DE2151341C3 - Verfahren zur Herstellung von Raffinadezucker - Google Patents
Verfahren zur Herstellung von RaffinadezuckerInfo
- Publication number
- DE2151341C3 DE2151341C3 DE2151341A DE2151341A DE2151341C3 DE 2151341 C3 DE2151341 C3 DE 2151341C3 DE 2151341 A DE2151341 A DE 2151341A DE 2151341 A DE2151341 A DE 2151341A DE 2151341 C3 DE2151341 C3 DE 2151341C3
- Authority
- DE
- Germany
- Prior art keywords
- sugar
- juice
- refined
- exchange resin
- ion exchange
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 21
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 title claims description 14
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 41
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 18
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 18
- 238000000909 electrodialysis Methods 0.000 claims description 14
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 12
- 239000012528 membrane Substances 0.000 claims description 12
- 239000003456 ion exchange resin Substances 0.000 claims description 11
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 11
- 239000001569 carbon dioxide Substances 0.000 claims description 9
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 9
- 238000007670 refining Methods 0.000 claims description 7
- 239000000920 calcium hydroxide Substances 0.000 claims description 6
- 235000011116 calcium hydroxide Nutrition 0.000 claims description 6
- 239000002244 precipitate Substances 0.000 claims description 6
- 238000004140 cleaning Methods 0.000 claims description 4
- 238000005119 centrifugation Methods 0.000 claims description 3
- 238000004042 decolorization Methods 0.000 claims description 3
- 238000000605 extraction Methods 0.000 claims description 3
- 238000001704 evaporation Methods 0.000 description 7
- 230000008020 evaporation Effects 0.000 description 7
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 6
- 235000007201 Saccharum officinarum Nutrition 0.000 description 6
- 240000000111 Saccharum officinarum Species 0.000 description 6
- 239000003957 anion exchange resin Substances 0.000 description 5
- 238000009835 boiling Methods 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000011347 resin Substances 0.000 description 5
- 229920005989 resin Polymers 0.000 description 5
- 238000003763 carbonization Methods 0.000 description 4
- 238000005115 demineralization Methods 0.000 description 4
- 230000002328 demineralizing effect Effects 0.000 description 4
- 238000009792 diffusion process Methods 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 239000003014 ion exchange membrane Substances 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 229910000019 calcium carbonate Inorganic materials 0.000 description 3
- 239000003729 cation exchange resin Substances 0.000 description 3
- 229920001429 chelating resin Polymers 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 238000005342 ion exchange Methods 0.000 description 3
- 235000013379 molasses Nutrition 0.000 description 3
- 239000006188 syrup Substances 0.000 description 3
- 235000020357 syrup Nutrition 0.000 description 3
- 241000609240 Ambelania acida Species 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 235000011941 Tilia x europaea Nutrition 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000010905 bagasse Substances 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 238000004040 coloring Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000004571 lime Substances 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 241000219310 Beta vulgaris subsp. vulgaris Species 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- 235000021536 Sugar beet Nutrition 0.000 description 1
- 238000005349 anion exchange Methods 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 238000005341 cation exchange Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000000502 dialysis Methods 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000012609 strong anion exchange resin Substances 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 239000012608 weak cation exchange resin Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/18—Purification of sugar juices by electrical means
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Non-Alcoholic Beverages (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9105370 | 1970-10-16 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2151341A1 DE2151341A1 (de) | 1972-04-20 |
