DE2134161B2 - Verfahren zur reduktion von nickel und cobaltoxyden - Google Patents
Verfahren zur reduktion von nickel und cobaltoxydenInfo
- Publication number
- DE2134161B2 DE2134161B2 DE19712134161 DE2134161A DE2134161B2 DE 2134161 B2 DE2134161 B2 DE 2134161B2 DE 19712134161 DE19712134161 DE 19712134161 DE 2134161 A DE2134161 A DE 2134161A DE 2134161 B2 DE2134161 B2 DE 2134161B2
- Authority
- DE
- Germany
- Prior art keywords
- bath
- nickel
- oxide
- oxygen
- reduction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 31
- 230000009467 reduction Effects 0.000 title claims description 15
- 229910052760 oxygen Inorganic materials 0.000 claims description 52
- 239000001301 oxygen Substances 0.000 claims description 52
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 50
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 36
- 239000003638 chemical reducing agent Substances 0.000 claims description 29
- 229910052751 metal Inorganic materials 0.000 claims description 29
- 239000002184 metal Substances 0.000 claims description 29
- 239000007789 gas Substances 0.000 claims description 22
- 239000012535 impurity Substances 0.000 claims description 19
- 229910052759 nickel Inorganic materials 0.000 claims description 18
- 238000006722 reduction reaction Methods 0.000 claims description 18
- 229910000480 nickel oxide Inorganic materials 0.000 claims description 16
- 239000000446 fuel Substances 0.000 claims description 15
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 claims description 15
- 150000001875 compounds Chemical class 0.000 claims description 14
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 13
- 229910052717 sulfur Inorganic materials 0.000 claims description 13
- 239000011593 sulfur Substances 0.000 claims description 13
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 12
- 239000000126 substance Substances 0.000 claims description 11
- 229910002091 carbon monoxide Inorganic materials 0.000 claims description 9
- 238000002844 melting Methods 0.000 claims description 8
- 230000008018 melting Effects 0.000 claims description 8
- 229910017052 cobalt Inorganic materials 0.000 claims description 7
- 239000010941 cobalt Substances 0.000 claims description 7
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 7
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(ii) oxide Chemical compound [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 claims description 7
- 229930195733 hydrocarbon Natural products 0.000 claims description 7
- 150000002430 hydrocarbons Chemical class 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- 229910044991 metal oxide Inorganic materials 0.000 claims description 6
- 150000004706 metal oxides Chemical class 0.000 claims description 6
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 5
- 239000008188 pellet Substances 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 229910000428 cobalt oxide Inorganic materials 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 229920006395 saturated elastomer Polymers 0.000 claims description 4
- 239000004215 Carbon black (E152) Substances 0.000 claims description 3
- 230000002378 acidificating effect Effects 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- 238000007670 refining Methods 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 229910052787 antimony Inorganic materials 0.000 claims description 2
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims description 2
- 229910052793 cadmium Inorganic materials 0.000 claims description 2
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 claims description 2
- 238000002485 combustion reaction Methods 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 229910000008 nickel(II) carbonate Inorganic materials 0.000 claims description 2
- ZULUUIKRFGGGTL-UHFFFAOYSA-L nickel(ii) carbonate Chemical compound [Ni+2].[O-]C([O-])=O ZULUUIKRFGGGTL-UHFFFAOYSA-L 0.000 claims description 2
- 229910052725 zinc Inorganic materials 0.000 claims description 2
