DE2527796A1 - Verfahren zur herstellung von tertiaeren phosphinoxiden - Google Patents
Verfahren zur herstellung von tertiaeren phosphinoxidenInfo
- Publication number
- DE2527796A1 DE2527796A1 DE19752527796 DE2527796A DE2527796A1 DE 2527796 A1 DE2527796 A1 DE 2527796A1 DE 19752527796 DE19752527796 DE 19752527796 DE 2527796 A DE2527796 A DE 2527796A DE 2527796 A1 DE2527796 A1 DE 2527796A1
- Authority
- DE
- Germany
- Prior art keywords
- phosphine oxides
- preparation
- quaternary phosphonium
- oxidation
- general formula
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 15
- 238000002360 preparation method Methods 0.000 title claims description 3
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 title description 4
- 229910000073 phosphorus hydride Inorganic materials 0.000 title description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- -1 phosphonium halides Chemical class 0.000 claims description 9
- MPQXHAGKBWFSNV-UHFFFAOYSA-N oxidophosphanium Chemical group [PH3]=O MPQXHAGKBWFSNV-UHFFFAOYSA-N 0.000 claims description 8
- 230000003647 oxidation Effects 0.000 claims description 7
- 238000007254 oxidation reaction Methods 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 4
- 238000010521 absorption reaction Methods 0.000 claims description 2
- 239000003570 air Substances 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 2
- 125000003118 aryl group Chemical group 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 150000001649 bromium compounds Chemical class 0.000 claims description 2
- 150000001805 chlorine compounds Chemical class 0.000 claims description 2
- 125000005843 halogen group Chemical group 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000007800 oxidant agent Substances 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 description 4
- 229910052698 phosphorus Inorganic materials 0.000 description 4
- 239000011574 phosphorus Substances 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- LRMLWYXJORUTBG-UHFFFAOYSA-N dimethylphosphorylmethane Chemical compound CP(C)(C)=O LRMLWYXJORUTBG-UHFFFAOYSA-N 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- NJFUXFRJVIXVSG-UHFFFAOYSA-M tetramethylphosphanium;chloride Chemical compound [Cl-].C[P+](C)(C)C NJFUXFRJVIXVSG-UHFFFAOYSA-M 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- BXYHVFRRNNWPMB-UHFFFAOYSA-N tetramethylphosphanium Chemical compound C[P+](C)(C)C BXYHVFRRNNWPMB-UHFFFAOYSA-N 0.000 description 2
- YCANCZRRZBHLEN-UHFFFAOYSA-N [N].O Chemical compound [N].O YCANCZRRZBHLEN-UHFFFAOYSA-N 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 238000005904 alkaline hydrolysis reaction Methods 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- USJRLGNYCQWLPF-UHFFFAOYSA-N chlorophosphane Chemical group ClP USJRLGNYCQWLPF-UHFFFAOYSA-N 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 150000002902 organometallic compounds Chemical class 0.000 description 1
- 150000002903 organophosphorus compounds Chemical class 0.000 description 1
- DJFBJKSMACBYBD-UHFFFAOYSA-N phosphane;hydrate Chemical group O.P DJFBJKSMACBYBD-UHFFFAOYSA-N 0.000 description 1
- 150000003003 phosphines Chemical group 0.000 description 1
- 239000004476 plant protection product Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000011814 protection agent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 238000002411 thermogravimetry Methods 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752527796 DE2527796A1 (de) | 1975-06-21 | 1975-06-21 | Verfahren zur herstellung von tertiaeren phosphinoxiden |
| CH613176A CH599238A5 (US06486227-20021126-C00005.png) | 1975-06-21 | 1976-05-17 | |
| GB21649/76A GB1499492A (en) | 1975-06-21 | 1976-05-25 | Production of tertiary phosphine oxides |
| CA253,977A CA1072983A (en) | 1975-06-21 | 1976-06-03 | Production of tertiary phosphine oxides |
