DE2611667A1 - Verfahren zur gewinnung von chlor und eisenoxid aus verunreinigten eisen(ii)-chloridhaltigen chloridgemischen, welche bei der chlorierung titanhaltiger rohstoffe anfallen - Google Patents
Verfahren zur gewinnung von chlor und eisenoxid aus verunreinigten eisen(ii)-chloridhaltigen chloridgemischen, welche bei der chlorierung titanhaltiger rohstoffe anfallenInfo
- Publication number
- DE2611667A1 DE2611667A1 DE19762611667 DE2611667A DE2611667A1 DE 2611667 A1 DE2611667 A1 DE 2611667A1 DE 19762611667 DE19762611667 DE 19762611667 DE 2611667 A DE2611667 A DE 2611667A DE 2611667 A1 DE2611667 A1 DE 2611667A1
- Authority
- DE
- Germany
- Prior art keywords
- chloride
- iron
- oxygen
- chlorine
- chlorination
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000000203 mixture Substances 0.000 title claims description 38
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 title claims description 32
- 238000005660 chlorination reaction Methods 0.000 title claims description 31
- 238000000034 method Methods 0.000 title claims description 30
- 239000000460 chlorine Substances 0.000 title claims description 28
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 title claims description 10
- 239000002994 raw material Substances 0.000 title claims description 8
- 229910001902 chlorine oxide Inorganic materials 0.000 title claims description 6
- 238000011084 recovery Methods 0.000 title description 2
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 title 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical class [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 title 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims description 37
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 33
- 239000001301 oxygen Substances 0.000 claims description 33
- 229910052760 oxygen Inorganic materials 0.000 claims description 33
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 31
- 239000007789 gas Substances 0.000 claims description 30
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 25
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical class Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 claims description 25
- 229910052801 chlorine Inorganic materials 0.000 claims description 20
- 229910021577 Iron(II) chloride Inorganic materials 0.000 claims description 19
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims description 19
- 238000006243 chemical reaction Methods 0.000 claims description 16
- 239000000571 coke Substances 0.000 claims description 15
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 10
- 239000010936 titanium Substances 0.000 claims description 10
- 229910052719 titanium Inorganic materials 0.000 claims description 10
- YDZQQRWRVYGNER-UHFFFAOYSA-N iron;titanium;trihydrate Chemical compound O.O.O.[Ti].[Fe] YDZQQRWRVYGNER-UHFFFAOYSA-N 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- 239000008247 solid mixture Substances 0.000 claims description 7
- 230000015572 biosynthetic process Effects 0.000 claims description 6
- 238000000926 separation method Methods 0.000 claims description 4
- 239000011541 reaction mixture Substances 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 description 14
- 238000007254 oxidation reaction Methods 0.000 description 14
- 239000000428 dust Substances 0.000 description 13
- 229910052742 iron Inorganic materials 0.000 description 8
- 239000000446 fuel Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- 229910004298 SiO 2 Inorganic materials 0.000 description 3
- 229910002091 carbon monoxide Inorganic materials 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 229910017135 Fe—O Inorganic materials 0.000 description 2
- 229910010413 TiO 2 Inorganic materials 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical class [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- 241000219198 Brassica Species 0.000 description 1
