DE250075C - - Google Patents
Info
- Publication number
- DE250075C DE250075C DENDAT250075D DE250075DA DE250075C DE 250075 C DE250075 C DE 250075C DE NDAT250075 D DENDAT250075 D DE NDAT250075D DE 250075D A DE250075D A DE 250075DA DE 250075 C DE250075 C DE 250075C
- Authority
- DE
- Germany
- Prior art keywords
- oxanthrone
- water
- halogen
- anthracene
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 229910052736 halogen Inorganic materials 0.000 claims description 8
- 150000002367 halogens Chemical class 0.000 claims description 8
- BJOAMCSNLUKBSK-UHFFFAOYSA-N 2h-dibenzo-p-dioxin-1-one Chemical compound O1C2=CC=CC=C2OC2=C1C(=O)CC=C2 BJOAMCSNLUKBSK-UHFFFAOYSA-N 0.000 claims description 7
- 239000003125 aqueous solvent Substances 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 150000001298 alcohols Chemical class 0.000 claims description 2
- -1 oxanthrone ethers Chemical class 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims 2
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 238000012986 modification Methods 0.000 claims 1
- 230000004048 modification Effects 0.000 claims 1
- 238000006467 substitution reaction Methods 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- PCFMUWBCZZUMRX-UHFFFAOYSA-N 9,10-Dihydroxyanthracene Chemical compound C1=CC=C2C(O)=C(C=CC=C3)C3=C(O)C2=C1 PCFMUWBCZZUMRX-UHFFFAOYSA-N 0.000 description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- AUKRYONWZHRJRE-UHFFFAOYSA-N 9-anthrol Chemical compound C1=CC=C2C(O)=C(C=CC=C3)C3=CC2=C1 AUKRYONWZHRJRE-UHFFFAOYSA-N 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 229960000583 acetic acid Drugs 0.000 description 3
- 239000012362 glacial acetic acid Substances 0.000 description 3
- NGGBYCPITQNVGN-UHFFFAOYSA-N 1-chloro-10h-anthracen-9-one Chemical compound C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2Cl NGGBYCPITQNVGN-UHFFFAOYSA-N 0.000 description 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 description 2
- 150000004056 anthraquinones Chemical class 0.000 description 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 2
- 229910052794 bromium Inorganic materials 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000012433 hydrogen halide Substances 0.000 description 2
- 229910000039 hydrogen halide Inorganic materials 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- FHYCCEAXIHMYHZ-UHFFFAOYSA-N 1-methoxy-10h-anthracen-9-one Chemical compound C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2OC FHYCCEAXIHMYHZ-UHFFFAOYSA-N 0.000 description 1
- VXADJQKRUPSPNZ-UHFFFAOYSA-N 2-chloroanthracen-1-ol Chemical compound C1=CC=C2C=C3C(O)=C(Cl)C=CC3=CC2=C1 VXADJQKRUPSPNZ-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 1
- SOIJWBIPWKSGET-UHFFFAOYSA-N anthracene;dihydrochloride Chemical compound Cl.Cl.C1=CC=CC2=CC3=CC=CC=C3C=C21 SOIJWBIPWKSGET-UHFFFAOYSA-N 0.000 description 1
- QGJOPFRUJISHPQ-NJFSPNSNSA-N carbon disulfide-14c Chemical compound S=[14C]=S QGJOPFRUJISHPQ-NJFSPNSNSA-N 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 125000003963 dichloro group Chemical group Cl* 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/76—Ketones containing a keto group bound to a six-membered aromatic ring
- C07C49/82—Ketones containing a keto group bound to a six-membered aromatic ring containing hydroxy groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE250075C true DE250075C (en:Method) |
Family
ID=508638
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT250075D Active DE250075C (en:Method) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE250075C (en:Method) |
-
0
- DE DENDAT250075D patent/DE250075C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2523696B2 (de) | Verfahren zur kontinuierlichen Herstellung von flüssigen Diglycidyiäthern zweiwertiger Phenole | |
| DE2532477A1 (de) | Verfahren zur entfernung des katalysators aus polyphenylenaethern | |
| DE2013419C3 (de) | Verfahren zum Einarbeiten von wasserunlöslichen, in organischen Lösungsmitteln jedoch löslichen Verbindungen in hydrophile Kollidgießzusammensetzungen für photographische, silberhalogenidhaltige Aufzeichnungsmaterialien | |
| DE1167334B (de) | Verfahren zur Herstellung von hochbasischen, oelloeslichen Metallsulfonaten mehrwertiger Metalle | |
| DE250075C (en:Method) | ||
| DE1928677C3 (de) | Phthalocyaninfarbstoffe und deren Verwendung zum Färben und Bedrucken cellulosehaltiger Materialien | |
| DE2119783A1 (de) | Überzugsmittel sowie Verfahren zu deren Herstellung | |
| DE2001748C3 (de) | Verfahren zur Herstellung von konzentrierten Lösungen kationischer Azofarbstoffe | |
| DE1147481B (de) | Verfahren zur Herstellung photographischer, gelatinehaltiger Halogen-silberemulsionen durch Ausfaellen der Gelatine und des Halogensilbers | |
| DE2157553C3 (de) | Phthalocyaninverbindungen, sie enthaltende Phthalocyaninpigmentgemische und deren Verwendung | |
| DE2906805C3 (de) | Konzentrierte, lagerstabile Lösungen von Kupplungskomponenten für die Eisfarbenfärberei, deren Herstellung und Verwendung | |
| DE1794368B2 (de) | Organische saure Lösungen von basischen Farbstoffen | |
| DE2033989C2 (de) | Lagerstabile konzentrierte Lösungen von Metallkomplexen von Azo- oder Azo-Azomethinfarbstoffen und ihre Verwendung | |
| DE1768725A1 (de) | Anthrachinonfarbstoffe und Verfahren zu deren Herstellung | |
| DE253683C (en:Method) | ||
| AT52528B (de) | Verfahren zur Darstellung eines schwer löslichen Formaldehydzinksulfoxylates. | |
| DE93938C (en:Method) | ||
| DE541714C (de) | Verfahren zur Darstellung neuer Kondensationsprodukte und Lackfarbstoffe der Anthrachinonreihe | |
| DE153861C (en:Method) | ||
| DE98273C (en:Method) | ||
| DE193141C (en:Method) | ||
| DE66361C (de) | Verfahren zur Darstellung eines am Azinstickstoff alkylirten Indulins und von Sulfosäuren desselben | |
| DE208472C (en:Method) | ||
| DE350322C (de) | Verfahren zur Herstellung eines zur Farblackbereitung geeigneten gruenen Farbstoffes | |
| DE589971C (de) | Verfahren zur Herstellung von 4, 8-Dioxy-1, 2, 5, 6-dibenzophenazinen |