DE2144642A1 - Verfahren und Vorrichtung zum Überführen einer Probe in Atome zwecks Analyse der Probe durch Atomspektroskopie - Google Patents
Verfahren und Vorrichtung zum Überführen einer Probe in Atome zwecks Analyse der Probe durch AtomspektroskopieInfo
- Publication number
- DE2144642A1 DE2144642A1 DE19712144642 DE2144642A DE2144642A1 DE 2144642 A1 DE2144642 A1 DE 2144642A1 DE 19712144642 DE19712144642 DE 19712144642 DE 2144642 A DE2144642 A DE 2144642A DE 2144642 A1 DE2144642 A1 DE 2144642A1
- Authority
- DE
- Germany
- Prior art keywords
- sample
- chamber
- atomic
- stream
- volume
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 40
- 238000000559 atomic spectroscopy Methods 0.000 title claims description 14
- 230000015572 biosynthetic process Effects 0.000 claims description 32
- 238000010438 heat treatment Methods 0.000 claims description 19
- 230000000737 periodic effect Effects 0.000 claims description 8
- 230000003647 oxidation Effects 0.000 claims description 6
- 238000007254 oxidation reaction Methods 0.000 claims description 6
- 239000000523 sample Substances 0.000 description 224
- 238000004458 analytical method Methods 0.000 description 51
- 230000005855 radiation Effects 0.000 description 50
- 239000000126 substance Substances 0.000 description 38
- 125000004429 atom Chemical group 0.000 description 35
- 238000001514 detection method Methods 0.000 description 29
- 238000001391 atomic fluorescence spectroscopy Methods 0.000 description 27
- 238000001636 atomic emission spectroscopy Methods 0.000 description 26
- 210000002966 serum Anatomy 0.000 description 18
- 229910052751 metal Inorganic materials 0.000 description 17
- 239000002184 metal Substances 0.000 description 16
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 15
- 239000007788 liquid Substances 0.000 description 15
- 150000003839 salts Chemical class 0.000 description 14
- 238000012545 processing Methods 0.000 description 11
- 210000002381 plasma Anatomy 0.000 description 10
- 238000012546 transfer Methods 0.000 description 10
- 239000000203 mixture Substances 0.000 description 9
- 230000035945 sensitivity Effects 0.000 description 9
- 239000003570 air Substances 0.000 description 8
- 229910052742 iron Inorganic materials 0.000 description 8
- 239000012071 phase Substances 0.000 description 8
- 229910052708 sodium Inorganic materials 0.000 description 8
- 238000004611 spectroscopical analysis Methods 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- 239000002245 particle Substances 0.000 description 7
- 239000000446 fuel Substances 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- 238000005259 measurement Methods 0.000 description 5
- 239000011734 sodium Substances 0.000 description 5
- 239000012080 ambient air Substances 0.000 description 4
- 238000000149 argon plasma sintering Methods 0.000 description 4
- 239000012530 fluid Substances 0.000 description 4
- 238000004445 quantitative analysis Methods 0.000 description 4
- 125000004436 sodium atom Chemical group 0.000 description 4
- OMOVVBIIQSXZSZ-UHFFFAOYSA-N [6-(4-acetyloxy-5,9a-dimethyl-2,7-dioxo-4,5a,6,9-tetrahydro-3h-pyrano[3,4-b]oxepin-5-yl)-5-formyloxy-3-(furan-3-yl)-3a-methyl-7-methylidene-1a,2,3,4,5,6-hexahydroindeno[1,7a-b]oxiren-4-yl] 2-hydroxy-3-methylpentanoate Chemical compound CC12C(OC(=O)C(O)C(C)CC)C(OC=O)C(C3(C)C(CC(=O)OC4(C)COC(=O)CC43)OC(C)=O)C(=C)C32OC3CC1C=1C=COC=1 OMOVVBIIQSXZSZ-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 238000004737 colorimetric analysis Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 230000005284 excitation Effects 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 238000000638 solvent extraction Methods 0.000 description 3
- 239000008346 aqueous phase Substances 0.000 description 2
- 238000001479 atomic absorption spectroscopy Methods 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 238000004807 desolvation Methods 0.000 description 2
- 239000002737 fuel gas Substances 0.000 description 2
- 230000002452 interceptive effect Effects 0.000 description 2
- 239000012074 organic phase Substances 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000000935 solvent evaporation Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241000347389 Serranus cabrilla Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 230000001174 ascending effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000012468 concentrated sample Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 238000012921 fluorescence analysis Methods 0.000 description 1
- 230000035876 healing Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000001678 irradiating effect Effects 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 229910052756 noble gas Inorganic materials 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 210000001747 pupil Anatomy 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 238000010408 sweeping Methods 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/71—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light thermally excited
