DE2542007C3 - Verfahren zum Färben von natürlichen und synthetischen Polyamidfasern - Google Patents
Verfahren zum Färben von natürlichen und synthetischen PolyamidfasernInfo
- Publication number
- DE2542007C3 DE2542007C3 DE19752542007 DE2542007A DE2542007C3 DE 2542007 C3 DE2542007 C3 DE 2542007C3 DE 19752542007 DE19752542007 DE 19752542007 DE 2542007 A DE2542007 A DE 2542007A DE 2542007 C3 DE2542007 C3 DE 2542007C3
- Authority
- DE
- Germany
- Prior art keywords
- water
- parts
- dye
- treated
- soluble
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 33
- 239000000835 fiber Substances 0.000 title claims description 20
- 238000004043 dyeing Methods 0.000 title claims description 16
- 239000004952 Polyamide Substances 0.000 title claims description 5
- 229920002647 polyamide Polymers 0.000 title claims description 5
- 239000000975 dye Substances 0.000 claims description 33
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 21
- 229910052804 chromium Inorganic materials 0.000 claims description 20
- 239000011651 chromium Substances 0.000 claims description 20
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 14
- 150000003839 salts Chemical class 0.000 claims description 14
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 14
- 235000011152 sodium sulphate Nutrition 0.000 claims description 14
- 238000004532 chromating Methods 0.000 claims description 13
- 239000003795 chemical substances by application Substances 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 9
- 239000002253 acid Substances 0.000 claims description 7
- -1 alkyl sulfone Chemical class 0.000 claims description 5
- 150000001450 anions Chemical class 0.000 claims description 5
- 239000000460 chlorine Substances 0.000 claims description 5
- 238000007747 plating Methods 0.000 claims description 5
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 4
- 229910052801 chlorine Inorganic materials 0.000 claims description 4
- 239000011593 sulfur Substances 0.000 claims description 4
- 229910052717 sulfur Inorganic materials 0.000 claims description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 3
- 239000011574 phosphorus Substances 0.000 claims description 3
- 229910052698 phosphorus Inorganic materials 0.000 claims description 3
- 125000002947 alkylene group Chemical group 0.000 claims description 2
- 125000005362 aryl sulfone group Chemical group 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 150000001447 alkali salts Chemical class 0.000 claims 2
- KMUONIBRACKNSN-UHFFFAOYSA-N potassium dichromate Chemical compound [K+].[K+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KMUONIBRACKNSN-UHFFFAOYSA-N 0.000 description 24
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 22
- 210000002268 wool Anatomy 0.000 description 20
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 18
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 11
- 235000019253 formic acid Nutrition 0.000 description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- JOPOVCBBYLSVDA-UHFFFAOYSA-N chromium(6+) Chemical compound [Cr+6] JOPOVCBBYLSVDA-UHFFFAOYSA-N 0.000 description 8