- 235000003351 Brassica cretica Nutrition 0.000 description 1
- 235000003343 Brassica rupestris Nutrition 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- QKSKPIVNLNLAAV-UHFFFAOYSA-N bis(2-chloroethyl) sulfide Chemical compound ClCCSCCCl QKSKPIVNLNLAAV-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 150000002483 hydrogen compounds Chemical class 0.000 description 1
- 239000001034 iron oxide pigment Substances 0.000 description 1
- LIKBJVNGSGBSGK-UHFFFAOYSA-N iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Fe+3].[Fe+3] LIKBJVNGSGBSGK-UHFFFAOYSA-N 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- 229910001510 metal chloride Inorganic materials 0.000 description 1
- 235000010460 mustard Nutrition 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- 230000036284 oxygen consumption Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/03—Preparation from chlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
- C01G49/02—Oxides; Hydroxides
- C01G49/06—Ferric oxide [Fe2O3]
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (11)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19762611667 DE2611667A1 (de) | 1976-03-19 | 1976-03-19 | Verfahren zur gewinnung von chlor und eisenoxid aus verunreinigten eisen(ii)-chloridhaltigen chloridgemischen, welche bei der chlorierung titanhaltiger rohstoffe anfallen |
| CA271,140A CA1082886A (en) | 1976-03-19 | 1977-02-07 | Process for recovery of iron oxide and chlorine from dust produced in chlorination of titaniferous ores |
| US05/768,542 US4060584A (en) | 1976-03-19 | 1977-02-14 | Process for recovery of iron oxide and chlorine from dust produced in chlorination of titaniferous ores |
| FI770500A FI770500A7 (enExample) | 1976-03-19 | 1977-02-16 | |
| AU23186/77A AU504250B2 (en) | 1976-03-19 | 1977-03-11 | Obtaining chlorine and ferric oxide from ferrous chloride |
| IT21308/77A IT1084454B (it) | 1976-03-19 | 1977-03-16 | Processo per il recupero di cloro e di ossido di ferro da miscugli impuri di cloruri contenenti cloruro di ferro (ii), sottoprodotti della clorurazione di materie prime contenenti titanio. |
| BE175863A BE852563A (fr) | 1976-03-19 | 1977-03-17 | Procede pour isoler le chlore et l'oxyde de fer de melanges de chlorures impurs contenant du chlorure de fer (ii) |
| FR7708073A FR2344496A1 (fr) | 1976-03-19 | 1977-03-17 | Procede pour preparer du chlore et de l'oxyde de fer a partir de melanges de chlorures impurs contenant du chlorure de fer (ii) |
| JP3021377A JPS52114491A (en) | 1976-03-19 | 1977-03-18 | Method of obtaining chlorine and iron oxide from impurified and iron*2* chlorideecontaining chloride mixture which is formed at chlorination of titaniummcontaining row materials |
| NL7702983A NL7702983A (nl) | 1976-03-19 | 1977-03-18 | Werkwijze om ijzer(ii)chloridemengsels op te werken. |
| GB11651/77A GB1517264A (en) | 1976-03-19 | 1977-03-18 | Treatment of iron(ii)chloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19762611667 DE2611667A1 (de) | 1976-03-19 | 1976-03-19 | Verfahren zur gewinnung von chlor und eisenoxid aus verunreinigten eisen(ii)-chloridhaltigen chloridgemischen, welche bei der chlorierung titanhaltiger rohstoffe anfallen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2611667A1 true DE2611667A1 (de) | 1977-09-29 |
Family
ID=5972920
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19762611667 Withdrawn DE2611667A1 (de) | 1976-03-19 | 1976-03-19 | Verfahren zur gewinnung von chlor und eisenoxid aus verunreinigten eisen(ii)-chloridhaltigen chloridgemischen, welche bei der chlorierung titanhaltiger rohstoffe anfallen |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4060584A (enExample) |
| JP (1) | JPS52114491A (enExample) |
| AU (1) | AU504250B2 (enExample) |
| BE (1) | BE852563A (enExample) |
| CA (1) | CA1082886A (enExample) |
| DE (1) | DE2611667A1 (enExample) |
| FI (1) | FI770500A7 (enExample) |
| FR (1) | FR2344496A1 (enExample) |
| GB (1) | GB1517264A (enExample) |
