DE2501630C2 - Verfahren zur Herstellung von Vinylchlorid-Polymeren - Google Patents
Verfahren zur Herstellung von Vinylchlorid-PolymerenInfo
- Publication number
- DE2501630C2 DE2501630C2 DE2501630A DE2501630A DE2501630C2 DE 2501630 C2 DE2501630 C2 DE 2501630C2 DE 2501630 A DE2501630 A DE 2501630A DE 2501630 A DE2501630 A DE 2501630A DE 2501630 C2 DE2501630 C2 DE 2501630C2
- Authority
- DE
- Germany
- Prior art keywords
- homogenization
- polymerization
- vinyl chloride
- polymerized
- initiator
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 34
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 title claims description 15
- 229920000642 polymer Polymers 0.000 title claims description 13
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000000265 homogenisation Methods 0.000 claims description 23
- 238000006116 polymerization reaction Methods 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 239000000463 material Substances 0.000 claims description 18
- 239000006185 dispersion Substances 0.000 claims description 16
- 239000003999 initiator Substances 0.000 claims description 15
- 239000000178 monomer Substances 0.000 claims description 11
- 239000002904 solvent Substances 0.000 claims description 10
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 230000001804 emulsifying effect Effects 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- 239000000375 suspending agent Substances 0.000 claims description 7
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 6
- 239000003995 emulsifying agent Substances 0.000 claims description 5
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 claims description 4
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 4
- 125000001931 aliphatic group Chemical group 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 238000009826 distribution Methods 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 150000003254 radicals Chemical class 0.000 claims description 3
- 239000008096 xylene Substances 0.000 claims description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 2
- 125000002015 acyclic group Chemical group 0.000 claims description 2
- 125000003118 aryl group Chemical group 0.000 claims description 2
- 239000000084 colloidal system Substances 0.000 claims description 2
- 229930195733 hydrocarbon Natural products 0.000 claims description 2
- 150000002576 ketones Chemical class 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- 239000000725 suspension Substances 0.000 claims description 2
- 238000005266 casting Methods 0.000 claims 2
- 230000000379 polymerizing effect Effects 0.000 claims 2
- 238000002360 preparation method Methods 0.000 claims 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims 2
- 229920002554 vinyl polymer Polymers 0.000 claims 2
- 102000007469 Actins Human genes 0.000 claims 1
- 108010085238 Actins Proteins 0.000 claims 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims 1
- 230000032683 aging Effects 0.000 claims 1
- 238000000137 annealing Methods 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 150000001805 chlorine compounds Chemical class 0.000 claims 1
- 238000000576 coating method Methods 0.000 claims 1
- 238000004512 die casting Methods 0.000 claims 1
- 238000007598 dipping method Methods 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- 239000006260 foam Substances 0.000 claims 1
- 150000002430 hydrocarbons Chemical class 0.000 claims 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- 238000001746 injection moulding Methods 0.000 claims 1
- 239000004014 plasticizer Substances 0.000 claims 1
- 238000001175 rotational moulding Methods 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
- 238000005507 spraying Methods 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 description 8
- -1 pentane Chemical class 0.000 description 6