- 239000011701 zinc Substances 0.000 claims description 2
- 230000004907 flux Effects 0.000 claims 2
- MPDDTAJMJCESGV-CTUHWIOQSA-M (3r,5r)-7-[2-(4-fluorophenyl)-5-[methyl-[(1r)-1-phenylethyl]carbamoyl]-4-propan-2-ylpyrazol-3-yl]-3,5-dihydroxyheptanoate Chemical compound C1([C@@H](C)N(C)C(=O)C2=NN(C(CC[C@@H](O)C[C@@H](O)CC([O-])=O)=C2C(C)C)C=2C=CC(F)=CC=2)=CC=CC=C1 MPDDTAJMJCESGV-CTUHWIOQSA-M 0.000 claims 1
- 101100493713 Caenorhabditis elegans bath-45 gene Proteins 0.000 claims 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims 1
- 235000011941 Tilia x europaea Nutrition 0.000 claims 1
- RACAZSJZTVYGKJ-UHFFFAOYSA-N [C].[Ni]=O Chemical compound [C].[Ni]=O RACAZSJZTVYGKJ-UHFFFAOYSA-N 0.000 claims 1
- 238000005275 alloying Methods 0.000 claims 1
- 239000012141 concentrate Substances 0.000 claims 1
- 238000009749 continuous casting Methods 0.000 claims 1
- 239000013067 intermediate product Substances 0.000 claims 1
- 239000011504 laterite Substances 0.000 claims 1
- 229910001710 laterite Inorganic materials 0.000 claims 1
- 238000002386 leaching Methods 0.000 claims 1
- 239000004571 lime Substances 0.000 claims 1
- 150000002739 metals Chemical class 0.000 claims 1
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 claims 1
- 238000010583 slow cooling Methods 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
- WWNBZGLDODTKEM-UHFFFAOYSA-N sulfanylidenenickel Chemical compound [Ni]=S WWNBZGLDODTKEM-UHFFFAOYSA-N 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 9
- 238000007792 addition Methods 0.000 description 8
- 229910052799 carbon Inorganic materials 0.000 description 8
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 8
- 230000008901 benefit Effects 0.000 description 5
- 239000000571 coke Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 238000009489 vacuum treatment Methods 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000007664 blowing Methods 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 239000003245 coal Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 229910052797 bismuth Inorganic materials 0.000 description 2
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 230000006698 induction Effects 0.000 description 2
- 238000003760 magnetic stirring Methods 0.000 description 2
- 238000010907 mechanical stirring Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 2
- 229910052753 mercury Inorganic materials 0.000 description 2
- 239000003345 natural gas Substances 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- -1 compounds nickel oxide Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000008451 emotion Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 230000002631 hypothermal effect Effects 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 239000011133 lead Substances 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 239000010747 number 6 fuel oil Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 230000001706 oxygenating effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B23/00—Obtaining nickel or cobalt
- C22B23/02—Obtaining nickel or cobalt by dry processes
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA087698A CA921708A (en) | 1970-07-08 | 1970-07-08 | Reduction of nickel and cobalt oxides |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2134161B2 true DE2134161B2 (de) | 1972-02-03 |
| DE2134161A1 DE2134161A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1972-02-03 |
Family
ID=4087157
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712134161 Withdrawn DE2134161B2 (de) | 1970-07-08 | 1971-07-08 | Verfahren zur reduktion von nickel und cobaltoxyden |
Country Status (9)
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3877933A (en) * | 1973-09-21 | 1975-04-15 | Int Nickel Co | Metallurgical addition product |
| JPH02221336A (ja) * | 1989-02-21 | 1990-09-04 | Nkk Corp | Ｎｉ鉱石の溶融還元法 |
| US5324341A (en) * | 1992-05-05 | 1994-06-28 | Molten Metal Technology, Inc. | Method for chemically reducing metals in waste compositions |