| IT (1) | IT1084454B (enExample) |
| NL (1) | NL7702983A (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0005054A3 (en) * | 1978-04-21 | 1979-11-28 | Mineral Process Licensing Corporation Bv | Process for the preparation of iron oxide and compositions containing iron oxide |
| CA1113225A (en) * | 1978-05-16 | 1981-12-01 | Mineral Process Licensing Corporation B.V. | Recovery of chlorine values |
| US4532113A (en) * | 1983-05-26 | 1985-07-30 | E. I. Du Pont De Nemours And Company | Iron chloride waste treatment in molten salt |
| GB8415034D0 (en) * | 1984-06-13 | 1984-07-18 | Laporte Industries Ltd | Recovery of chlorine |
| US5064632A (en) * | 1984-08-08 | 1991-11-12 | Scm Chemicals, Inc. | Process for partial oxidation of FeCl2 to FeCl3 |
| US4994255A (en) * | 1986-07-24 | 1991-02-19 | Scm Chemicals, Inc. | Oxidation of ferrous chloride directly to chlorine in a fluid bed reactor |
| EP0272465B1 (de) * | 1986-12-10 | 1993-02-24 | BBC Brown Boveri AG | Verfahren und Vorrichtung zur Trennung und/oder Umsatz von Partikeln |
| GB9803018D0 (en) * | 1998-02-13 | 1998-04-08 | Tioxide Group Services Ltd | Treatment of metal chloride |
| AUPP455098A0 (en) | 1998-07-07 | 1998-07-30 | Commonwealth Scientific And Industrial Research Organisation | Process for chlorine recovery |
| US6277354B1 (en) * | 1999-06-10 | 2001-08-21 | E. I. Dupont De Nemours And Company | Process for the recovery of chlorine from iron chlorides |
| JP2010504423A (ja) * | 2006-09-21 | 2010-02-12 | キュイテ−フェル エ チタン インコーポレイティド | 鉄分の豊富な金属塩化物の廃棄物からの金属鉄および塩素価値の回収のための電気化学的方法 |
| EP2265749B8 (en) * | 2008-03-20 | 2013-07-31 | Rio Tinto Fer et Titane Inc. | Electrochemical process for the recovery of metallic iron and chlorine values from iron-rich metal chloride wastes |
| RU2663742C2 (ru) | 2013-03-06 | 2018-08-09 | Тохо Титаниум Ко., Лтд. | Способ получения тетрахлорида титана |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB306691A (en) * | 1928-02-10 | 1929-02-28 | Stanley Isaac Levy | Improvements in and relating to the treatment of pyrites |
| US3325252A (en) * | 1964-02-26 | 1967-06-13 | American Cyanamid Co | Preparation of iron oxide and chlorine by two-zone oxidation of iron chloride |
| BE795169A (fr) * | 1972-02-09 | 1973-08-08 | Du Pont | Procede d'oxydation des chlorures de fer |
| GB1407034A (en) * | 1972-07-21 | 1975-09-24 | Laporte Industries Ltd | Process for the recovery of chlorine |
| US3865920A (en) * | 1973-03-14 | 1975-02-11 | Rutile & Zircon Mines Newcastl | Process for beneficiating a titaniferous ore and production of chlorine and iron oxide |
| JPS5519300B2 (enExample) * | 1973-07-12 | 1980-05-24 |
-
1976
- 1976-03-19 DE DE19762611667 patent/DE2611667A1/de not_active Withdrawn
-
1977
- 1977-02-07 CA CA271,140A patent/CA1082886A/en not_active Expired
- 1977-02-14 US US05/768,542 patent/US4060584A/en not_active Expired - Lifetime
- 1977-02-16 FI FI770500A patent/FI770500A7/fi not_active Application Discontinuation
- 1977-03-11 AU AU23186/77A patent/AU504250B2/en not_active Expired
- 1977-03-16 IT IT21308/77A patent/IT1084454B/it active
- 1977-03-17 FR FR7708073A patent/FR2344496A1/fr active Granted
- 1977-03-17 BE BE175863A patent/BE852563A/xx unknown
- 1977-03-18 GB GB11651/77A patent/GB1517264A/en not_active Expired
- 1977-03-18 JP JP3021377A patent/JPS52114491A/ja active Pending
- 1977-03-18 NL NL7702983A patent/NL7702983A/xx not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| US4060584A (en) | 1977-11-29 |
| IT1084454B (it) | 1985-05-25 |
| BE852563A (fr) | 1977-07-18 |
| GB1517264A (en) | 1978-07-12 |
| FR2344496B1 (enExample) | 1980-10-24 |
| JPS52114491A (en) | 1977-09-26 |
| FR2344496A1 (fr) | 1977-10-14 |
| AU2318677A (en) | 1978-09-14 |
| CA1082886A (en) | 1980-08-05 |
| NL7702983A (nl) | 1977-09-21 |
| FI770500A7 (enExample) | 1977-09-20 |
| AU504250B2 (en) | 1979-10-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| 8130 | Withdrawal |