- IZHYRVRPSNAXGV-UHFFFAOYSA-M potassium;naphthalene-1-sulfonate Chemical compound [K+].C1=CC=C2C(S(=O)(=O)[O-])=CC=CC2=C1 IZHYRVRPSNAXGV-UHFFFAOYSA-M 0.000 description 7
- 238000005254 chromizing Methods 0.000 description 6
- IBWNNKCIOUIBJP-UHFFFAOYSA-N sulfurous acid;urea Chemical compound NC(N)=O.OS(O)=O IBWNNKCIOUIBJP-UHFFFAOYSA-N 0.000 description 5
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 description 4
- 238000004040 coloring Methods 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- MCSXGCZMEPXKIW-UHFFFAOYSA-N 3-hydroxy-4-[(4-methyl-2-nitrophenyl)diazenyl]-N-(3-nitrophenyl)naphthalene-2-carboxamide Chemical compound Cc1ccc(N=Nc2c(O)c(cc3ccccc23)C(=O)Nc2cccc(c2)[N+]([O-])=O)c(c1)[N+]([O-])=O MCSXGCZMEPXKIW-UHFFFAOYSA-N 0.000 description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- IPTLKMXBROVJJF-UHFFFAOYSA-N azanium;methyl sulfate Chemical compound N.COS(O)(=O)=O IPTLKMXBROVJJF-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- BEQIIZJSZSVJJK-UHFFFAOYSA-M chembl2028372 Chemical compound [Na+].OC1=CC=C(S([O-])(=O)=O)C=C1N=NC1=C(O)C=CC2=CC=CC=C12 BEQIIZJSZSVJJK-UHFFFAOYSA-M 0.000 description 2
- ZQWICJYATMSSSD-UHFFFAOYSA-M chembl2028584 Chemical compound [Na+].C1=CC=C2C(N=NC3=C4C=CC=CC4=CC=C3O)=C(O)C=C(S([O-])(=O)=O)C2=C1 ZQWICJYATMSSSD-UHFFFAOYSA-M 0.000 description 2
- 229910000073 phosphorus hydride Inorganic materials 0.000 description 2
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 2
- LFORPQYIKMHOCK-UHFFFAOYSA-M sodium;3-methylbutyl sulfate Chemical compound [Na+].CC(C)CCOS([O-])(=O)=O LFORPQYIKMHOCK-UHFFFAOYSA-M 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- AZXGXVQWEUFULR-UHFFFAOYSA-N 2',4',5',7'-tetrabromofluorescein Chemical compound OC(=O)C1=CC=CC=C1C1=C2C=C(Br)C(=O)C(Br)=C2OC2=C(Br)C(O)=C(Br)C=C21 AZXGXVQWEUFULR-UHFFFAOYSA-N 0.000 description 1
- PCTPNZUXYWWIEQ-UHFFFAOYSA-N 8-methoxy-6-(p-methoxyphenyl)-13-methyl-6,12-methano-12h-dibenzo(d,g)(1,3)dioxocin-3-ol acetate Chemical compound C1=CC(OC)=CC=C1C1(OC2=C(OC)C=CC=C22)C(C)C2C2=CC=C(OC(C)=O)C=C2O1 PCTPNZUXYWWIEQ-UHFFFAOYSA-N 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- KIWBPDUYBMNFTB-UHFFFAOYSA-N Ethyl hydrogen sulfate Chemical compound CCOS(O)(=O)=O KIWBPDUYBMNFTB-UHFFFAOYSA-N 0.000 description 1
- 241000083473 Lychnis Species 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- CIUQDSCDWFSTQR-UHFFFAOYSA-N [C]1=CC=CC=C1 Chemical compound [C]1=CC=CC=C1 CIUQDSCDWFSTQR-UHFFFAOYSA-N 0.000 description 1
- KCGAKPRPJUVRFP-UHFFFAOYSA-N [Cr](=O)([O-])O[Cr](=O)[O-].[K+].[K+] Chemical compound [Cr](=O)([O-])O[Cr](=O)[O-].[K+].[K+] KCGAKPRPJUVRFP-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical class N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 150000005840 aryl radicals Chemical class 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- LNXMADNIUWFTPP-UHFFFAOYSA-L chembl2028186 Chemical compound [Na+].[Na+].OC1=CC=C(Cl)C=C1N=NC1=C(O)C2=C(O)C=C(S([O-])(=O)=O)C=C2C=C1S([O-])(=O)=O LNXMADNIUWFTPP-UHFFFAOYSA-L 0.000 description 1
