DE2515370C3 - Verfahren zur Herstellung von Maddrellschem Salz - Google Patents
Verfahren zur Herstellung von Maddrellschem SalzInfo
- Publication number
- DE2515370C3 DE2515370C3 DE2515370A DE2515370A DE2515370C3 DE 2515370 C3 DE2515370 C3 DE 2515370C3 DE 2515370 A DE2515370 A DE 2515370A DE 2515370 A DE2515370 A DE 2515370A DE 2515370 C3 DE2515370 C3 DE 2515370C3
- Authority
- DE
- Germany
- Prior art keywords
- salt
- maddrell
- water
- production
- orthophosphate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 9
- 238000000034 method Methods 0.000 title description 21
- 235000019983 sodium metaphosphate Nutrition 0.000 title description 15
- AQMNWCRSESPIJM-UHFFFAOYSA-M sodium metaphosphate Chemical compound [Na+].[O-]P(=O)=O AQMNWCRSESPIJM-UHFFFAOYSA-M 0.000 title description 14
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 14
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 7
- 150000003839 salts Chemical class 0.000 claims description 6
- 235000019820 disodium diphosphate Nutrition 0.000 claims description 3
- GYQBBRRVRKFJRG-UHFFFAOYSA-L disodium pyrophosphate Chemical compound [Na+].[Na+].OP([O-])(=O)OP(O)([O-])=O GYQBBRRVRKFJRG-UHFFFAOYSA-L 0.000 claims description 3
- 229940038485 disodium pyrophosphate Drugs 0.000 claims description 3
- 229910019142 PO4 Inorganic materials 0.000 claims 1
- 238000010348 incorporation Methods 0.000 claims 1
- 235000021317 phosphate Nutrition 0.000 claims 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 239000000203 mixture Substances 0.000 description 9
- 239000000047 product Substances 0.000 description 7
- 238000000227 grinding Methods 0.000 description 6
- DZHMRSPXDUUJER-UHFFFAOYSA-N [amino(hydroxy)methylidene]azanium;dihydrogen phosphate Chemical compound NC(N)=O.OP(O)(O)=O DZHMRSPXDUUJER-UHFFFAOYSA-N 0.000 description 4
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 description 4
- 150000003016 phosphoric acids Chemical class 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- 238000001354 calcination Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
- ZRIUUUJAJJNDSS-UHFFFAOYSA-N ammonium phosphates Chemical class [NH4+].[NH4+].[NH4+].[O-]P([O-])([O-])=O ZRIUUUJAJJNDSS-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000004202 carbamide Substances 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 238000011417 postcuring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000000606 toothpaste Substances 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 239000004254 Ammonium phosphate Substances 0.000 description 1
- 239000004114 Ammonium polyphosphate Substances 0.000 description 1
- 239000005696 Diammonium phosphate Substances 0.000 description 1
- KJNJCRABCUHOJK-UHFFFAOYSA-N [Pb].[P] Chemical compound [Pb].[P] KJNJCRABCUHOJK-UHFFFAOYSA-N 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- VFTOLAKHPLTCIF-UHFFFAOYSA-N aminoazanium;dihydrogen phosphate Chemical compound NN.OP(O)(O)=O VFTOLAKHPLTCIF-UHFFFAOYSA-N 0.000 description 1
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 description 1
- 235000019289 ammonium phosphates Nutrition 0.000 description 1
- 235000019826 ammonium polyphosphate Nutrition 0.000 description 1
- 229920001276 ammonium polyphosphate Polymers 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- CEDDGDWODCGBFQ-UHFFFAOYSA-N carbamimidoylazanium;hydron;phosphate Chemical compound NC(N)=N.OP(O)(O)=O CEDDGDWODCGBFQ-UHFFFAOYSA-N 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- -1 compounds sodium trimetaphosphate Chemical class 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 1
- 235000019838 diammonium phosphate Nutrition 0.000 description 1
- 229910000388 diammonium phosphate Inorganic materials 0.000 description 1
- XPPKVPWEQAFLFU-UHFFFAOYSA-J diphosphate(4-) Chemical compound [O-]P([O-])(=O)OP([O-])([O-])=O XPPKVPWEQAFLFU-UHFFFAOYSA-J 0.000 description 1
- 235000011180 diphosphates Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- RBLWMQWAHONKNC-UHFFFAOYSA-N hydroxyazanium Chemical compound O[NH3+] RBLWMQWAHONKNC-UHFFFAOYSA-N 0.000 description 1
- XBUFCZMOAHHGMX-UHFFFAOYSA-N hydroxylamine;phosphoric acid Chemical compound ON.ON.ON.OP(O)(O)=O XBUFCZMOAHHGMX-UHFFFAOYSA-N 0.000 description 1
- 150000002605 large molecules Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 235000019837 monoammonium phosphate Nutrition 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 238000005453 pelletization Methods 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- XFZRQAZGUOTJCS-UHFFFAOYSA-N phosphoric acid;1,3,5-triazine-2,4,6-triamine Chemical compound OP(O)(O)=O.NC1=NC(N)=NC(N)=N1 XFZRQAZGUOTJCS-UHFFFAOYSA-N 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/38—Condensed phosphates
- C01B25/44—Metaphosphates
- C01B25/445—Metaphosphates of alkali metals
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- Organic Chemistry (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cosmetics (AREA)
