DE2415557C2 - Verfahren zur Herstellung von schnell-löslichen Süßstoff-Mischungen und diese Mischungen als solche - Google Patents
Verfahren zur Herstellung von schnell-löslichen Süßstoff-Mischungen und diese Mischungen als solcheInfo
- Publication number
- DE2415557C2 DE2415557C2 DE2415557A DE2415557A DE2415557C2 DE 2415557 C2 DE2415557 C2 DE 2415557C2 DE 2415557 A DE2415557 A DE 2415557A DE 2415557 A DE2415557 A DE 2415557A DE 2415557 C2 DE2415557 C2 DE 2415557C2
- Authority
- DE
- Germany
- Prior art keywords
- dipeptide
- acid
- solubility
- mixtures
- ground
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000203 mixture Substances 0.000 title claims description 27
- 238000000034 method Methods 0.000 title claims description 14
- 235000003599 food sweetener Nutrition 0.000 title claims description 10
- 239000003765 sweetening agent Substances 0.000 title claims description 10
- 230000008569 process Effects 0.000 title claims description 5
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 108010016626 Dipeptides Proteins 0.000 claims description 84
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 56
- 239000002245 particle Substances 0.000 claims description 25
- 239000007788 liquid Substances 0.000 claims description 22
- 235000015165 citric acid Nutrition 0.000 claims description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 10
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 10
- 235000011090 malic acid Nutrition 0.000 claims description 10
- 239000001630 malic acid Substances 0.000 claims description 10
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 8
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 8
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 claims description 6
- 235000011037 adipic acid Nutrition 0.000 claims description 3
- 239000001361 adipic acid Substances 0.000 claims description 3
- 150000001735 carboxylic acids Chemical class 0.000 claims description 3
- 239000002253 acid Substances 0.000 description 60
- 238000004090 dissolution Methods 0.000 description 21
- 235000013361 beverage Nutrition 0.000 description 9
- 235000013305 food Nutrition 0.000 description 9
- 238000002156 mixing Methods 0.000 description 7
- 239000000126 substance Substances 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 description 5
- 235000010357 aspartame Nutrition 0.000 description 5
- 238000000227 grinding Methods 0.000 description 5
- 150000004702 methyl esters Chemical class 0.000 description 4
- 108090000765 processed proteins & peptides Proteins 0.000 description 4
- 230000009467 reduction Effects 0.000 description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 3
- 229930006000 Sucrose Natural products 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 3
- 238000005054 agglomeration Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000003801 milling Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000005720 sucrose Substances 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 235000014171 carbonated beverage Nutrition 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 235000011850 desserts Nutrition 0.000 description 2
- 238000009837 dry grinding Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000008369 fruit flavor Substances 0.000 description 2
- 239000008240 homogeneous mixture Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 230000003993 interaction Effects 0.000 description 2
- 239000011872 intimate mixture Substances 0.000 description 2
- 230000005588 protonation Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 235000019640 taste Nutrition 0.000 description 2
- PXRKCOCTEMYUEG-UHFFFAOYSA-N 5-aminoisoindole-1,3-dione Chemical compound NC1=CC=C2C(=O)NC(=O)C2=C1 PXRKCOCTEMYUEG-UHFFFAOYSA-N 0.000 description 1
- 108010011485 Aspartame Proteins 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000000605 aspartame Substances 0.000 description 1
- 229960003438 aspartame Drugs 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 150000001983 dialkylethers Chemical class 0.000 description 1
- 229940082150 encore Drugs 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 235000007983 food acid Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 235000015122 lemonade Nutrition 0.000 description 1