- AMMWFYKTZVIRFN-UHFFFAOYSA-M chembl2028442 Chemical compound [Na+].C1=CC=CC2=C(O)C(N=NC3=C4C=CC(=CC4=C(C=C3O)S([O-])(=O)=O)[N+]([O-])=O)=CC=C21 AMMWFYKTZVIRFN-UHFFFAOYSA-M 0.000 description 1
- 238000013098 chemical test method Methods 0.000 description 1
- 230000001055 chewing effect Effects 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- SOCTUWSJJQCPFX-UHFFFAOYSA-N dichromate(2-) Chemical compound [O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O SOCTUWSJJQCPFX-UHFFFAOYSA-N 0.000 description 1
- FBNOWTWLVCWGCZ-UHFFFAOYSA-L disodium 6-[(5-chloro-2-hydroxy-4-sulfonatophenyl)diazenyl]-5-hydroxynaphthalene-1-sulfonate Chemical compound [Na+].[Na+].Oc1cc(c(Cl)cc1N=Nc1ccc2c(cccc2c1O)S([O-])(=O)=O)S([O-])(=O)=O FBNOWTWLVCWGCZ-UHFFFAOYSA-L 0.000 description 1
- 244000144992 flock Species 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 238000010409 ironing Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000010446 mirabilite Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 description 1
- CGEXUOTXYSGBLV-UHFFFAOYSA-N phenyl benzenesulfonate Chemical compound C=1C=CC=CC=1S(=O)(=O)OC1=CC=CC=C1 CGEXUOTXYSGBLV-UHFFFAOYSA-N 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- ZLMJMSJWJFRBEC-OUBTZVSYSA-N potassium-40 Chemical group [40K] ZLMJMSJWJFRBEC-OUBTZVSYSA-N 0.000 description 1
- XWIJIXWOZCRYEL-UHFFFAOYSA-M potassium;methanesulfonate Chemical compound [K+].CS([O-])(=O)=O XWIJIXWOZCRYEL-UHFFFAOYSA-M 0.000 description 1
- 229940077386 sodium benzenesulfonate Drugs 0.000 description 1
- RSIJVJUOQBWMIM-UHFFFAOYSA-L sodium sulfate decahydrate Chemical compound O.O.O.O.O.O.O.O.O.O.[Na+].[Na+].[O-]S([O-])(=O)=O RSIJVJUOQBWMIM-UHFFFAOYSA-L 0.000 description 1
- VHAXKEBRMSFJMC-UHFFFAOYSA-M sodium;2-methylbenzenesulfonate Chemical compound [Na+].CC1=CC=CC=C1S([O-])(=O)=O VHAXKEBRMSFJMC-UHFFFAOYSA-M 0.000 description 1
- DGXTZMPQSMIFEC-UHFFFAOYSA-M sodium;4-anilinobenzenesulfonate Chemical compound [Na+].C1=CC(S(=O)(=O)[O-])=CC=C1NC1=CC=CC=C1 DGXTZMPQSMIFEC-UHFFFAOYSA-M 0.000 description 1
- MZSDGDXXBZSFTG-UHFFFAOYSA-M sodium;benzenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C1=CC=CC=C1 MZSDGDXXBZSFTG-UHFFFAOYSA-M 0.000 description 1
- RRLOOYQHUHGIRJ-UHFFFAOYSA-M sodium;ethyl sulfate Chemical compound [Na+].CCOS([O-])(=O)=O RRLOOYQHUHGIRJ-UHFFFAOYSA-M 0.000 description 1
- KKVTYAVXTDIPAP-UHFFFAOYSA-M sodium;methanesulfonate Chemical compound [Na+].CS([O-])(=O)=O KKVTYAVXTDIPAP-UHFFFAOYSA-M 0.000 description 1
- HIEHAIZHJZLEPQ-UHFFFAOYSA-M sodium;naphthalene-1-sulfonate Chemical compound [Na+].C1=CC=C2C(S(=O)(=O)[O-])=CC=CC2=C1 HIEHAIZHJZLEPQ-UHFFFAOYSA-M 0.000 description 1
- YNBRSWNUNPAQOF-UHFFFAOYSA-M sodium;phenylmethanesulfonate Chemical compound [Na+].[O-]S(=O)(=O)CC1=CC=CC=C1 YNBRSWNUNPAQOF-UHFFFAOYSA-M 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- IIACRCGMVDHOTQ-UHFFFAOYSA-N sulfamic acid Chemical compound NS(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 description 1
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/046—Material containing basic nitrogen containing amide groups using metallisable or mordant dyes
