DE2013858A1 - Herstellung von Phosphorpentafluorid - Google Patents
Herstellung von PhosphorpentafluoridInfo
- Publication number
- DE2013858A1 DE2013858A1 DE19702013858 DE2013858A DE2013858A1 DE 2013858 A1 DE2013858 A1 DE 2013858A1 DE 19702013858 DE19702013858 DE 19702013858 DE 2013858 A DE2013858 A DE 2013858A DE 2013858 A1 DE2013858 A1 DE 2013858A1
- Authority
- DE
- Germany
- Prior art keywords
- acid
- phosphorus pentafluoride
- sulfur trioxide
- hexafluorophosphoric acid
- phosphorus
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- OBCUTHMOOONNBS-UHFFFAOYSA-N phosphorus pentafluoride Chemical compound FP(F)(F)(F)F OBCUTHMOOONNBS-UHFFFAOYSA-N 0.000 title claims description 32
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 claims description 37
- 238000000034 method Methods 0.000 claims description 25
- PNGLEYLFMHGIQO-UHFFFAOYSA-M sodium;3-(n-ethyl-3-methoxyanilino)-2-hydroxypropane-1-sulfonate;dihydrate Chemical compound O.O.[Na+].[O-]S(=O)(=O)CC(O)CN(CC)C1=CC=CC(OC)=C1 PNGLEYLFMHGIQO-UHFFFAOYSA-M 0.000 claims description 22
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 16
- 229910000040 hydrogen fluoride Inorganic materials 0.000 claims description 16
- FFUQCRZBKUBHQT-UHFFFAOYSA-N phosphoryl fluoride Chemical compound FP(F)(F)=O FFUQCRZBKUBHQT-UHFFFAOYSA-N 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- UQSQSQZYBQSBJZ-UHFFFAOYSA-N fluorosulfonic acid Chemical compound OS(F)(=O)=O UQSQSQZYBQSBJZ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- VFNGKCDDZUSWLR-UHFFFAOYSA-N disulfuric acid Chemical compound OS(=O)(=O)OS(O)(=O)=O VFNGKCDDZUSWLR-UHFFFAOYSA-N 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- 239000000376 reactant Substances 0.000 claims description 4
- 239000007795 chemical reaction product Substances 0.000 claims description 3
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 239000012442 inert solvent Substances 0.000 claims description 2
- 229910052698 phosphorus Inorganic materials 0.000 claims description 2
- 239000011574 phosphorus Substances 0.000 claims description 2
- VVRKSAMWBNJDTH-UHFFFAOYSA-N difluorophosphane Chemical compound FPF VVRKSAMWBNJDTH-UHFFFAOYSA-N 0.000 claims 1
- 229910019256 POF3 Inorganic materials 0.000 description 4
- 101100408805 Schizosaccharomyces pombe (strain 972 / ATCC 24843) pof3 gene Proteins 0.000 description 4
- 229910004713 HPF6 Inorganic materials 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- QTZBTBLHYPSFMG-UHFFFAOYSA-N 5-chloro-3-methylpyridin-2-amine Chemical compound CC1=CC(Cl)=CN=C1N QTZBTBLHYPSFMG-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- DWYMPOCYEZONEA-UHFFFAOYSA-N fluorophosphoric acid Chemical compound OP(O)(F)=O DWYMPOCYEZONEA-UHFFFAOYSA-N 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000283707 Capra Species 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- 229910004698 HPO2F2 Inorganic materials 0.000 description 1
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 1
- CQXADFVORZEARL-UHFFFAOYSA-N Rilmenidine Chemical compound C1CC1C(C1CC1)NC1=NCCO1 CQXADFVORZEARL-UHFFFAOYSA-N 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical group 0.000 description 1