- Catalysts (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Priority Applications (12)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2515370A DE2515370C3 (de) | 1975-04-09 | 1975-04-09 | Verfahren zur Herstellung von Maddrellschem Salz |
| IT20002/76A IT1055153B (it) | 1975-04-09 | 1976-02-09 | Processo per la preparazione di sale di maddrell |
| SE7601701A SE413664B (sv) | 1975-04-09 | 1976-02-16 | Sett att framstella maddrells salt |
| NLAANVRAGE7603139,A NL180404C (nl) | 1975-04-09 | 1976-03-25 | Werkwijze ter bereiding van maddrell's zout. |
| ES446408A ES446408A1 (es) | 1975-04-09 | 1976-03-26 | Procedimiento para la preparacion de sal de maddrell. |
| AT241276A AT353747B (de) | 1975-04-09 | 1976-04-02 | Verfahren zur herstellung von maddrell'schem salz |
| CH431276A CH618947A5 (https=) | 1975-04-09 | 1976-04-06 | |
| US05/674,123 US4029742A (en) | 1975-04-09 | 1976-04-06 | Process of producing Maddrell salt |
| GB14187/76A GB1492006A (en) | 1975-04-09 | 1976-04-07 | Process for the production of maddrell's salt |
| DD192272A DD123593A5 (https=) | 1975-04-09 | 1976-04-08 | |
| FR7610258A FR2306938A1 (fr) | 1975-04-09 | 1976-04-08 | Procede de preparation du sel de maddrell |
| BE166025A BE840596A (fr) | 1975-04-09 | 1976-04-09 | Procede de preparation de sel de maddrell, et sel de maddrell ainsi prepare |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2515370A DE2515370C3 (de) | 1975-04-09 | 1975-04-09 | Verfahren zur Herstellung von Maddrellschem Salz |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2515370A1 DE2515370A1 (de) | 1976-10-14 |
| DE2515370B2 DE2515370B2 (de) | 1978-04-06 |
| DE2515370C3 true DE2515370C3 (de) | 1978-11-30 |
Family
ID=5943359
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2515370A Expired DE2515370C3 (de) | 1975-04-09 | 1975-04-09 | Verfahren zur Herstellung von Maddrellschem Salz |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US4029742A (https=) |
| AT (1) | AT353747B (https=) |
| BE (1) | BE840596A (https=) |
| CH (1) | CH618947A5 (https=) |
| DD (1) | DD123593A5 (https=) |
| DE (1) | DE2515370C3 (https=) |
| ES (1) | ES446408A1 (https=) |
| FR (1) | FR2306938A1 (https=) |
| GB (1) | GB1492006A (https=) |
| IT (1) | IT1055153B (https=) |
| NL (1) | NL180404C (https=) |
| SE (1) | SE413664B (https=) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3543394A1 (de) * | 1985-12-07 | 1987-06-11 | Benckiser Knapsack Gmbh | Verfahren zur herstellung von maddrellschem salz, sowie natriumdihydrogenphosphat, enthaltend 0,05 - 2,5 mol% phosphorsaeure oder ammoniumphosphat in statistischer verteilung |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4162300A (en) * | 1976-04-15 | 1979-07-24 | Hoechst Aktiengesellschaft | Production of Maddrell salt |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1050908B (https=) * | 1959-02-19 | |||
| US3230041A (en) * | 1962-11-29 | 1966-01-18 | Monsanto Co | Method for making tetra-alkali metal pyrophosphate |
-
1975
- 1975-04-09 DE DE2515370A patent/DE2515370C3/de not_active Expired
-
1976
- 1976-02-09 IT IT20002/76A patent/IT1055153B/it active
- 1976-02-16 SE SE7601701A patent/SE413664B/xx not_active IP Right Cessation
- 1976-03-25 NL NLAANVRAGE7603139,A patent/NL180404C/xx not_active IP Right Cessation
- 1976-03-26 ES ES446408A patent/ES446408A1/es not_active Expired
- 1976-04-02 AT AT241276A patent/AT353747B/de not_active IP Right Cessation
- 1976-04-06 US US05/674,123 patent/US4029742A/en not_active Expired - Lifetime
- 1976-04-06 CH CH431276A patent/CH618947A5/de not_active IP Right Cessation
- 1976-04-07 GB GB14187/76A patent/GB1492006A/en not_active Expired
- 1976-04-08 FR FR7610258A patent/FR2306938A1/fr active Granted
- 1976-04-08 DD DD192272A patent/DD123593A5/xx unknown
- 1976-04-09 BE BE166025A patent/BE840596A/xx not_active IP Right Cessation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3543394A1 (de) * | 1985-12-07 | 1987-06-11 | Benckiser Knapsack Gmbh | Verfahren zur herstellung von maddrellschem salz, sowie natriumdihydrogenphosphat, enthaltend 0,05 - 2,5 mol% phosphorsaeure oder ammoniumphosphat in statistischer verteilung |
Also Published As
| Publication number | Publication date |
|---|---|
| NL180404C (nl) | 1987-02-16 |
| NL7603139A (nl) | 1976-10-12 |
| SE413664B (sv) | 1980-06-16 |
| FR2306938B1 (https=) | 1979-05-04 |
| IT1055153B (it) | 1981-12-21 |
| FR2306938A1 (fr) | 1976-11-05 |
| SE7601701L (sv) | 1976-10-10 |
| DE2515370B2 (de) | 1978-04-06 |
| DE2515370A1 (de) | 1976-10-14 |
| CH618947A5 (https=) | 1980-08-29 |
| BE840596A (fr) | 1976-08-02 |
| GB1492006A (en) | 1977-11-16 |
| DD123593A5 (https=) | 1977-01-05 |
| US4029742A (en) | 1977-06-14 |
| ES446408A1 (es) | 1977-06-16 |
| AT353747B (de) | 1979-11-26 |
| NL180404B (nl) | 1986-09-16 |
| ATA241276A (de) | 1979-05-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) |