DE2449531A1 - Verfahren zum hydrieren von kohle - Google Patents
Verfahren zum hydrieren von kohleInfo
- Publication number
- DE2449531A1 DE2449531A1 DE19742449531 DE2449531A DE2449531A1 DE 2449531 A1 DE2449531 A1 DE 2449531A1 DE 19742449531 DE19742449531 DE 19742449531 DE 2449531 A DE2449531 A DE 2449531A DE 2449531 A1 DE2449531 A1 DE 2449531A1
- Authority
- DE
- Germany
- Prior art keywords
- coal
- hydrogenation
- zone
- hydrogen
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000003245 coal Substances 0.000 title claims description 106
- 238000000034 method Methods 0.000 title claims description 39
- 230000000887 hydrating effect Effects 0.000 title 1
- 239000007789 gas Substances 0.000 claims description 115
- 229910052739 hydrogen Inorganic materials 0.000 claims description 73
- 239000001257 hydrogen Substances 0.000 claims description 67
- 238000005984 hydrogenation reaction Methods 0.000 claims description 66
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 60
- 229930195733 hydrocarbon Natural products 0.000 claims description 33
- 150000002430 hydrocarbons Chemical class 0.000 claims description 33
- 238000006243 chemical reaction Methods 0.000 claims description 30
- 239000007788 liquid Substances 0.000 claims description 26
- 239000003054 catalyst Substances 0.000 claims description 25
- 238000002407 reforming Methods 0.000 claims description 24
- 229910052760 oxygen Inorganic materials 0.000 claims description 23
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 22
- 239000001301 oxygen Substances 0.000 claims description 22
- 229910002091 carbon monoxide Inorganic materials 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 12
- 150000001720 carbohydrates Chemical class 0.000 claims description 11
- 230000015572 biosynthetic process Effects 0.000 claims description 10
- 239000007787 solid Substances 0.000 claims description 10
- 239000011269 tar Substances 0.000 claims description 10
- 150000002431 hydrogen Chemical class 0.000 claims description 7
- 239000004215 Carbon black (E152) Substances 0.000 claims description 5
- 239000000126 substance Substances 0.000 claims description 4
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 3
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000011065 in-situ storage Methods 0.000 claims description 3
- 239000004571 lime Substances 0.000 claims description 3
- 239000000575 pesticide Substances 0.000 claims description 3
- 238000006057 reforming reaction Methods 0.000 claims 2
- 241000607479 Yersinia pestis Species 0.000 claims 1
- 230000005494 condensation Effects 0.000 claims 1
- 238000009833 condensation Methods 0.000 claims 1
- 239000003921 oil Substances 0.000 description 25
- 238000007906 compression Methods 0.000 description 11
- 230000006835 compression Effects 0.000 description 10
- 239000000047 product Substances 0.000 description 10
- 235000014633 carbohydrates Nutrition 0.000 description 9
- 229910052717 sulfur Inorganic materials 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 239000002956 ash Substances 0.000 description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
- 229910052799 carbon Inorganic materials 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- 238000000926 separation method Methods 0.000 description 7
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 5
- 238000010586 diagram Methods 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 5
- 239000011593 sulfur Substances 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- 238000001816 cooling Methods 0.000 description 4
- 238000002309 gasification Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 229910052750 molybdenum Inorganic materials 0.000 description 3
- 239000011733 molybdenum Substances 0.000 description 3
- 239000008188 pellet Substances 0.000 description 3
- 239000003208 petroleum Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000003502 gasoline Substances 0.000 description 2
- 230000008676 import Effects 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- -1 steam Substances 0.000 description 2
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- 235000002918 Fraxinus excelsior Nutrition 0.000 description 1
- YZCKVEUIGOORGS-UHFFFAOYSA-N Hydrogen atom Chemical compound [H] YZCKVEUIGOORGS-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 description 1
- 229940010552 ammonium molybdate Drugs 0.000 description 1
- 235000018660 ammonium molybdate Nutrition 0.000 description 1
- 239000011609 ammonium molybdate Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 239000010883 coal ash Substances 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 229910003439 heavy metal oxide Inorganic materials 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 150000002736 metal compounds Chemical class 0.000 description 1
- 229910052976 metal sulfide Inorganic materials 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000002816 nickel compounds Chemical class 0.000 description 1
- 239000003209 petroleum derivative Substances 0.000 description 1
- 235000021395 porridge Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000011819 refractory material Substances 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000004230 steam cracking Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 239000011289 tar acid Substances 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 239000011135 tin Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/06—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by destructive hydrogenation