- 239000011734 sodium Substances 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000004816 latex Substances 0.000 description 4
- 229920000126 latex Polymers 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 125000000129 anionic group Chemical group 0.000 description 3
- BEQKKZICTDFVMG-UHFFFAOYSA-N 1,2,3,4,6-pentaoxepane-5,7-dione Chemical compound O=C1OOOOC(=O)O1 BEQKKZICTDFVMG-UHFFFAOYSA-N 0.000 description 2
- YIVJZNGAASQVEM-UHFFFAOYSA-N Lauroyl peroxide Chemical compound CCCCCCCCCCCC(=O)OOC(=O)CCCCCCCCCCC YIVJZNGAASQVEM-UHFFFAOYSA-N 0.000 description 2
- RDOXTESZEPMUJZ-UHFFFAOYSA-N anisole Chemical compound COC1=CC=CC=C1 RDOXTESZEPMUJZ-UHFFFAOYSA-N 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000011010 flushing procedure Methods 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- CBFCDTFDPHXCNY-UHFFFAOYSA-N icosane Chemical compound CCCCCCCCCCCCCCCCCCCC CBFCDTFDPHXCNY-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- PCJGHYSTCBLKIA-UHFFFAOYSA-N (1-acetylcyclohexyl)sulfonyloxy 1-acetylcyclohexane-1-sulfonate Chemical compound C1CCCCC1(C(C)=O)S(=O)(=O)OOS(=O)(=O)C1(C(=O)C)CCCCC1 PCJGHYSTCBLKIA-UHFFFAOYSA-N 0.000 description 1
- LGJCFVYMIJLQJO-UHFFFAOYSA-N 1-dodecylperoxydodecane Chemical compound CCCCCCCCCCCCOOCCCCCCCCCCCC LGJCFVYMIJLQJO-UHFFFAOYSA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 150000008055 alkyl aryl sulfonates Chemical class 0.000 description 1
- 150000001555 benzenes Chemical class 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- PUBNPKMXGRPTQT-UHFFFAOYSA-N decyl benzenesulfonate Chemical compound CCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 PUBNPKMXGRPTQT-UHFFFAOYSA-N 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 239000002283 diesel fuel Substances 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- YRIUSKIDOIARQF-UHFFFAOYSA-N dodecyl benzenesulfonate Chemical compound CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 YRIUSKIDOIARQF-UHFFFAOYSA-N 0.000 description 1
- 229940071161 dodecylbenzenesulfonate Drugs 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- QWVBGCWRHHXMRM-UHFFFAOYSA-N hexadecoxycarbonyloxy hexadecyl carbonate Chemical compound CCCCCCCCCCCCCCCCOC(=O)OOC(=O)OCCCCCCCCCCCCCCCC QWVBGCWRHHXMRM-UHFFFAOYSA-N 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- UZKWTJUDCOPSNM-UHFFFAOYSA-N methoxybenzene Substances CCCCOC=C UZKWTJUDCOPSNM-UHFFFAOYSA-N 0.000 description 1
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003505 polymerization initiator Substances 0.000 description 1
- 229920002689 polyvinyl acetate Polymers 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 description 1
- 150000003738 xylenes Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F14/02—Monomers containing chlorine
- C08F14/04—Monomers containing two carbon atoms
- C08F14/06—Vinyl chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
- Paints Or Removers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3100/74A GB1492028A (en) | 1974-01-23 | 1974-01-23 | Vinyl chloride polymerisation process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2501630A1 DE2501630A1 (de) | 1975-07-24 |
| DE2501630C2 true DE2501630C2 (de) | 1985-01-10 |
Family
ID=9751943
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2501630A Expired DE2501630C2 (de) | 1974-01-23 | 1975-01-16 | Verfahren zur Herstellung von Vinylchlorid-Polymeren |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US3974133A (en, 2012) |
| JP (1) | JPS58454B2 (en, 2012) |
| AT (1) | AT332646B (en, 2012) |
| BE (1) | BE824678A (en, 2012) |
| BR (1) | BR7500418A (en, 2012) |
| DE (1) | DE2501630C2 (en, 2012) |
| ES (1) | ES434077A1 (en, 2012) |
| FR (1) | FR2258404B1 (en, 2012) |
| GB (1) | GB1492028A (en, 2012) |
| IT (1) | IT1028357B (en, 2012) |
| NL (1) | NL7500256A (en, 2012) |
| NO (1) | NO141995C (en, 2012) |
| SE (1) | SE408427B (en, 2012) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4081588A (en) * | 1973-06-08 | 1978-03-28 | Imperial Chemical Industries Limited | Vinyl chloride polymerization process |
