DE1918697B2 - Verfahren zur herstellung von phosphornitridchloriden - Google Patents
Verfahren zur herstellung von phosphornitridchloridenInfo
- Publication number
- DE1918697B2 DE1918697B2 DE19691918697 DE1918697A DE1918697B2 DE 1918697 B2 DE1918697 B2 DE 1918697B2 DE 19691918697 DE19691918697 DE 19691918697 DE 1918697 A DE1918697 A DE 1918697A DE 1918697 B2 DE1918697 B2 DE 1918697B2
- Authority
- DE
- Germany
- Prior art keywords
- phosphorus
- ammonia
- solution
- cyclic
- phosphorus pentachloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 title description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 35
- 229910021529 ammonia Inorganic materials 0.000 claims description 18
- 229910052698 phosphorus Inorganic materials 0.000 claims description 18
- 239000011574 phosphorus Substances 0.000 claims description 18
- UHZYTMXLRWXGPK-UHFFFAOYSA-N phosphorus pentachloride Chemical compound ClP(Cl)(Cl)(Cl)Cl UHZYTMXLRWXGPK-UHFFFAOYSA-N 0.000 claims description 14
- -1 phosphorus nitride Chemical class 0.000 claims description 12
- 125000004122 cyclic group Chemical group 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 claims description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- 239000012442 inert solvent Substances 0.000 claims description 4
- 239000003208 petroleum Substances 0.000 claims description 3
- 150000001805 chlorine compounds Chemical class 0.000 claims description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims 3
- 239000007795 chemical reaction product Substances 0.000 claims 2
- GJQZKBVGMRTLJN-UHFFFAOYSA-N [P].P(Cl)(Cl)Cl Chemical compound [P].P(Cl)(Cl)Cl GJQZKBVGMRTLJN-UHFFFAOYSA-N 0.000 claims 1
- 150000004820 halides Chemical class 0.000 claims 1
- 229930195733 hydrocarbon Natural products 0.000 claims 1
- 150000002430 hydrocarbons Chemical class 0.000 claims 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 10
- QPFMBZIOSGYJDE-UHFFFAOYSA-N 1,1,2,2-tetrachloroethane Chemical compound ClC(Cl)C(Cl)Cl QPFMBZIOSGYJDE-UHFFFAOYSA-N 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 4
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 3
- 239000011541 reaction mixture Substances 0.000 description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 239000012043 crude product Substances 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 150000004767 nitrides Chemical class 0.000 description 2
- FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical compound ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- UXJHQBVRZUANLK-UHFFFAOYSA-N azanylidyne(dichloro)-$l^{5}-phosphane Chemical class ClP(Cl)#N UXJHQBVRZUANLK-UHFFFAOYSA-N 0.000 description 1
- ZSTLPJLUQNQBDQ-UHFFFAOYSA-N azanylidyne(dihydroxy)-$l^{5}-phosphane Chemical compound OP(O)#N ZSTLPJLUQNQBDQ-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- VZGDMQKNWNREIO-UHFFFAOYSA-N carbon tetrachloride Substances ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- OHZZTXYKLXZFSZ-UHFFFAOYSA-I manganese(3+) 5,10,15-tris(1-methylpyridin-1-ium-4-yl)-20-(1-methylpyridin-4-ylidene)porphyrin-22-ide pentachloride Chemical compound [Cl-].[Cl-].[Cl-].[Cl-].[Cl-].[Mn+3].C1=CN(C)C=CC1=C1C(C=C2)=NC2=C(C=2C=C[N+](C)=CC=2)C([N-]2)=CC=C2C(C=2C=C[N+](C)=CC=2)=C(C=C2)N=C2C(C=2C=C[N+](C)=CC=2)=C2N=C1C=C2 OHZZTXYKLXZFSZ-UHFFFAOYSA-I 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- OBSZRRSYVTXPNB-UHFFFAOYSA-N tetraphosphorus Chemical compound P12P3P1P32 OBSZRRSYVTXPNB-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/097—Compounds containing nitrogen and non-metals and optionally metals containing phosphorus atoms