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/002—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal in combination with oil conversion- or refining processes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US412026A US3926775A (en) | 1973-11-01 | 1973-11-01 | Hydrogenation of coal |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2449531A1 true DE2449531A1 (de) | 1975-05-07 |
Family
ID=23631268
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19742449531 Withdrawn DE2449531A1 (de) | 1973-11-01 | 1974-10-17 | Verfahren zum hydrieren von kohle |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US3926775A (https=) |
| JP (1) | JPS5743117B2 (https=) |
| CA (1) | CA1030470A (https=) |
| DE (1) | DE2449531A1 (https=) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5344184B2 (https=) * | 1974-10-16 | 1978-11-27 | ||
| US4011153A (en) * | 1975-04-01 | 1977-03-08 | The United States Of America As Represented By The United States Energy Research And Development Administration | Liquefaction and desulfurization of coal using synthesis gas |
| US4007108A (en) * | 1975-06-02 | 1977-02-08 | Arnold Marcel Leas | Converting solid fuels to gaseous and liquid fuels |
| AU517024B2 (en) * | 1976-09-20 | 1981-07-02 | Kobe Steel Limited | Coking low ranking coals |
| US4331530A (en) * | 1978-02-27 | 1982-05-25 | Occidental Research Corporation | Process for the conversion of coal |
| US4226698A (en) * | 1978-08-04 | 1980-10-07 | Schroeder Wilburn C | Ash removal and synthesis gas generation from heavy oils produced by coal hydrogenation |
| US4206033A (en) * | 1978-08-14 | 1980-06-03 | Exxon Research & Engineering Co. | CO2 Pretreatment prevents calcium carbonate formation |
| US4266083A (en) * | 1979-06-08 | 1981-05-05 | The Rust Engineering Company | Biomass liquefaction process |
| US4366045A (en) * | 1980-01-22 | 1982-12-28 | Rollan Swanson | Process for conversion of coal to gaseous hydrocarbons |
| DE3114766A1 (de) * | 1980-04-15 | 1982-06-16 | Rollan Dr. 89316 Eureka Nev. Swanson | Verfahren zum umwandeln von kohle oder torf in gasfoermige kohlenwasserstoffe oder fluechtige destillate oder gemische hiervon |
| EP0093501B1 (en) * | 1982-03-29 | 1988-07-13 | Asahi Kasei Kogyo Kabushiki Kaisha | Process for thermal cracking of carbonaceous substances which increases gasoline fraction and light oil conversions |
| JPS5936191A (ja) * | 1982-08-24 | 1984-02-28 | Asahi Chem Ind Co Ltd | 炭素質物質の処理方法 |
| JPS59124990A (ja) * | 1983-01-04 | 1984-07-19 | Asahi Chem Ind Co Ltd | 石炭の水添熱分解法 |
| US4468316A (en) * | 1983-03-03 | 1984-08-28 | Chemroll Enterprises, Inc. | Hydrogenation of asphaltenes and the like |
| DE3322784A1 (de) * | 1983-06-24 | 1985-01-03 | Ruhrkohle Ag, 4300 Essen | Verfahren zur behandlung von prozessabwaessern und abwaessern bei der hydrierung von kohle |
| US4578175A (en) * | 1984-04-02 | 1986-03-25 | Conoco Inc. | Combined process for coal pyrolysis and char gasification |
| EP0177676B1 (de) * | 1984-09-13 | 1992-03-04 | Ruhrkohle Aktiengesellschaft | Verfahren zur Prozesseinstellung mit Wärmerückgewinnung für die Sumpfphasehydrierung mit integrierter Gasphasehydrierung |
| DE3438606A1 (de) * | 1984-10-20 | 1986-04-24 | Ruhrkohle Ag, 4300 Essen | Verfahren fuer mehrphasen-reaktoren mit exothermer waermetoenung, speziell fuer hydrierreaktoren in der sumpfphase |
| JP3198306B2 (ja) | 1999-08-19 | 2001-08-13 | 経済産業省産業技術総合研究所長 | 低品位炭の改質方法 |
| CN1642851B (zh) * | 2002-02-05 | 2010-04-14 | 加利福尼亚大学董事会 | 采用自支持加氢气化从含碳材料制备合成运输燃料 |
| US8603430B2 (en) * | 2002-02-05 | 2013-12-10 | The Regents Of The University Of California | Controlling the synthesis gas composition of a steam methane reformer |
| US20080021119A1 (en) * | 2006-07-18 | 2008-01-24 | Norbeck Joseph M | Operation of a steam methane reformer by direct feeding of steam rich producer gas from steam hydro-gasification |
| US8349288B2 (en) | 2006-12-06 | 2013-01-08 | The Regents Of The University Of California | Process for enhancing the operability of hot gas cleanup for the production of synthesis gas from steam-hydrogasification producer gas |
| US20080031809A1 (en) * | 2006-07-18 | 2008-02-07 | Norbeck Joseph M | Controlling the synthesis gas composition of a steam methane reformer |
| JP2009035946A (ja) * | 2007-08-02 | 2009-02-19 | Taisei Corp | 柱状構造物の動揺防止構造、柱状構造物の設置システム及び柱状構造物の設置方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3194644A (en) * | 1965-07-13 | Production of pipeline gas from | ||
| US2840462A (en) * | 1955-05-12 | 1958-06-24 | Consolidation Coal Co | Production of high btu-content gas from carbonaceous solid fuels |
| US3556749A (en) * | 1968-07-05 | 1971-01-19 | Gen Electric | Apparatus and method for the hydrogenation of coal |
| US3527691A (en) * | 1968-12-31 | 1970-09-08 | Shell Oil Co | Process for conversion of coal |
| US3708269A (en) * | 1970-11-12 | 1973-01-02 | Inst Gas Technology | Fossil fuel hydrogasification process for production of synthetic pipeline gas |
| US3755137A (en) * | 1971-03-24 | 1973-08-28 | Hydrocarbon Research Inc | Multi-stage ebullated bed coal-oil hydrogenation and hydrocracking process |
| US3823084A (en) * | 1972-06-30 | 1974-07-09 | W Schroeder | Hydrogenation of coal |
-
1973
- 1973-11-01 US US412026A patent/US3926775A/en not_active Expired - Lifetime
-
1974
- 1974-10-08 CA CA210,971A patent/CA1030470A/en not_active Expired
- 1974-10-17 DE DE19742449531 patent/DE2449531A1/de not_active Withdrawn
- 1974-11-01 JP JP49126499A patent/JPS5743117B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US3926775A (en) | 1975-12-16 |
| CA1030470A (en) | 1978-05-02 |
| JPS5075202A (https=) | 1975-06-20 |
| JPS5743117B2 (https=) | 1982-09-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| 8128 | New person/name/address of the agent |
Representative=s name: KERN, R., DIPL.-ING., PAT.-ANW., 8000 MUENCHEN |
|
| 8139 | Disposal/non-payment of the annual fee |