DE2109754B2 - Verfahren zur kontinuierlichen Her stellung von Aminoplastlosungen - Google Patents
Verfahren zur kontinuierlichen Her stellung von AminoplastlosungenInfo
- Publication number
- DE2109754B2 DE2109754B2 DE19712109754 DE2109754A DE2109754B2 DE 2109754 B2 DE2109754 B2 DE 2109754B2 DE 19712109754 DE19712109754 DE 19712109754 DE 2109754 A DE2109754 A DE 2109754A DE 2109754 B2 DE2109754 B2 DE 2109754B2
- Authority
- DE
- Germany
- Prior art keywords
- formaldehyde
- aminoplast
- stirred
- solution
- solutions
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 229920003180 amino resin Polymers 0.000 title claims description 19
- 238000000034 method Methods 0.000 title claims description 15
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 78
- 239000000243 solution Substances 0.000 claims description 47
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 23
- 239000004202 carbamide Substances 0.000 claims description 23
- 238000002156 mixing Methods 0.000 claims description 19
- 238000006243 chemical reaction Methods 0.000 claims description 16
- 239000003054 catalyst Substances 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 13
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 12
- 239000007864 aqueous solution Substances 0.000 claims description 11
- 229920005989 resin Polymers 0.000 claims description 10
- 239000011347 resin Substances 0.000 claims description 10
- 150000001412 amines Chemical class 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 7
- 229910021529 ammonia Inorganic materials 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 230000002378 acidificating effect Effects 0.000 claims description 5
- 150000008043 acidic salts Chemical class 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 239000008098 formaldehyde solution Substances 0.000 claims description 3
- 230000007935 neutral effect Effects 0.000 claims description 3
- 239000000376 reactant Substances 0.000 claims description 3
- 239000012429 reaction media Substances 0.000 claims description 3
- 150000007513 acids Chemical class 0.000 claims description 2
- 238000009833 condensation Methods 0.000 claims 6
- 230000005494 condensation Effects 0.000 claims 6
- 238000010924 continuous production Methods 0.000 claims 5
- 238000004519 manufacturing process Methods 0.000 claims 3
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims 2
- 241001026509 Kata Species 0.000 claims 1
- 230000006978 adaptation Effects 0.000 claims 1
- ZHNUHDYFZUAESO-OUBTZVSYSA-N aminoformaldehyde Chemical compound N[13CH]=O ZHNUHDYFZUAESO-OUBTZVSYSA-N 0.000 claims 1
- 238000004140 cleaning Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 238000002347 injection Methods 0.000 claims 1
- 239000007924 injection Substances 0.000 claims 1
- 239000003350 kerosene Substances 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 230000020477 pH reduction Effects 0.000 claims 1
- 230000035484 reaction time Effects 0.000 claims 1
- 238000004804 winding Methods 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 8
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 6
- 239000007787 solid Substances 0.000 description 5
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 235000019253 formic acid Nutrition 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 238000006482 condensation reaction Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 1
- 240000006240 Linum usitatissimum Species 0.000 description 1
- 229920000877 Melamine resin Polymers 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 1
- 150000003973 alkyl amines Chemical class 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical compound OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 description 1
- 229940106681 chloroacetic acid Drugs 0.000 description 1
- QGBSISYHAICWAH-UHFFFAOYSA-N dicyandiamide Chemical compound NC(N)=NC#N QGBSISYHAICWAH-UHFFFAOYSA-N 0.000 description 1
- 235000004426 flaxseed Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- -1 hydrogen ions Chemical class 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 230000006855 networking Effects 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
- C08G12/04—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds
- C08G12/10—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds with acyclic compounds having the moiety X=C(—N<)2 in which X is O, S or —N
- C08G12/12—Ureas; Thioureas
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Phenolic Resins Or Amino Resins (AREA)
- Adhesives Or Adhesive Processes (AREA)
Priority Applications (18)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712109754 DE2109754B2 (de) | 1971-03-02 | 1971-03-02 | Verfahren zur kontinuierlichen Her stellung von Aminoplastlosungen |
| FI43472A FI56973C (fi) | 1971-03-02 | 1972-02-17 | Foerfarande foer kontinuerlig framstaellning av aminoplastloesningar |
| JP47018590A JPS5241318B1 (enrdf_load_stackoverflow) | 1971-03-02 | 1972-02-24 | |
| SU1751532A SU451251A3 (ru) | 1971-03-02 | 1972-02-25 | Способ непрерывного получени растворов мочевиноформальдегидной смолы |
| NO58972A NO130945C (enrdf_load_stackoverflow) | 1971-03-02 | 1972-02-25 | |
| BE780022A BE780022A (fr) | 1971-03-02 | 1972-02-29 | Procede de preparation en continu de solutions d'aminoplastes |
| SE253972A SE400981B (sv) | 1971-03-02 | 1972-02-29 | Forfarande for kontinuerlig framstellning av aminoplastlosningar |
| IT4870172A IT952052B (it) | 1971-03-02 | 1972-03-01 | Procedimento per la produzione continua di soluzioni amminopla stiche |
| DD16122472A DD95686A5 (enrdf_load_stackoverflow) | 1971-03-02 | 1972-03-01 | |
| CA136,002A CA987825A (en) | 1971-03-02 | 1972-03-01 | Continuous manufacture of amino resin solutions |
| GB946072A GB1375502A (enrdf_load_stackoverflow) | 1971-03-02 | 1972-03-01 | |
| CS135972A CS171721B2 (enrdf_load_stackoverflow) | 1971-03-02 | 1972-03-01 | |
| FR7207049A FR2128470B1 (enrdf_load_stackoverflow) | 1971-03-02 | 1972-03-01 | |
| PL15380672A PL82347B1 (en) | 1971-03-02 | 1972-03-01 | Continuous manufacture of amino resin solutions[ca987825a] |
| NL7202783A NL156727B (nl) | 1971-03-02 | 1972-03-02 | Werkwijze voor het continu bereiden van een lijmoplossing op basis van een ureum-formaldehyde-condensatieprodukt. |
| RO6995472A RO59357A (enrdf_load_stackoverflow) | 1971-03-02 | 1972-03-02 | |
| US00264233A US3816376A (en) | 1971-03-02 | 1972-06-19 | Continuous manufacture of amino resin solutions |
| DE19722241995 DE2241995C2 (de) | 1971-03-02 | 1972-08-26 | Verfahren zur kontinuierlichen Herstellung von Harnstoffharzlösungen |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712109754 DE2109754B2 (de) | 1971-03-02 | 1971-03-02 | Verfahren zur kontinuierlichen Her stellung von Aminoplastlosungen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2109754A1 DE2109754A1 (de) | 1972-09-14 |
| DE2109754B2 true DE2109754B2 (de) | 1973-11-29 |
Family
ID=5800223
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712109754 Ceased DE2109754B2 (de) | 1971-03-02 | 1971-03-02 | Verfahren zur kontinuierlichen Her stellung von Aminoplastlosungen |
Country Status (16)
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2231735B1 (en) * | 2007-12-21 | 2016-06-08 | Dynea Austria GmbH | A process for the continuous production of high efficient aqueous amino formaldehyde resin solutions |
| PT2835388T (pt) | 2013-08-06 | 2017-04-04 | Basf Se | Processo para a preparação de soluções de aminoplasto |
-
1971
- 1971-03-02 DE DE19712109754 patent/DE2109754B2/de not_active Ceased
-
1972
- 1972-02-17 FI FI43472A patent/FI56973C/fi active
- 1972-02-24 JP JP47018590A patent/JPS5241318B1/ja active Pending
- 1972-02-25 SU SU1751532A patent/SU451251A3/ru active
- 1972-02-25 NO NO58972A patent/NO130945C/no unknown
- 1972-02-29 BE BE780022A patent/BE780022A/xx not_active IP Right Cessation
- 1972-02-29 SE SE253972A patent/SE400981B/xx unknown
- 1972-03-01 DD DD16122472A patent/DD95686A5/xx unknown
- 1972-03-01 GB GB946072A patent/GB1375502A/en not_active Expired
- 1972-03-01 IT IT4870172A patent/IT952052B/it active
- 1972-03-01 FR FR7207049A patent/FR2128470B1/fr not_active Expired
- 1972-03-01 PL PL15380672A patent/PL82347B1/pl unknown
- 1972-03-01 CA CA136,002A patent/CA987825A/en not_active Expired
- 1972-03-01 CS CS135972A patent/CS171721B2/cs unknown
- 1972-03-02 RO RO6995472A patent/RO59357A/ro unknown
- 1972-03-02 NL NL7202783A patent/NL156727B/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DE2109754A1 (de) | 1972-09-14 |
| CA987825A (en) | 1976-04-20 |
| SE400981B (sv) | 1978-04-17 |
| PL82347B1 (en) | 1975-10-31 |
| IT952052B (it) | 1973-07-20 |
| JPS5241318B1 (enrdf_load_stackoverflow) | 1977-10-18 |
| GB1375502A (enrdf_load_stackoverflow) | 1974-11-27 |
| NL156727B (nl) | 1978-05-16 |
| NO130945C (enrdf_load_stackoverflow) | 1975-03-12 |
| FI56973B (fi) | 1980-01-31 |
| RO59357A (enrdf_load_stackoverflow) | 1976-02-15 |
| FR2128470B1 (enrdf_load_stackoverflow) | 1974-09-13 |
| BE780022A (fr) | 1972-08-29 |
| SU451251A3 (ru) | 1974-11-25 |
| NO130945B (enrdf_load_stackoverflow) | 1974-12-02 |
| CS171721B2 (enrdf_load_stackoverflow) | 1976-10-29 |
| FI56973C (fi) | 1980-05-12 |
| FR2128470A1 (enrdf_load_stackoverflow) | 1972-10-20 |
| DD95686A5 (enrdf_load_stackoverflow) | 1973-02-12 |
| NL7202783A (enrdf_load_stackoverflow) | 1972-09-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| BI | Miscellaneous see part 2 | ||
| BHV | Refusal |