DE2113591A1 - Verfahren zur Herstellung von Borhalogeniden - Google Patents
Verfahren zur Herstellung von BorhalogenidenInfo
- Publication number
- DE2113591A1 DE2113591A1 DE19712113591 DE2113591A DE2113591A1 DE 2113591 A1 DE2113591 A1 DE 2113591A1 DE 19712113591 DE19712113591 DE 19712113591 DE 2113591 A DE2113591 A DE 2113591A DE 2113591 A1 DE2113591 A1 DE 2113591A1
- Authority
- DE
- Germany
- Prior art keywords
- boron
- hydrogen
- reaction
- halogen
- alkaline earth
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 15
- -1 boron halides Chemical class 0.000 title claims description 10
- 229910052796 boron Inorganic materials 0.000 title claims description 9
- 238000002360 preparation method Methods 0.000 title description 2
- 229910052736 halogen Inorganic materials 0.000 claims description 10
- 150000002367 halogens Chemical class 0.000 claims description 10
- 229910000039 hydrogen halide Inorganic materials 0.000 claims description 7
- 239000012433 hydrogen halide Substances 0.000 claims description 7
- 229910052791 calcium Inorganic materials 0.000 claims description 6
- 239000011575 calcium Substances 0.000 claims description 6
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 3
- BICAGYDGRXJYGD-UHFFFAOYSA-N hydrobromide;hydrochloride Chemical compound Cl.Br BICAGYDGRXJYGD-UHFFFAOYSA-N 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 5
- CPELXLSAUQHCOX-UHFFFAOYSA-N Hydrogen bromide Chemical compound Br CPELXLSAUQHCOX-UHFFFAOYSA-N 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 229910052580 B4C Inorganic materials 0.000 description 3
- INAHAJYZKVIDIZ-UHFFFAOYSA-N boron carbide Chemical compound B12B3B4C32B41 INAHAJYZKVIDIZ-UHFFFAOYSA-N 0.000 description 3
- 150000001639 boron compounds Chemical class 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- FAQYAMRNWDIXMY-UHFFFAOYSA-N trichloroborane Chemical compound ClB(Cl)Cl FAQYAMRNWDIXMY-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- ILAHWRKJUDSMFH-UHFFFAOYSA-N boron tribromide Chemical compound BrB(Br)Br ILAHWRKJUDSMFH-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 229910000042 hydrogen bromide Inorganic materials 0.000 description 2
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 241001101998 Galium Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 1
- LBZRRXXISSKCHV-UHFFFAOYSA-N [B].[O] Chemical class [B].[O] LBZRRXXISSKCHV-UHFFFAOYSA-N 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052810 boron oxide Inorganic materials 0.000 description 1
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical class [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 230000002140 halogenating effect Effects 0.000 description 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 1
- 229910000043 hydrogen iodide Inorganic materials 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B35/00—Boron; Compounds thereof
- C01B35/06—Boron halogen compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Catalysts (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Luminescent Compositions (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712113591 DE2113591A1 (de) | 1971-03-20 | 1971-03-20 | Verfahren zur Herstellung von Borhalogeniden |
| NL7203078A NL7203078A (https=) | 1971-03-20 | 1972-03-08 | |
| US00234675A US3839538A (en) | 1971-03-20 | 1972-03-14 | Process for the manufacture of boron halides |
| FR7209396A FR2130379B1 (https=) | 1971-03-20 | 1972-03-17 | |
| GB1258372A GB1387665A (en) | 1971-03-20 | 1972-03-17 | Process for the manufacture of boron halides |
| JP47028478A JPS5139198B1 (https=) | 1971-03-20 | 1972-03-21 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712113591 DE2113591A1 (de) | 1971-03-20 | 1971-03-20 | Verfahren zur Herstellung von Borhalogeniden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2113591A1 true DE2113591A1 (de) | 1972-11-30 |
Family
ID=5802253
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712113591 Pending DE2113591A1 (de) | 1971-03-20 | 1971-03-20 | Verfahren zur Herstellung von Borhalogeniden |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3839538A (https=) |
| JP (1) | JPS5139198B1 (https=) |
| DE (1) | DE2113591A1 (https=) |
| FR (1) | FR2130379B1 (https=) |
| GB (1) | GB1387665A (https=) |
| NL (1) | NL7203078A (https=) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103506056B (zh) * | 2012-06-28 | 2015-09-30 | 广东先导稀材股份有限公司 | 无筛板的流化床及三氯化硼的制备方法 |
| CN115124048A (zh) * | 2022-06-13 | 2022-09-30 | 安徽泽升科技有限公司 | 一种高纯三溴化硼的生产方法 |
-
1971
- 1971-03-20 DE DE19712113591 patent/DE2113591A1/de active Pending
-
1972
- 1972-03-08 NL NL7203078A patent/NL7203078A/xx unknown
- 1972-03-14 US US00234675A patent/US3839538A/en not_active Expired - Lifetime
- 1972-03-17 GB GB1258372A patent/GB1387665A/en not_active Expired
- 1972-03-17 FR FR7209396A patent/FR2130379B1/fr not_active Expired
- 1972-03-21 JP JP47028478A patent/JPS5139198B1/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US3839538A (en) | 1974-10-01 |
| GB1387665A (en) | 1975-03-19 |
| FR2130379B1 (https=) | 1974-09-13 |
| NL7203078A (https=) | 1972-09-22 |
| FR2130379A1 (https=) | 1972-11-03 |
| JPS5139198B1 (https=) | 1976-10-26 |
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