| US4093581A (en) * | 1976-11-11 | 1978-06-06 | Stauffer Chemical Company | Emulsion polymerization of vinyl chloride using prehomogenized mixed emulsifier system |
| JPS5916562B2 (ja) * | 1978-05-23 | 1984-04-16 | 日本ゼオン株式会社 | 塩化ビニルの重合方法 |
| NO145164C (no) * | 1978-11-06 | 1982-01-27 | Sintef | Fremgangsmaate for fremstilling av polymerlateks. |
| DE3120708A1 (de) * | 1981-05-25 | 1982-12-09 | Basf Ag, 6700 Ludwigshafen | Verfahren zur diskontinuierlichen polymerisation von vinylchlorid |
| US4500649A (en) * | 1981-10-12 | 1985-02-19 | Wako Pure Chemical Industries, Ltd. | Process for producing aqueous suspension containing organic azo compound as polymerization initiator |
| JPS6015405A (ja) * | 1983-07-07 | 1985-01-26 | Wako Pure Chem Ind Ltd | アゾ系重合開始剤捏和体 |
| DE3343766A1 (de) * | 1983-12-03 | 1985-06-13 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von verpastbaren vinylchloridpolymerisaten |
| JP2501322B2 (ja) * | 1986-08-07 | 1996-05-29 | 東ソー株式会社 | 重合方法 |
| AU642072B2 (en) * | 1991-03-01 | 1993-10-07 | B.F. Goodrich Company, The | High melt flow crosslinked PVC resin, compound, and articles derived therefrom |
| DE4443752A1 (de) * | 1994-12-08 | 1996-06-13 | Vinnolit Kunststoff Gmbh | Verfahren zur radikalischen Polymerisation ethylenisch ungesättigter Monomere in wäßrigem Medium |
| JP2002020407A (ja) * | 2000-07-05 | 2002-01-23 | Kanegafuchi Chem Ind Co Ltd | 塩化ビニル系ペースト樹脂の製造方法 |
| CN102952228A (zh) * | 2011-08-26 | 2013-03-06 | 沈阳化工股份有限公司 | 一种提高糊树脂生产效率的制备方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB978875A (en, 2012) * | 1963-03-29 | Ici Ltd | ||
| GB1102980A (en) * | 1966-01-31 | 1968-02-14 | Kanegafuchi Chemical Ind | Improvements in and relating to the preparation of vinyl chloride polymers |
-
1974
- 1974-01-23 GB GB3100/74A patent/GB1492028A/en not_active Expired
-
1975
- 1975-01-08 US US05/539,385 patent/US3974133A/en not_active Expired - Lifetime
- 1975-01-09 NL NL7500256A patent/NL7500256A/xx not_active Application Discontinuation
- 1975-01-10 NO NO750065A patent/NO141995C/no unknown
- 1975-01-14 IT IT7519256A patent/IT1028357B/it active
- 1975-01-16 DE DE2501630A patent/DE2501630C2/de not_active Expired
- 1975-01-20 FR FR7501598A patent/FR2258404B1/fr not_active Expired
- 1975-01-22 SE SE7500671A patent/SE408427B/xx not_active IP Right Cessation
- 1975-01-22 AT AT46375*#A patent/AT332646B/de not_active IP Right Cessation
- 1975-01-22 BR BR418/75A patent/BR7500418A/pt unknown
- 1975-01-23 ES ES434077A patent/ES434077A1/es not_active Expired
- 1975-01-23 JP JP50010122A patent/JPS58454B2/ja not_active Expired
- 1975-01-23 BE BE152621A patent/BE824678A/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| GB1492028A (en) | 1977-11-16 |
| JPS50104288A (en, 2012) | 1975-08-18 |
| FR2258404A1 (en, 2012) | 1975-08-18 |
| NO141995C (no) | 1980-06-11 |
| ATA46375A (de) | 1976-01-15 |
| SE408427B (sv) | 1979-06-11 |
| BR7500418A (pt) | 1975-11-04 |
| ES434077A1 (es) | 1976-12-16 |
| NL7500256A (nl) | 1975-07-25 |
| BE824678A (fr) | 1975-07-23 |
| FR2258404B1 (en, 2012) | 1979-06-08 |
| NO750065L (en, 2012) | 1975-08-18 |
| DE2501630A1 (de) | 1975-07-24 |
| NO141995B (no) | 1980-03-03 |
| US3974133A (en) | 1976-08-10 |
| AT332646B (de) | 1976-10-11 |
| SE7500671L (en, 2012) | 1975-07-24 |
| IT1028357B (it) | 1979-01-30 |
| JPS58454B2 (ja) | 1983-01-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: EUROPEAN VINYLS CORP. (TECHNOLOGY) AG, ZUG, CH |
|
| 8328 | Change in the person/name/address of the agent |
Free format text: STOLBERG-WERNIGERODE, GRAF ZU, U., DIPL.-CHEM. DR.RER.NAT. SUCHANTKE, J., DIPL.-ING. HUBER, A., DIPL.-ING. VON KAMEKE, A., DIPL.-CHEM. DR.RER.NAT. VOELKER, I., DIPL.-BIOL. FRANCK, P., DIPL.-CHEM.ETH DR.SC.TECHN. BOTH, G., DIPL.-PHYS. DR.RER.NAT., PAT.-ANWAELTE, 2000 HAMBURG |