOYSA-N 0.000 description 2
• GRWZHXKQBITJKP-UHFFFAOYSA-L dithionite(2-) Chemical compound [O-]S(=O)S([O-])=O GRWZHXKQBITJKP-UHFFFAOYSA-L 0.000 description 2
• 238000010438 heat treatment Methods 0.000 description 2
• RNVCVTLRINQCPJ-UHFFFAOYSA-N o-toluidine Chemical compound CC1=CC=CC=C1N RNVCVTLRINQCPJ-UHFFFAOYSA-N 0.000 description 2
• 238000003756 stirring Methods 0.000 description 2
• GDALETGZDYOOGB-UHFFFAOYSA-N Acridone Natural products C1=C(O)C=C2N(C)C3=CC=CC=C3C(=O)C2=C1O GDALETGZDYOOGB-UHFFFAOYSA-N 0.000 description 1
• VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
• LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
• 229910001369 Brass Inorganic materials 0.000 description 1
• 239000002253 acid Substances 0.000 description 1
• FZEYVTFCMJSGMP-UHFFFAOYSA-N acridone Chemical compound C1=CC=C2C(=O)C3=CC=CC=C3NC2=C1 FZEYVTFCMJSGMP-UHFFFAOYSA-N 0.000 description 1
• -1 anthraquinone radical Chemical class 0.000 description 1
• 239000010951 brass Substances 0.000 description 1
• 239000003795 chemical substances by application Substances 0.000 description 1
• 239000003086 colorant Substances 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 239000000975 dye Substances 0.000 description 1
• 150000002697 manganese compounds Chemical class 0.000 description 1
• 239000002994 raw material Substances 0.000 description 1