- G01N21/72—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light thermally excited using flame burners
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/3103—Atomic absorption analysis
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US7177470A | 1970-09-14 | 1970-09-14 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2144642A1 true DE2144642A1 (de) | 1972-03-30 |
Family
ID=22103500
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712144642 Pending DE2144642A1 (de) | 1970-09-14 | 1971-09-07 | Verfahren und Vorrichtung zum Überführen einer Probe in Atome zwecks Analyse der Probe durch Atomspektroskopie |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3740145A (enExample) |
| AU (1) | AU454603B2 (enExample) |
| BE (1) | BE772218A (enExample) |
| CA (1) | CA949349A (enExample) |
| DE (1) | DE2144642A1 (enExample) |
| FR (1) | FR2107508A5 (enExample) |
| GB (1) | GB1354977A (enExample) |
| IT (1) | IT961044B (enExample) |
| NL (1) | NL7112536A (enExample) |
| SE (1) | SE379856B (enExample) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2729744A1 (de) * | 1977-07-01 | 1979-01-11 | Bodenseewerk Perkin Elmer Co | Verfahren und vorrichtung zur automatischen erzeugung und messung gasfoermiger proben aus einer reihe fluessiger proben |
| DE3307409A1 (de) * | 1983-03-02 | 1984-09-06 | Kosizky, Wladimir, Dr., 8000 München | Atomabsorptions-spektrophotometer mit rueckkopplung |
| EP0208901A1 (de) * | 1985-06-15 | 1987-01-21 | Harald Dr. Berndt | Vorrichtung zum Zerstäuben von Probenflüssigkeit für spektroskopische Zwecke |
| DE3818058A1 (de) * | 1988-05-27 | 1989-12-07 | Bodenseewerk Perkin Elmer Co | Vorrichtung zur zufuhr von fluessigkeit zu einem zerstaeuber bei einem spektrometer |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3866831A (en) * | 1973-10-10 | 1975-02-18 | Research Corp | Pulsed ultrasonic nebulization system and method for flame spectroscopy |
| US4865444A (en) * | 1984-04-05 | 1989-09-12 | Mobil Oil Corporation | Apparatus and method for determining luminosity of hydrocarbon fuels |
| GB2178850A (en) * | 1985-08-05 | 1987-02-18 | Mobil Oil Corp | Apparatus and method for determining luminosity of hydrocarbon fuels |
| ATE140395T1 (de) * | 1990-08-09 | 1996-08-15 | Fisons Plc | Verfahren und vorrichtung zur vorbereitung analytischer proben |
| CN113418879A (zh) * | 2021-06-24 | 2021-09-21 | 宁夏新龙蓝天科技股份有限公司 | 氯化铜溶液检测方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3419359A (en) * | 1965-07-08 | 1968-12-31 | Atomic Energy Commission Usa | Flame ionization detector |
| US3521959A (en) * | 1967-08-29 | 1970-07-28 | Atomic Energy Commission | Method for direct spectrographic analysis of molten metals |
| US3620628A (en) * | 1968-05-04 | 1971-11-16 | Hitachi Ltd | Photoelectric sample measuring apparatus |
-
1970
- 1970-09-14 US US00071774A patent/US3740145A/en not_active Expired - Lifetime
-
1971
- 1971-08-31 AU AU32892/71A patent/AU454603B2/en not_active Expired
- 1971-09-02 CA CA121,998A patent/CA949349A/en not_active Expired
- 1971-09-06 BE BE772218A patent/BE772218A/xx unknown
- 1971-09-07 GB GB4164771A patent/GB1354977A/en not_active Expired
- 1971-09-07 DE DE19712144642 patent/DE2144642A1/de active Pending
- 1971-09-10 FR FR7132664A patent/FR2107508A5/fr not_active Expired
- 1971-09-11 IT IT28520/71A patent/IT961044B/it active
- 1971-09-13 NL NL7112536A patent/NL7112536A/xx unknown
- 1971-09-14 SE SE7111665A patent/SE379856B/xx unknown
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2729744A1 (de) * | 1977-07-01 | 1979-01-11 | Bodenseewerk Perkin Elmer Co | Verfahren und vorrichtung zur automatischen erzeugung und messung gasfoermiger proben aus einer reihe fluessiger proben |
| DE3307409A1 (de) * | 1983-03-02 | 1984-09-06 | Kosizky, Wladimir, Dr., 8000 München | Atomabsorptions-spektrophotometer mit rueckkopplung |
| EP0208901A1 (de) * | 1985-06-15 | 1987-01-21 | Harald Dr. Berndt | Vorrichtung zum Zerstäuben von Probenflüssigkeit für spektroskopische Zwecke |
| US4886359A (en) * | 1985-06-15 | 1989-12-12 | Harald Berndt | Device for nebuilizing sample liquid for spectroscopical purposes |
| DE3818058A1 (de) * | 1988-05-27 | 1989-12-07 | Bodenseewerk Perkin Elmer Co | Vorrichtung zur zufuhr von fluessigkeit zu einem zerstaeuber bei einem spektrometer |
Also Published As
| Publication number | Publication date |
|---|---|
| IT961044B (it) | 1973-12-10 |
| FR2107508A5 (enExample) | 1972-05-05 |
| SE379856B (enExample) | 1975-10-20 |
| AU454603B2 (en) | 1974-10-31 |
| US3740145A (en) | 1973-06-19 |
| CA949349A (en) | 1974-06-18 |
| BE772218A (fr) | 1972-03-06 |
| AU3289271A (en) | 1973-03-08 |
| GB1354977A (en) | 1974-06-05 |
| NL7112536A (enExample) | 1972-03-16 |
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