DE2133198C3 - Verfahren zur Herstellung von O-(2,2-Dichlorvinyl)-thionophosphorsäureesterdichlorid - Google Patents
Verfahren zur Herstellung von O-(2,2-Dichlorvinyl)-thionophosphorsäureesterdichloridInfo
- Publication number
- DE2133198C3 DE2133198C3 DE2133198A DE2133198A DE2133198C3 DE 2133198 C3 DE2133198 C3 DE 2133198C3 DE 2133198 A DE2133198 A DE 2133198A DE 2133198 A DE2133198 A DE 2133198A DE 2133198 C3 DE2133198 C3 DE 2133198C3
- Authority
- DE
- Germany
- Prior art keywords
- acid ester
- dichlorovinyl
- ester dichloride
- preparation
- thionophosphoric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 8
- -1 O- (2,2-dichlorovinyl) thionophosphoric acid ester Chemical class 0.000 title claims description 7
- 238000006243 chemical reaction Methods 0.000 description 7
- CYQAYERJWZKYML-UHFFFAOYSA-N phosphorus pentasulfide Chemical compound S1P(S2)(=S)SP3(=S)SP1(=S)SP2(=S)S3 CYQAYERJWZKYML-UHFFFAOYSA-N 0.000 description 5
- 150000002148 esters Chemical class 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- WQYSXVGEZYESBR-UHFFFAOYSA-N thiophosphoryl chloride Chemical compound ClP(Cl)(Cl)=S WQYSXVGEZYESBR-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 150000003014 phosphoric acid esters Chemical class 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 238000009835 boiling Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- OKQKDCXVLPGWPO-UHFFFAOYSA-N sulfanylidenephosphane Chemical compound S=P OKQKDCXVLPGWPO-UHFFFAOYSA-N 0.000 description 2
- MNRWIFMPVCLIDS-UHFFFAOYSA-N 2,2-dichloroethenyl dihydrogen phosphate Chemical compound OP(O)(=O)OC=C(Cl)Cl MNRWIFMPVCLIDS-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N phosphoric acid Substances OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 1
- 239000004476 plant protection product Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/20—Esters of thiophosphoric acids containing P-halide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/173—Esters of thiophosphoric acids with unsaturated acyclic alcohols
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
Priority Applications (11)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE785786D BE785786A (fr) | 1971-07-03 | Procede de preparation de dichlorure d'ester o-(2,2-dichlorovinylique) d'acide thionophosphorique | |
| DE2133198A DE2133198C3 (de) | 1971-07-03 | 1971-07-03 | Verfahren zur Herstellung von O-(2,2-Dichlorvinyl)-thionophosphorsäureesterdichlorid |
| BR4266/72A BR7204266D0 (pt) | 1971-07-03 | 1972-06-29 | Processo para preparacao de dicloreto de ester de acido(2,2-diclorovinil) tionofosforico |
| NL7209203A NL7209203A (OSRAM) | 1971-07-03 | 1972-06-30 | |
| JP6579972A JPS5536677B1 (OSRAM) | 1971-07-03 | 1972-06-30 | |
| CH989172A CH570415A5 (OSRAM) | 1971-07-03 | 1972-06-30 | |
| IL39800A IL39800A (en) | 1971-07-03 | 1972-06-30 | A thionophosphoric acid ester dichloride and its preparation |
| IT26520/72A IT962348B (it) | 1971-07-03 | 1972-07-01 | Procedimento per la preparazione di o 2 2 diclorovinil tionofo sforesteredicloruro |
| GB3095572A GB1331889A (en) | 1971-07-03 | 1972-07-03 | Thionophosphoric acid ester dichloride and its prepration |
| FR7223950A FR2144728B1 (OSRAM) | 1971-07-03 | 1972-07-03 | |
| US386682A US3862276A (en) | 1971-07-03 | 1973-08-08 | Preparation of 0-(2,2-dichlorovinyl)-thionophosphoric acid ester dichloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2133198A DE2133198C3 (de) | 1971-07-03 | 1971-07-03 | Verfahren zur Herstellung von O-(2,2-Dichlorvinyl)-thionophosphorsäureesterdichlorid |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2133198A1 DE2133198A1 (de) | 1973-01-11 |
| DE2133198B2 DE2133198B2 (de) | 1978-04-13 |
| DE2133198C3 true DE2133198C3 (de) | 1978-12-07 |
Family
ID=5812608
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2133198A Expired DE2133198C3 (de) | 1971-07-03 | 1971-07-03 | Verfahren zur Herstellung von O-(2,2-Dichlorvinyl)-thionophosphorsäureesterdichlorid |
Country Status (10)
| Country | Link |
|---|---|
| JP (1) | JPS5536677B1 (OSRAM) |
| BE (1) | BE785786A (OSRAM) |
| BR (1) | BR7204266D0 (OSRAM) |
| CH (1) | CH570415A5 (OSRAM) |
| DE (1) | DE2133198C3 (OSRAM) |
| FR (1) | FR2144728B1 (OSRAM) |
| GB (1) | GB1331889A (OSRAM) |
| IL (1) | IL39800A (OSRAM) |
| IT (1) | IT962348B (OSRAM) |
| NL (1) | NL7209203A (OSRAM) |
-
0
- BE BE785786D patent/BE785786A/xx unknown
-
1971
- 1971-07-03 DE DE2133198A patent/DE2133198C3/de not_active Expired
-
1972
- 1972-06-29 BR BR4266/72A patent/BR7204266D0/pt unknown
- 1972-06-30 CH CH989172A patent/CH570415A5/xx not_active IP Right Cessation
- 1972-06-30 JP JP6579972A patent/JPS5536677B1/ja active Pending
- 1972-06-30 NL NL7209203A patent/NL7209203A/xx not_active Application Discontinuation
- 1972-06-30 IL IL39800A patent/IL39800A/xx unknown
- 1972-07-01 IT IT26520/72A patent/IT962348B/it active
- 1972-07-03 FR FR7223950A patent/FR2144728B1/fr not_active Expired
- 1972-07-03 GB GB3095572A patent/GB1331889A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5536677B1 (OSRAM) | 1980-09-22 |
| BE785786A (fr) | 1973-01-03 |
| IL39800A (en) | 1974-12-31 |
| BR7204266D0 (pt) | 1973-06-14 |
| DE2133198B2 (de) | 1978-04-13 |
| DE2133198A1 (de) | 1973-01-11 |
| GB1331889A (en) | 1973-09-26 |
| IL39800A0 (en) | 1972-08-30 |
| FR2144728B1 (OSRAM) | 1976-08-06 |
| CH570415A5 (OSRAM) | 1975-12-15 |
| FR2144728A1 (OSRAM) | 1973-02-16 |
| NL7209203A (OSRAM) | 1973-01-05 |
| IT962348B (it) | 1973-12-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| EHV | Ceased/renunciation |