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752542007 DE2542007C3 (de) | 1975-09-20 | 1975-09-20 | Verfahren zum Färben von natürlichen und synthetischen Polyamidfasern |
| GB3800976A GB1512914A (en) | 1975-09-20 | 1976-09-14 | Process for dyeing natural and synthetic polyamide fibres |
| JP51110951A JPS5838556B2 (ja) | 1975-09-20 | 1976-09-17 | 天燃および合成のポリアミド繊維の染色法 |
| IT2736476A IT1068323B (it) | 1975-09-20 | 1976-09-17 | Procedimento per la tintura di fibre poliammidiche naturali e sintetiche |
| FR7628200A FR2324792A1 (fr) | 1975-09-20 | 1976-09-20 | Procede de teinture de fibres de polyamides naturels et synthetiques |
| BE170767A BE846374A (fr) | 1975-09-20 | 1976-09-20 | Procede de teinture de fibres de polyamides naturels et synthetiques |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752542007 DE2542007C3 (de) | 1975-09-20 | 1975-09-20 | Verfahren zum Färben von natürlichen und synthetischen Polyamidfasern |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2542007A1 DE2542007A1 (de) | 1977-03-24 |
| DE2542007B2 DE2542007B2 (de) | 1978-11-09 |
| DE2542007C3 true DE2542007C3 (de) | 1979-07-12 |
Family
ID=5956990
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752542007 Expired DE2542007C3 (de) | 1975-09-20 | 1975-09-20 | Verfahren zum Färben von natürlichen und synthetischen Polyamidfasern |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS5838556B2 (OSRAM) |
| BE (1) | BE846374A (OSRAM) |
| DE (1) | DE2542007C3 (OSRAM) |
| FR (1) | FR2324792A1 (OSRAM) |
| GB (1) | GB1512914A (OSRAM) |
| IT (1) | IT1068323B (OSRAM) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2821909A1 (de) * | 1978-05-19 | 1979-11-22 | Bayer Ag | Verfahren zum faerben von synthetischen polyamid- und polyurethanfasern |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1469744A1 (de) * | 1965-12-16 | 1968-12-12 | Hoechst Ag | Verfahren zum Faerben von Wolle unterhalb Kochtemperatur mit Saeure- und Chromfarbstoffen |
-
1975
- 1975-09-20 DE DE19752542007 patent/DE2542007C3/de not_active Expired
-
1976
- 1976-09-14 GB GB3800976A patent/GB1512914A/en not_active Expired
- 1976-09-17 JP JP51110951A patent/JPS5838556B2/ja not_active Expired
- 1976-09-17 IT IT2736476A patent/IT1068323B/it active
- 1976-09-20 BE BE170767A patent/BE846374A/xx not_active IP Right Cessation
- 1976-09-20 FR FR7628200A patent/FR2324792A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| FR2324792B1 (OSRAM) | 1982-07-30 |
| BE846374A (fr) | 1977-03-21 |
| IT1068323B (it) | 1985-03-21 |
| FR2324792A1 (fr) | 1977-04-15 |
| DE2542007B2 (de) | 1978-11-09 |
| GB1512914A (en) | 1978-06-01 |
| JPS5838556B2 (ja) | 1983-08-23 |
| JPS5240685A (en) | 1977-03-29 |
| DE2542007A1 (de) | 1977-03-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| C3 | Grant after two publication steps (3rd publication) | ||
| 8381 | Inventor (new situation) |
Free format text: MEIER, GERHARD, 5090 LEVERKUSEN, DE LANGMANN, WERNER, DR., 5000 KOELN, DE |
|
| 8339 | Ceased/non-payment of the annual fee |