- C01B21/098—Phosphonitrilic dihalides; Polymers thereof
- C01B21/0986—Phosphonitrilic dichlorides; Polymers thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691918697 DE1918697B2 (de) | 1969-04-12 | 1969-04-12 | Verfahren zur herstellung von phosphornitridchloriden |
| US26749A US3656916A (en) | 1969-04-12 | 1970-04-08 | Production of phosphonitrilic chlorides |
| NL7005128A NL7005128A (enrdf_load_stackoverflow) | 1969-04-12 | 1970-04-09 | |
| FR7012842A FR2043129A5 (enrdf_load_stackoverflow) | 1969-04-12 | 1970-04-09 | |
| GB1296439D GB1296439A (enrdf_load_stackoverflow) | 1969-04-12 | 1970-04-10 | |
| BE748775D BE748775A (fr) | 1969-04-12 | 1970-04-10 | Procede pour la fabrication de nitrurochlorures de phosphore |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691918697 DE1918697B2 (de) | 1969-04-12 | 1969-04-12 | Verfahren zur herstellung von phosphornitridchloriden |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE1918697A1 DE1918697A1 (de) | 1970-11-05 |
| DE1918697B2 true DE1918697B2 (de) | 1973-08-23 |
Family
ID=5731048
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19691918697 Granted DE1918697B2 (de) | 1969-04-12 | 1969-04-12 | Verfahren zur herstellung von phosphornitridchloriden |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3656916A (enrdf_load_stackoverflow) |
| BE (1) | BE748775A (enrdf_load_stackoverflow) |
| DE (1) | DE1918697B2 (enrdf_load_stackoverflow) |
| FR (1) | FR2043129A5 (enrdf_load_stackoverflow) |
| GB (1) | GB1296439A (enrdf_load_stackoverflow) |
| NL (1) | NL7005128A (enrdf_load_stackoverflow) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4046857A (en) * | 1974-07-01 | 1977-09-06 | Fmc Corporation | Continuous process for the production of phosphonitrilic chlorides |
| US4196179A (en) * | 1975-07-03 | 1980-04-01 | Ethyl Corporation | Process for preparing high cyclic phosphonitrilic halides |
| US4198381A (en) * | 1978-08-21 | 1980-04-15 | Ethyl Corporation | Process for preparing low molecular weight linear phosphonitrilic chloride oligomers |
| US4892025A (en) * | 1988-07-22 | 1990-01-09 | Steinberger Sound Corporation | Tremolo device having an adjustable counterspring and lock |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1157097A (fr) * | 1956-08-01 | 1958-05-27 | Cfmc | Nouveaux composés du phosphore, leurs procédés de préparation et leurs applications dans l'ignifugation |
| GB905314A (en) * | 1958-04-25 | 1962-09-05 | Albright & Wilson Mfg Ltd | The production of cyclic phosphonitrilic chloride polymers |
-
1969
- 1969-04-12 DE DE19691918697 patent/DE1918697B2/de active Granted
-
1970
- 1970-04-08 US US26749A patent/US3656916A/en not_active Expired - Lifetime
- 1970-04-09 NL NL7005128A patent/NL7005128A/xx unknown
- 1970-04-09 FR FR7012842A patent/FR2043129A5/fr not_active Expired
- 1970-04-10 GB GB1296439D patent/GB1296439A/en not_active Expired
- 1970-04-10 BE BE748775D patent/BE748775A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE1918697A1 (de) | 1970-11-05 |
| BE748775A (fr) | 1970-10-12 |
| NL7005128A (enrdf_load_stackoverflow) | 1970-10-14 |
| FR2043129A5 (enrdf_load_stackoverflow) | 1971-02-12 |
| US3656916A (en) | 1972-04-18 |
| GB1296439A (enrdf_load_stackoverflow) | 1972-11-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| EHV | Ceased/renunciation |