- -1 hexafluorophosphoric acid hydrate Chemical compound 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 210000004197 pelvis Anatomy 0.000 description 1
- UHZYTMXLRWXGPK-UHFFFAOYSA-N phosphorus pentachloride Chemical compound ClP(Cl)(Cl)(Cl)Cl UHZYTMXLRWXGPK-UHFFFAOYSA-N 0.000 description 1
- WKFBZNUBXWCCHG-UHFFFAOYSA-N phosphorus trifluoride Chemical compound FP(F)F WKFBZNUBXWCCHG-UHFFFAOYSA-N 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229950011008 tetrachloroethylene Drugs 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/10—Halides or oxyhalides of phosphorus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB01526/70A GB1298159A (en) | 1970-03-10 | 1970-03-10 | Manufacture of phosphorus pentafluoride |
| FR7009646A FR2082502A5 (https=) | 1970-03-10 | 1970-03-18 | |
| DE19702013858 DE2013858A1 (de) | 1970-03-10 | 1970-03-23 | Herstellung von Phosphorpentafluorid |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB01526/70A GB1298159A (en) | 1970-03-10 | 1970-03-10 | Manufacture of phosphorus pentafluoride |
| FR7009646A FR2082502A5 (https=) | 1970-03-10 | 1970-03-18 | |
| DE19702013858 DE2013858A1 (de) | 1970-03-10 | 1970-03-23 | Herstellung von Phosphorpentafluorid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2013858A1 true DE2013858A1 (de) | 1971-10-14 |
Family
ID=27182490
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19702013858 Pending DE2013858A1 (de) | 1970-03-10 | 1970-03-23 | Herstellung von Phosphorpentafluorid |
Country Status (3)
| Country | Link |
|---|---|
| DE (1) | DE2013858A1 (https=) |
| FR (1) | FR2082502A5 (https=) |
| GB (1) | GB1298159A (https=) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN120057872A (zh) * | 2025-04-29 | 2025-05-30 | 池州天赐高新材料有限公司 | 一种以二氟磷酸为原料合成五氟化磷的方法 |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1394108A1 (en) * | 2002-08-19 | 2004-03-03 | Lithdyne LLC | Preparation of hexafluorophosphoric acid |
| JP5254555B2 (ja) | 2007-02-08 | 2013-08-07 | ステラケミファ株式会社 | 五フッ化リン及び六フッ化リン酸塩の製造方法 |
| JP5307409B2 (ja) | 2007-08-16 | 2013-10-02 | ステラケミファ株式会社 | 五フッ化リン及び六フッ化リン酸塩の製造方法 |
| JP2010042937A (ja) | 2008-08-08 | 2010-02-25 | Stella Chemifa Corp | 五フッ化リン及び六フッ化リン酸塩の製造方法 |
| CN115106022B (zh) * | 2022-06-20 | 2024-06-21 | 江苏九九久科技有限公司 | 利用热形变控制反应进程的高安全五氟化磷发生器 |
| CN115784181B (zh) * | 2022-11-22 | 2023-09-22 | 福建省德旭新材料有限公司 | 五氟化磷的连续反应精馏制备系统及其制备 |
| CN121735214A (zh) * | 2024-09-27 | 2026-03-27 | 九江天赐高新材料有限公司 | 一种五氟化磷制备方法 |
| CN120246946B (zh) * | 2025-06-03 | 2025-09-09 | 池州天赐高新材料有限公司 | 一种采用磷酸与氟化氢高效合成五氟化磷的方法 |
| CN120246947B (zh) * | 2025-06-03 | 2025-09-05 | 池州天赐高新材料有限公司 | 采用管式反应器以连续性反应制备五氟化磷的方法和系统 |
-
1970
- 1970-03-10 GB GB01526/70A patent/GB1298159A/en not_active Expired
- 1970-03-18 FR FR7009646A patent/FR2082502A5/fr not_active Expired
- 1970-03-23 DE DE19702013858 patent/DE2013858A1/de active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN120057872A (zh) * | 2025-04-29 | 2025-05-30 | 池州天赐高新材料有限公司 | 一种以二氟磷酸为原料合成五氟化磷的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2082502A5 (https=) | 1971-12-10 |
| GB1298159A (en) | 1972-11-29 |
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