| RU2134729C1 (ru) * | 1998-02-12 | 1999-08-20 | Попов Владимир Максимович | Способ переработки окисленных никелевых руд |
| RU2132400C1 (ru) * | 1998-09-03 | 1999-06-27 | Открытое акционерное общество "Серовский металлургический завод" | Способ переработки окисленных никелевых руд |
| AU2008316326B2 (en) * | 2007-10-26 | 2013-06-20 | Bhp Billiton Innovation Pty Ltd | Production of nickel |
| US8557019B2 (en) * | 2008-02-08 | 2013-10-15 | Vale Inco Limited | Process for production of nickel and cobalt using metal hydroxide, metal oxide and/or metal carbonate |
| EP2337873A4 (en) * | 2008-02-12 | 2015-04-15 | Bhp Billiton Innovation Pty | NICKEL PRODUCTION |
| FR3008426B1 (fr) * | 2013-07-15 | 2015-08-07 | Eramet | Procede d'elaboration de nickel metallique a partir d'oxyde de nickel par fusion-reduction |
| RU2621496C2 (ru) * | 2015-06-09 | 2017-06-06 | Александр Александрович Веселовский | Способ переработки окисленных никелевых руд и отвальных никелевых шлаков химико-термической обработкой |
| CN112584949A (zh) * | 2018-09-26 | 2021-03-30 | 松下知识产权经营株式会社 | 镍颗粒的制造方法、硫酸镍的制造方法和二次电池用正极活性物质的制造方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1828752A (en) * | 1928-05-03 | 1931-10-27 | Int Nickel Co | Desulphurizing nickel-containing matte |
| US2740710A (en) * | 1951-03-02 | 1956-04-03 | Johannsen Friedrich | Method for the production of iron, nickel, cobalt, manganese, and chromium from their ores |
| US2815279A (en) * | 1953-11-02 | 1957-12-03 | Nat Res Corp | Process of preparing high purity nickel |
| US3030201A (en) * | 1960-09-02 | 1962-04-17 | Int Nickel Co | Method of producing ferro-nickel from nickel-containing silicate ores |
| US3157489A (en) * | 1961-03-09 | 1964-11-17 | Pullman Inc | Method for reducing metal oxides |
| US3169055A (en) * | 1961-10-12 | 1965-02-09 | Stora Kopparbergs Bergslags Ab | Process for producing pig iron in rotary furnace |
| US3188198A (en) * | 1962-08-23 | 1965-06-08 | Gen Electric | Method for deoxidizing metals |
| US3326671A (en) * | 1963-02-21 | 1967-06-20 | Howard K Worner | Direct smelting of metallic ores |
| US3188196A (en) * | 1963-06-19 | 1965-06-08 | Pullman Inc | Method for desiccating and reducing ore |
| US3640701A (en) * | 1964-04-30 | 1972-02-08 | Creusot Loire | Direct reduction of oxides |
| FR1436799A (fr) * | 1965-03-18 | 1966-04-29 | Soc Metallurgique Imphy | Procédé et installation de réduction d'oxydes métalliques |
| DE1458771B2 (de) * | 1965-06-23 | 1973-01-04 | Metallgesellschaft Ag, 6000 Frankfurt | Verfahren zum Reduzieren von Eisenerzen im Drehrohrofen |
-
1970
- 1970-07-08 CA CA087698A patent/CA921708A/en not_active Expired
-
1971
- 1971-06-21 US US00155354A patent/US3769002A/en not_active Expired - Lifetime
- 1971-06-28 ZA ZA714230A patent/ZA714230B/xx unknown
- 1971-06-30 NO NO02487/71A patent/NO128620B/no unknown
- 1971-07-07 GB GB3195771A patent/GB1316200A/en not_active Expired
- 1971-07-08 FR FR7125112A patent/FR2098258B1/fr not_active Expired
- 1971-07-08 DO DO1971001829A patent/DOP1971001829A/es unknown
- 1971-07-08 DE DE19712134161 patent/DE2134161B2/de not_active Withdrawn
- 1971-07-08 JP JP46050649A patent/JPS5227612B1/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| FR2098258B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1974-04-05 |
| FR2098258A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1972-03-10 |
| CA921708A (en) | 1973-02-27 |
| DE2134161A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1972-02-03 |
| JPS5227612B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1977-07-21 |
| DOP1971001829A (es) | 1976-05-12 |
| NO128620B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1973-12-17 |
| ZA714230B (en) | 1972-03-29 |
| US3769002A (en) | 1973-10-30 |
| GB1316200A (en) | 1973-05-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| E77 | Valid patent as to the heymanns-index 1977 | ||
| EHJ | Ceased/non-payment of the annual fee |