| DE2151341B2 DE2151341B2 (de) | 1977-10-27 |
| DE2151341C3 true DE2151341C3 (de) | 1978-07-13 |
Family
ID=14015748
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2151341A Expired DE2151341C3 (de) | 1970-10-16 | 1971-10-15 | Verfahren zur Herstellung von Raffinadezucker |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3781174A (enExample) |
| BR (1) | BR7106173D0 (enExample) |
| DE (1) | DE2151341C3 (enExample) |
| FR (1) | FR2109613A5 (enExample) |
| GB (1) | GB1350261A (enExample) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT989187B (it) * | 1973-06-15 | 1975-05-20 | Tecneco Spa | Processo per la depurazione di acque di scarico |
| US3887391A (en) * | 1974-02-19 | 1975-06-03 | Amalgamated Sugar Co | Process for the decalcification sugar beet juice |
| US4376023A (en) * | 1980-11-03 | 1983-03-08 | The Hubinger Company | Process for the preferential separation of dextrose from oligosaccharides |
| US4299677A (en) * | 1980-11-03 | 1981-11-10 | The Hubinger Co. | Process for the preferential separation of fructose from glucose |
| US5051236A (en) * | 1988-12-19 | 1991-09-24 | Fmc Corporation | Process for reducing the concentration of viable cells in a flowable fluid |
| US4936962A (en) * | 1989-03-01 | 1990-06-26 | Fmc Corporation | Process for adjusting the pH of an aqueous flowable fluid |
| US4938856A (en) * | 1989-03-01 | 1990-07-03 | Fmc Corporation | Process for mild heat treatment of a flowable fluid |
| US4880647A (en) * | 1989-03-10 | 1989-11-14 | Fmc Corporation | Process for mild heat treatment of concentrated fluids from membranes |
| FR2707997B1 (fr) * | 1993-07-19 | 1995-09-29 | Applexion Ste Nle Rech Applic | Procédé de raffinage d'un sucre brut, notamment de sucre roux provenant de l'industrie sucrière de la canne à sucre. |
| US5554227A (en) * | 1993-11-12 | 1996-09-10 | Societe Nouvelle De Recherches Et D'applications Industrielles D'echangeurs D'ions Applexion | Process of manufacturing crystal sugar from an aqueous sugar juice such as cane juice or sugar beet juice |
| US5468300A (en) * | 1994-04-07 | 1995-11-21 | International Food Processing Incorporated | Process for producing refined sugar directly from sugarcane |
| AU692864B2 (en) * | 1994-04-07 | 1998-06-18 | International Food Processing, Incorporated | Process for producing refined sugar |
| FR2719505B1 (fr) * | 1994-05-09 | 1996-06-14 | Vidaubanaise Ingenierie | Procédé de déminéralisation d'un liquide contenant en solution des matières organiques et des sels. |
| US5454875A (en) * | 1994-07-01 | 1995-10-03 | Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College | Softening and purification of molasses or syrup |
| RU2114177C1 (ru) * | 1997-06-02 | 1998-06-27 | Товарищество с ограниченной ответственностью Центр содействия развитию новых технологий "Кантэк" | Способ производства сахарного сиропа из сахаросодержащего сырья |
| US6017433A (en) * | 1997-11-12 | 2000-01-25 | Archer Daniels Midland Company | Desalting aqueous streams via filled cell electrodialysis |
| US6037456A (en) * | 1998-03-10 | 2000-03-14 | Biosource Technologies, Inc. | Process for isolating and purifying viruses, soluble proteins and peptides from plant sources |
| GB2433518A (en) * | 2005-12-21 | 2007-06-27 | Danisco | Process for the recovery of sucrose and non-sucrose materials |
| US20070256936A1 (en) * | 2006-05-04 | 2007-11-08 | Robert Jansen | Method for Deashing Syrup by Electrodialysis |
| CN101508707B (zh) * | 2009-03-25 | 2011-09-28 | 湖南尔康制药股份有限公司 | 药用蔗糖的生产工艺 |
| CN109825651A (zh) * | 2019-04-08 | 2019-05-31 | 中国科学院过程工程研究所 | 一种膜法制糖工艺中多联产的方法 |
-
1971
- 1971-04-19 GB GB2525471*A patent/GB1350261A/en not_active Expired
- 1971-06-09 FR FR7120985A patent/FR2109613A5/fr not_active Expired
- 1971-09-20 BR BR6173/71A patent/BR7106173D0/pt unknown
- 1971-10-13 US US00188851A patent/US3781174A/en not_active Expired - Lifetime
- 1971-10-15 DE DE2151341A patent/DE2151341C3/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| BR7106173D0 (pt) | 1973-03-29 |
| DE2151341A1 (de) | 1972-04-20 |
| US3781174A (en) | 1973-12-25 |
| DE2151341B2 (de) | 1977-10-27 |
| GB1350261A (en) | 1974-04-18 |
| FR2109613A5 (enExample) | 1972-05-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |