DE2060089C3 - Verfahren zur Herstellung von aktivem Magnesiumoxid mit großer spezifischer Oberfläche - Google Patents
Verfahren zur Herstellung von aktivem Magnesiumoxid mit großer spezifischer OberflächeInfo
- Publication number
- DE2060089C3 DE2060089C3 DE2060089A DE2060089A DE2060089C3 DE 2060089 C3 DE2060089 C3 DE 2060089C3 DE 2060089 A DE2060089 A DE 2060089A DE 2060089 A DE2060089 A DE 2060089A DE 2060089 C3 DE2060089 C3 DE 2060089C3
- Authority
- DE
- Germany
- Prior art keywords
- magnesium oxide
- magnesium
- magnesium hydroxide
- temperature
- specific surface
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 title claims description 33
- 239000000395 magnesium oxide Substances 0.000 title claims description 28
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 title claims description 23
- 238000000034 method Methods 0.000 title claims description 14
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 23
- 239000000347 magnesium hydroxide Substances 0.000 claims description 23
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000002002 slurry Substances 0.000 claims description 10
- 238000005406 washing Methods 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 6
- 238000003776 cleavage reaction Methods 0.000 claims description 3
- 230000007017 scission Effects 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 10
- 229910052740 iodine Inorganic materials 0.000 description 10
- 239000011630 iodine Substances 0.000 description 10
- 239000012065 filter cake Substances 0.000 description 6
- 238000001354 calcination Methods 0.000 description 5
- 238000001914 filtration Methods 0.000 description 5
- 239000012452 mother liquor Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical group [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 4
- 238000005868 electrolysis reaction Methods 0.000 description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 3
- 229910052801 chlorine Inorganic materials 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000005979 thermal decomposition reaction Methods 0.000 description 3
- 235000016068 Berberis vulgaris Nutrition 0.000 description 2
- 241000335053 Beta vulgaris Species 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910001629 magnesium chloride Inorganic materials 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 239000013535 sea water Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 1
- 238000010793 Steam injection (oil industry) Methods 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- PXQPYSJHFKRUAJ-UHFFFAOYSA-M [Cl-].[Mg+2].[O-2].[Mg+2] Chemical compound [Cl-].[Mg+2].[O-2].[Mg+2] PXQPYSJHFKRUAJ-UHFFFAOYSA-M 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
- 238000000429 assembly Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 150000002681 magnesium compounds Chemical group 0.000 description 1
- 239000003758 nuclear fuel Substances 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000004227 thermal cracking Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/02—Magnesia
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/14—Magnesium hydroxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2060089A DE2060089C3 (de) | 1970-12-07 | 1970-12-07 | Verfahren zur Herstellung von aktivem Magnesiumoxid mit großer spezifischer Oberfläche |
| GB3593471A GB1346830A (en) | 1970-12-07 | 1971-07-30 | Method of preparing active magnesium oxide with a large specific surface area |
| IL37512A IL37512A (en) | 1970-12-07 | 1971-08-16 | The preparation of active magnesium oxide with a large specific surface area |
| ES394805A ES394805A1 (es) | 1970-12-07 | 1971-09-04 | Procedimiento para la preparacion de oxido de magnesio ac- tivo con gran superficie especifica. |
| IT12948/71A IT940802B (it) | 1970-12-07 | 1971-09-28 | Procedimento per la produzione di ossido attivo di magnesio a grande superficie specifica |
| US00197155A US3800032A (en) | 1970-12-07 | 1971-11-09 | Active magnesium oxide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2060089A DE2060089C3 (de) | 1970-12-07 | 1970-12-07 | Verfahren zur Herstellung von aktivem Magnesiumoxid mit großer spezifischer Oberfläche |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2060089A1 DE2060089A1 (de) | 1972-06-22 |
| DE2060089B2 DE2060089B2 (OSRAM) | 1974-10-10 |
| DE2060089C3 true DE2060089C3 (de) | 1975-05-28 |
Family
ID=5790202
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2060089A Expired DE2060089C3 (de) | 1970-12-07 | 1970-12-07 | Verfahren zur Herstellung von aktivem Magnesiumoxid mit großer spezifischer Oberfläche |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3800032A (OSRAM) |
| DE (1) | DE2060089C3 (OSRAM) |
| ES (1) | ES394805A1 (OSRAM) |
| GB (1) | GB1346830A (OSRAM) |
| IL (1) | IL37512A (OSRAM) |
| IT (1) | IT940802B (OSRAM) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3965240A (en) * | 1973-12-12 | 1976-06-22 | Basic Incorporated | High density magnesia pellet and method for making same |
| AT337654B (de) * | 1975-01-31 | 1977-07-11 | Veitscher Magnesitwerke Ag | Verfahren zur herstellung von granuliertem magnesiumhydroxyd |
| US4035469A (en) * | 1975-12-05 | 1977-07-12 | Martin Marietta Corporation | Pretreatment of brine for boron removal |
| IT1276322B1 (it) * | 1994-07-21 | 1997-10-28 | Vbc Srl | Procedimento per la purificazione dell'idrossido di magnesio |
| JP3603473B2 (ja) * | 1996-01-31 | 2004-12-22 | 日本ゼオン株式会社 | 低発熱性ゴム組成物およびロール |
| US7771682B2 (en) * | 2006-01-31 | 2010-08-10 | Council Of Scientific And Industrial Research | Process for the preparation of magnesia (MgO) from crude Mg (OH)2 |
| CN101865856A (zh) * | 2010-06-08 | 2010-10-20 | 中冶建筑研究总院有限公司 | 一种钢渣中游离氧化镁含量分析测试方法 |
| US20130040799A1 (en) * | 2011-08-08 | 2013-02-14 | Basf Se | Process for preparing high-purity magnesium hydroxide and magnesium oxide |
| MX2021001571A (es) | 2018-08-09 | 2021-07-15 | Joint Stock Company Kaustik | Óxido de magnesio activo de alta pureza y su método de producción. |
| CN110203950A (zh) * | 2019-06-14 | 2019-09-06 | 河北镁神科技股份有限公司 | 涂料级硅酸镁锂及其专用的超细片状氧化镁以及制备方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2035460A (en) * | 1932-11-11 | 1936-03-31 | Marine Chemicals Company Ltd | Magnesium product and process of manufacture |
| US2219726A (en) * | 1940-01-06 | 1940-10-29 | Westvaco Chlorine Products Cor | Activated magnesia and method of making |
| US3111376A (en) * | 1961-02-27 | 1963-11-19 | Morton Salt Co | Production of magnesium hydroxide |
-
1970
- 1970-12-07 DE DE2060089A patent/DE2060089C3/de not_active Expired
-
1971
- 1971-07-30 GB GB3593471A patent/GB1346830A/en not_active Expired
- 1971-08-16 IL IL37512A patent/IL37512A/en unknown
- 1971-09-04 ES ES394805A patent/ES394805A1/es not_active Expired
- 1971-09-28 IT IT12948/71A patent/IT940802B/it active
- 1971-11-09 US US00197155A patent/US3800032A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| US3800032A (en) | 1974-03-26 |
| DE2060089A1 (de) | 1972-06-22 |
| DE2060089B2 (OSRAM) | 1974-10-10 |
| IT940802B (it) | 1973-02-20 |
| GB1346830A (en) | 1974-02-13 |
| ES394805A1 (es) | 1974-03-01 |
| IL37512A (en) | 1976-01-30 |
| IL37512A0 (en) | 1971-11-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| BI | Miscellaneous see part 2 | ||
| 8330 | Complete renunciation |