| JP51071659A JPS523022A (en) | 1975-06-21 | 1976-06-17 | Process for manufacturing tertiary phosphine oxides |
| US05/696,921 US4096189A (en) | 1975-06-21 | 1976-06-17 | Production of tertiary phosphine oxides |
| NL7606651A NL7606651A (nl) | 1975-06-21 | 1976-06-18 | Werkwijze voor de bereiding van tertiaire fosfienoxyden. |
| IT49989/76A IT1061692B (it) | 1975-06-21 | 1976-06-18 | Procedimento per produrre ossidi fosfinici terziari |
| BE168135A BE843197A (fr) | 1975-06-21 | 1976-06-21 | Procede de preparation d'oxydes de phosphines tertiaires |
| FR7618829A FR2316244A1 (fr) | 1975-06-21 | 1976-06-21 | Procede de preparation d'oxydes de phosphines tertiaires |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752527796 DE2527796A1 (de) | 1975-06-21 | 1975-06-21 | Verfahren zur herstellung von tertiaeren phosphinoxiden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2527796A1 true DE2527796A1 (de) | 1976-12-30 |
Family
ID=5949677
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752527796 Withdrawn DE2527796A1 (de) | 1975-06-21 | 1975-06-21 | Verfahren zur herstellung von tertiaeren phosphinoxiden |
Country Status (10)
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0062024A1 (en) * | 1981-02-09 | 1982-10-06 | FMC Corporation | Method of oxidizing tertiary phosphines |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5153502A (en) * | 1974-11-05 | 1976-05-12 | Kogyo Gijutsuin | Sekyukeijushitsuyu omochiiru sekitanno ekitaikaho |
| US4487968A (en) * | 1982-06-28 | 1984-12-11 | Fmc Corporation | Production of tertiary haloalkylphosphine oxides |
| JPS60185838A (ja) * | 1984-03-01 | 1985-09-21 | ユニチカ株式会社 | 加工糸織物の製織方法 |
| DE3737938A1 (de) * | 1987-11-07 | 1989-05-18 | Hoechst Ag | Verfahren zur herstellung von tertiaeren phosphanoxiden |
| DE10343377B3 (de) † | 2003-09-17 | 2005-04-28 | Groz Beckert Kg | Schaftantrieb für Webmaschinenschäfte |
| JP5496027B2 (ja) | 2010-09-09 | 2014-05-21 | 日立オートモティブシステムズ株式会社 | 熱式空気流量計 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1050506A (US06486227-20021126-C00005.png) * | 1963-12-09 | |||
| US3520939A (en) * | 1968-04-18 | 1970-07-21 | Monsanto Co | Process for preparing phosphine oxides |
| US3784638A (en) * | 1969-12-24 | 1974-01-08 | Polaroid Corp | Preparation of tertiary organo-phosphine oxides |
| US3751482A (en) * | 1971-12-01 | 1973-08-07 | Union Carbide Corp | Process for the production of tertiary phosphine oxides |
-
1975
- 1975-06-21 DE DE19752527796 patent/DE2527796A1/de not_active Withdrawn
-
1976
- 1976-05-17 CH CH613176A patent/CH599238A5/xx not_active IP Right Cessation
- 1976-05-25 GB GB21649/76A patent/GB1499492A/en not_active Expired
- 1976-06-03 CA CA253,977A patent/CA1072983A/en not_active Expired
- 1976-06-17 US US05/696,921 patent/US4096189A/en not_active Expired - Lifetime
- 1976-06-17 JP JP51071659A patent/JPS523022A/ja active Pending
- 1976-06-18 IT IT49989/76A patent/IT1061692B/it active
- 1976-06-18 NL NL7606651A patent/NL7606651A/xx not_active Application Discontinuation
- 1976-06-21 FR FR7618829A patent/FR2316244A1/fr active Granted
- 1976-06-21 BE BE168135A patent/BE843197A/xx not_active IP Right Cessation
Non-Patent Citations (1)
| Title |
|---|
| NICHTS-ERMITTELT * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0062024A1 (en) * | 1981-02-09 | 1982-10-06 | FMC Corporation | Method of oxidizing tertiary phosphines |
Also Published As
| Publication number | Publication date |
|---|---|
| CH599238A5 (US06486227-20021126-C00005.png) | 1978-05-31 |
| US4096189A (en) | 1978-06-20 |
| IT1061692B (it) | 1983-04-30 |
| JPS523022A (en) | 1977-01-11 |
| BE843197A (fr) | 1976-12-21 |
| NL7606651A (nl) | 1976-12-23 |
| FR2316244A1 (fr) | 1977-01-28 |
| FR2316244B1 (US06486227-20021126-C00005.png) | 1981-05-29 |
| GB1499492A (en) | 1978-02-01 |
| CA1072983A (en) | 1980-03-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| 8130 | Withdrawal |