- 235000021056 liquid food Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 229910000150 monocalcium phosphate Inorganic materials 0.000 description 1
- 235000019691 monocalcium phosphate Nutrition 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 230000010399 physical interaction Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 235000014438 salad dressings Nutrition 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000011973 solid acid Substances 0.000 description 1
- 235000021055 solid food Nutrition 0.000 description 1
- 239000008247 solid mixture Substances 0.000 description 1
- 235000019614 sour taste Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
- A23L27/31—Artificial sweetening agents containing amino acids, nucleotides, peptides or derivatives
- A23L27/32—Artificial sweetening agents containing amino acids, nucleotides, peptides or derivatives containing dipeptides or derivatives
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Seasonings (AREA)
- Non-Alcoholic Beverages (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
- Peptides Or Proteins (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US34700573A | 1973-04-02 | 1973-04-02 | |
| US347094A US3868472A (en) | 1973-04-02 | 1973-04-02 | Method of producing fast dissolving dipeptide sweetner for sweet/sour systems |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2415557A1 DE2415557A1 (de) | 1974-10-17 |
| DE2415557C2 true DE2415557C2 (de) | 1983-07-21 |
Family
ID=26995084
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2415557A Expired DE2415557C2 (de) | 1973-04-02 | 1974-03-30 | Verfahren zur Herstellung von schnell-löslichen Süßstoff-Mischungen und diese Mischungen als solche |
Country Status (7)
| Country | Link |
|---|---|
| JP (1) | JPS5718460B2 (cg-RX-API-DMAC7.html) |
| DE (1) | DE2415557C2 (cg-RX-API-DMAC7.html) |
| FR (1) | FR2222961B1 (cg-RX-API-DMAC7.html) |
| GB (1) | GB1468222A (cg-RX-API-DMAC7.html) |
| IE (1) | IE39105B1 (cg-RX-API-DMAC7.html) |
| IT (1) | IT1013929B (cg-RX-API-DMAC7.html) |
| NL (1) | NL7404428A (cg-RX-API-DMAC7.html) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IE44797B1 (en) * | 1976-04-05 | 1982-04-07 | Gen Foods Corp | Sweetening composition and method for the preparation thereof |
| JPS585140A (ja) * | 1981-07-02 | 1983-01-12 | Ajinomoto Co Inc | 清涼菓子組成物 |
| BE1010071A3 (nl) * | 1996-04-10 | 1997-12-02 | Holland Sweetener Co | Aspartaam op drager. |
| NL1015370C2 (nl) * | 2000-05-31 | 2001-12-03 | Holland Sweetener Co | Intensieve zoetstof op drager. |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3245798A (en) * | 1963-05-20 | 1966-04-12 | Monsanto Co | Soluble fumaric acid and adipic acid compositions |
| DE1692768C3 (de) * | 1968-02-16 | 1973-10-25 | G.D. Searle & Co., Chicago, Ill. (V.St.A.) | Süßstoff |
-
1974
- 1974-03-25 GB GB1321374A patent/GB1468222A/en not_active Expired
- 1974-03-27 IE IE00666/74A patent/IE39105B1/xx unknown
- 1974-03-29 IT IT42596/74A patent/IT1013929B/it active
- 1974-03-30 DE DE2415557A patent/DE2415557C2/de not_active Expired
- 1974-04-01 NL NL7404428A patent/NL7404428A/xx not_active Application Discontinuation
- 1974-04-02 JP JP3730674A patent/JPS5718460B2/ja not_active Expired
- 1974-04-02 FR FR7411685A patent/FR2222961B1/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| IE39105B1 (en) | 1978-08-02 |
| FR2222961B1 (cg-RX-API-DMAC7.html) | 1981-05-29 |
| IT1013929B (it) | 1977-03-30 |
| GB1468222A (en) | 1977-03-23 |
| AU6714574A (en) | 1975-10-02 |
| FR2222961A1 (cg-RX-API-DMAC7.html) | 1974-10-25 |
| JPS49126856A (cg-RX-API-DMAC7.html) | 1974-12-04 |
| DE2415557A1 (de) | 1974-10-17 |
| NL7404428A (cg-RX-API-DMAC7.html) | 1974-10-04 |
| IE39105L (en) | 1974-10-02 |
| JPS5718460B2 (cg-RX-API-DMAC7.html) | 1982-04-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8128 | New person/name/address of the agent |
Representative=s name: SCHOENWALD, K., DR.-ING. FUES, J., DIPL.-CHEM. DR. |
|
| 8110 | Request for examination paragraph 44 | ||
| 8125 | Change of the main classification |
Ipc: A23L 1/236 |
|
| 8126 | Change of the secondary classification |
Ipc: C07C103/52 |
|
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |