DE2201433A1 - Verfahren zur stabilisierung von chlorkohlensaeureestern - Google Patents
Verfahren zur stabilisierung von chlorkohlensaeureesternInfo
- Publication number
- DE2201433A1 DE2201433A1 DE19722201433 DE2201433A DE2201433A1 DE 2201433 A1 DE2201433 A1 DE 2201433A1 DE 19722201433 DE19722201433 DE 19722201433 DE 2201433 A DE2201433 A DE 2201433A DE 2201433 A1 DE2201433 A1 DE 2201433A1
- Authority
- DE
- Germany
- Prior art keywords
- esters
- acid esters
- chlorocarbody
- stabilization
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 6
- 150000002148 esters Chemical class 0.000 title description 6
- 230000006641 stabilisation Effects 0.000 title 1
- 238000011105 stabilization Methods 0.000 title 1
- 150000001408 amides Chemical class 0.000 claims description 10
- AOGYCOYQMAVAFD-UHFFFAOYSA-N chlorocarbonic acid Chemical class OC(Cl)=O AOGYCOYQMAVAFD-UHFFFAOYSA-N 0.000 claims description 9
- -1 chlorocarbonic acid ester Chemical class 0.000 claims description 8
- ZHNUHDYFZUAESO-UHFFFAOYSA-N Formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 claims description 4
- 230000000087 stabilizing effect Effects 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 claims 1
- 239000007789 gas Substances 0.000 description 5
- 239000000654 additive Substances 0.000 description 3
- 238000000354 decomposition reaction Methods 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- ULYZAYCEDJDHCC-UHFFFAOYSA-N isopropyl chloride Chemical compound CC(C)Cl ULYZAYCEDJDHCC-UHFFFAOYSA-N 0.000 description 3
- 239000003381 stabilizer Substances 0.000 description 3
- DLFVBJFMPXGRIB-UHFFFAOYSA-N Acetamide Chemical compound CC(N)=O DLFVBJFMPXGRIB-UHFFFAOYSA-N 0.000 description 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 238000004587 chromatography analysis Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 description 2
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
- LCEDQNDDFOCWGG-UHFFFAOYSA-N morpholine-4-carbaldehyde Chemical compound O=CN1CCOCC1 LCEDQNDDFOCWGG-UHFFFAOYSA-N 0.000 description 2
- BSSNZUFKXJJCBG-UPHRSURJSA-N (z)-but-2-enediamide Chemical compound NC(=O)\C=C/C(N)=O BSSNZUFKXJJCBG-UPHRSURJSA-N 0.000 description 1
- YOETUEMZNOLGDB-UHFFFAOYSA-N 2-methylpropyl carbonochloridate Chemical class CC(C)COC(Cl)=O YOETUEMZNOLGDB-UHFFFAOYSA-N 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- MGJKQDOBUOMPEZ-UHFFFAOYSA-N N,N'-dimethylurea Chemical compound CNC(=O)NC MGJKQDOBUOMPEZ-UHFFFAOYSA-N 0.000 description 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 1
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 description 1
- 229940051881 anilide analgesics and antipyretics Drugs 0.000 description 1
- 150000003931 anilides Chemical class 0.000 description 1
- DNSISZSEWVHGLH-UHFFFAOYSA-N butanamide Chemical compound CCCC(N)=O DNSISZSEWVHGLH-UHFFFAOYSA-N 0.000 description 1
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 description 1
- SNCZNSNPXMPCGN-UHFFFAOYSA-N butanediamide Chemical compound NC(=O)CCC(N)=O SNCZNSNPXMPCGN-UHFFFAOYSA-N 0.000 description 1
- NRDQFWXVTPZZAZ-UHFFFAOYSA-N butyl carbonochloridate Chemical group CCCCOC(Cl)=O NRDQFWXVTPZZAZ-UHFFFAOYSA-N 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 150000004651 carbonic acid esters Chemical class 0.000 description 1
- 150000003857 carboxamides Chemical class 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 230000004992 fission Effects 0.000 description 1
- UUZWCFHODWKNLS-UHFFFAOYSA-N formamide;1-methylpyrrolidin-2-one Chemical compound NC=O.CN1CCCC1=O UUZWCFHODWKNLS-UHFFFAOYSA-N 0.000 description 1
- 125000002485 formyl group Chemical group [H]C(*)=O 0.000 description 1
- 239000005337 ground glass Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 1
- VKOFPDUSOTWTPX-UHFFFAOYSA-N nonyl carbonochloridate Chemical class CCCCCCCCCOC(Cl)=O VKOFPDUSOTWTPX-UHFFFAOYSA-N 0.000 description 1
- XNGIFLGASWRNHJ-UHFFFAOYSA-N o-dicarboxybenzene Natural products OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 1
- RCCYSVYHULFYHE-UHFFFAOYSA-N pentanediamide Chemical compound NC(=O)CCCC(N)=O RCCYSVYHULFYHE-UHFFFAOYSA-N 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- IVRIRQXJSNCSPQ-UHFFFAOYSA-N propan-2-yl carbonochloridate Chemical class CC(C)OC(Cl)=O IVRIRQXJSNCSPQ-UHFFFAOYSA-N 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 150000003333 secondary alcohols Chemical class 0.000 description 1
- 150000003335 secondary amines Chemical class 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 150000003673 urethanes Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C68/00—Preparation of esters of carbonic or haloformic acids
- C07C68/08—Purification; Separation; Stabilisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyrrole Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE794008D BE794008A (fr) | 1972-01-13 | Procede de stabilisation d'esters d'acide chlorocarbonique | |
| DE19722201433 DE2201433A1 (de) | 1972-01-13 | 1972-01-13 | Verfahren zur stabilisierung von chlorkohlensaeureestern |
| IT3306572A IT971947B (it) | 1972-01-13 | 1972-12-18 | Processo per la stabilizzazione di esteri dell acido clorocarbo nico |
| NL7300415A NL7300415A (enExample) | 1972-01-13 | 1973-01-11 | |
| FR7301026A FR2168010A1 (en) | 1972-01-13 | 1973-01-12 | Chlorocarbonic ester stabilisation - using amides pref formamide or n-methylpyrrolidone |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19722201433 DE2201433A1 (de) | 1972-01-13 | 1972-01-13 | Verfahren zur stabilisierung von chlorkohlensaeureestern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2201433A1 true DE2201433A1 (de) | 1973-07-19 |
Family
ID=5832871
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19722201433 Pending DE2201433A1 (de) | 1972-01-13 | 1972-01-13 | Verfahren zur stabilisierung von chlorkohlensaeureestern |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE794008A (enExample) |
| DE (1) | DE2201433A1 (enExample) |
| FR (1) | FR2168010A1 (enExample) |
| IT (1) | IT971947B (enExample) |
| NL (1) | NL7300415A (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002059017A1 (de) | 2001-01-23 | 2002-08-01 | Basf Aktiengesellschaft | Verfahren zur lagerung und zum transport von chlorameisensäureestern |
-
0
- BE BE794008D patent/BE794008A/xx unknown
-
1972
- 1972-01-13 DE DE19722201433 patent/DE2201433A1/de active Pending
- 1972-12-18 IT IT3306572A patent/IT971947B/it active
-
1973
- 1973-01-11 NL NL7300415A patent/NL7300415A/xx unknown
- 1973-01-12 FR FR7301026A patent/FR2168010A1/fr not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002059017A1 (de) | 2001-01-23 | 2002-08-01 | Basf Aktiengesellschaft | Verfahren zur lagerung und zum transport von chlorameisensäureestern |
Also Published As
| Publication number | Publication date |
|---|---|
| IT971947B (it) | 1974-05-10 |
| FR2168010A1 (en) | 1973-08-24 |
| NL7300415A (enExample) | 1973-07-17 |
| BE794008A (fr) | 1973-07-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2430960A1 (de) | Antistatische massen fuer harze | |
| DE2201433A1 (de) | Verfahren zur stabilisierung von chlorkohlensaeureestern | |
| DE1052682B (de) | Verfahren zur Herstellung von schaumfoermigen Polyamiden | |
| DE3108622A1 (de) | "verfahren zur stabilisierung waesseriger loesungen von acetoacetamiden" | |
| DE896412C (de) | Verfahren zur Herstellung hochmolekularer Kondensationsprodukte | |
| DE888617C (de) | Verfahren zur Herstellung von stickstoffhaltigen Polykondensaten | |
| US2840484A (en) | Process for plastifying cellulosederivatives | |
| DE2931777A1 (de) | Verfahren zur herstellung von alkylchloriden | |
| DE888168C (de) | Verfahren zur Herstellung von Kondensationsprodukten von der Art der linearen Polyamide | |
| DE898516C (de) | Verfahren zur Herstellung von Polykondensationsprodukten | |
| DE1544939B2 (de) | Verfahren zur herstellung von gleitlagermaterial | |
| DE1135893B (de) | Verfahren zur Herstellung von Chlorkohlenwasserstoffen der Acetylenreihe | |
| DE2831555C2 (enExample) | ||
| AT252933B (de) | Verfahren zur Verbesserung der Lagereigenschaften von Harnstoff | |
| DE2638824A1 (de) | Verfahren zur herstellung von salzen aus dicarbonsaeuren und diaminen | |
| DE1109876B (de) | Das Aufschaeumen von thermoplastischen oder elastomeren kautschukaehnlichen Kunststoffen | |
| AT337159B (de) | Verfahren zur herstellung von neuen sulfonylaminophenylglycinen sowie deren estern, amiden und saureadditionssalzen | |
| DE933028C (de) | Verfahren zur Herstellung von am zentralen Kohlenstoffatom substituierten Diarylacetonitrilen | |
| DE1190932C2 (de) | Verfahren zur herstellung von terpenallyl-carbonsaeureestern | |
| DE949654C (de) | Verfahren zur Herstellung von Acrylsaeure und ihren funktionellen Derivaten | |
| AT222102B (de) | Verfahren zur Abtrennung von Acrylnitril aus gasförmigen Gemischen | |
| DE814143C (de) | Verfahren zur Herstellung von Sulfurylamid und Amidosulfonsaeure | |
| AT214419B (de) | Verfahren zur Herstellung von farblosen oder fast farblosen höhermolekularen Monocarbonsäureamidhalogenmethylverbindungen | |
| DE1163022B (de) | Verfahren zur Herstellung von linearen Polyamiden | |
| DE939027C (de) | Verfahren zur Herstellung von N, N'-Dinitroso-N, N'-dialkylamiden aromatischer Dicarbonsaeuren |