DE1496611B1 - Durchsichtige glaskeramik mit niedrigem waermeausdehnungs koeffizienten verfahren zur herstellung eines aus ihr be stehenden gegenstanes ihre verwendung in teleskopspiegeln sowie thermisch kristallisierbares gla - Google Patents
Durchsichtige glaskeramik mit niedrigem waermeausdehnungs koeffizienten verfahren zur herstellung eines aus ihr be stehenden gegenstanes ihre verwendung in teleskopspiegeln sowie thermisch kristallisierbares glaInfo
- Publication number
- DE1496611B1 DE1496611B1 DE19651496611 DE1496611A DE1496611B1 DE 1496611 B1 DE1496611 B1 DE 1496611B1 DE 19651496611 DE19651496611 DE 19651496611 DE 1496611 A DE1496611 A DE 1496611A DE 1496611 B1 DE1496611 B1 DE 1496611B1
- Authority
- DE
- Germany
- Prior art keywords
- glass
- temperature
- sio
- ceramic
- thermal expansion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000011521 glass Substances 0.000 title description 109
- 239000000919 ceramic Substances 0.000 title description 36
- 238000004519 manufacturing process Methods 0.000 title description 12
- 238000000034 method Methods 0.000 title description 7
- 239000002241 glass-ceramic Substances 0.000 claims description 52
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 47
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 41
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 23
- 229910018068 Li 2 O Inorganic materials 0.000 claims description 20
- 238000002425 crystallisation Methods 0.000 claims description 17
- 230000008025 crystallization Effects 0.000 claims description 17
- 238000011065 in-situ storage Methods 0.000 claims description 10
- 239000006121 base glass Substances 0.000 claims description 9
- 239000000203 mixture Substances 0.000 description 48
- 239000013078 crystal Substances 0.000 description 37
- 238000010438 heat treatment Methods 0.000 description 32
- 239000011734 sodium Substances 0.000 description 21
- 238000010899 nucleation Methods 0.000 description 19
- 230000006911 nucleation Effects 0.000 description 19
- 238000001816 cooling Methods 0.000 description 8
- 229910000174 eucryptite Inorganic materials 0.000 description 8
- 239000000156 glass melt Substances 0.000 description 5
- 239000011159 matrix material Substances 0.000 description 5
- 239000002667 nucleating agent Substances 0.000 description 5
- 229910052642 spodumene Inorganic materials 0.000 description 5
- 238000011282 treatment Methods 0.000 description 5
- 238000004031 devitrification Methods 0.000 description 4
- 238000000227 grinding Methods 0.000 description 4
- 238000005498 polishing Methods 0.000 description 4
- 238000002441 X-ray diffraction Methods 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
- CNLWCVNCHLKFHK-UHFFFAOYSA-N aluminum;lithium;dioxido(oxo)silane Chemical compound [Li+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O CNLWCVNCHLKFHK-UHFFFAOYSA-N 0.000 description 3
- 230000014509 gene expression Effects 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 230000003287 optical effect Effects 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 235000019738 Limestone Nutrition 0.000 description 2
- 229910052785 arsenic Inorganic materials 0.000 description 2
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 239000006028 limestone Substances 0.000 description 2
- FUJCRWPEOMXPAD-UHFFFAOYSA-N lithium oxide Chemical compound [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 description 2
- 229910001947 lithium oxide Inorganic materials 0.000 description 2
- 239000013081 microcrystal Substances 0.000 description 2
- 239000006060 molten glass Substances 0.000 description 2
- 230000000737 periodic effect Effects 0.000 description 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 2
- 239000005297 pyrex Substances 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- 230000037390 scarring Effects 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910052845 zircon Inorganic materials 0.000 description 2
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 description 2
- 229910052644 β-spodumene Inorganic materials 0.000 description 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229910013553 LiNO Inorganic materials 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 241001508691 Martes zibellina Species 0.000 description 1
- 101150049168 Nisch gene Proteins 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- HEHRHMRHPUNLIR-UHFFFAOYSA-N aluminum;hydroxy-[hydroxy(oxo)silyl]oxy-oxosilane;lithium Chemical compound [Li].[Al].O[Si](=O)O[Si](O)=O.O[Si](=O)O[Si](O)=O HEHRHMRHPUNLIR-UHFFFAOYSA-N 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 239000003484 crystal nucleating agent Substances 0.000 description 1
- 239000006092 crystalline glass-ceramic Substances 0.000 description 1
- 238000002224 dissection Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 229910052670 petalite Inorganic materials 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 239000004323 potassium nitrate Substances 0.000 description 1
- 235000010333 potassium nitrate Nutrition 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 238000010583 slow cooling Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- 210000004127 vitreous body Anatomy 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/10—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels to produce uniformly-coloured transparent products
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
- C03C10/0018—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing SiO2, Al2O3 and monovalent metal oxide as main constituents
- C03C10/0027—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing SiO2, Al2O3 and monovalent metal oxide as main constituents containing SiO2, Al2O3, Li2O as main constituents
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/083—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound
- C03C3/085—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound containing an oxide of a divalent metal
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/02—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of crystals, e.g. rock-salt, semi-conductors
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/08—Mirrors
- G02B5/10—Mirrors with curved faces
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- General Physics & Mathematics (AREA)
- Dispersion Chemistry (AREA)
- Ceramic Engineering (AREA)
- Optics & Photonics (AREA)
- Glass Compositions (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US38669364A | 1964-07-31 | 1964-07-31 | |
| US39601164A | 1964-09-14 | 1964-09-14 | |
| US46414765A | 1965-06-15 | 1965-06-15 | |
| US46809165A | 1965-06-29 | 1965-06-29 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1496611B1 true DE1496611B1 (de) | 1972-02-03 |
Family
ID=27503264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19651496611 Withdrawn DE1496611B1 (de) | 1964-07-31 | 1965-07-30 | Durchsichtige glaskeramik mit niedrigem waermeausdehnungs koeffizienten verfahren zur herstellung eines aus ihr be stehenden gegenstanes ihre verwendung in teleskopspiegeln sowie thermisch kristallisierbares gla |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS4910134B1 (enrdf_load_stackoverflow) |
| BE (1) | BE706265A (enrdf_load_stackoverflow) |
| CH (1) | CH491827A (enrdf_load_stackoverflow) |
| DE (1) | DE1496611B1 (enrdf_load_stackoverflow) |
| GB (2) | GB1124001A (enrdf_load_stackoverflow) |
| NL (1) | NL6509945A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2901172A1 (de) * | 1978-02-06 | 1979-08-16 | Ibm | Verfahren zum herstellen von mehrschichtigen gesinterten glaskeramiksubstraten mit aus gold, silber oder kupfer bestehenden leitungsmustern und dadurch hergestellte substrate |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2076470B1 (fr) * | 2006-10-27 | 2017-12-13 | Eurokera S.N.C. | Procede d'affinage d'un verre alumino-silicate de lithium et vitroceramique obtenue |
| FR2907776B1 (fr) * | 2006-10-27 | 2009-02-06 | Snc Eurokera Soc En Nom Collec | Vitroceramique de beta-quartz bleues, articles en lesdites vitroceramiques; procede de fabrication |
| FR2946039A1 (fr) * | 2009-05-29 | 2010-12-03 | Eurokera | Plaque en vitroceramique |
| RU2448918C1 (ru) * | 2010-11-22 | 2012-04-27 | Государственное образовательное учреждение высшего профессионального образования "Томский государственный архитектурно-строительный университет" (ГОУВПО "ТГАСУ") | Стеклокристаллический материал для напольной и облицовочной плитки |
| EP2890652B1 (en) * | 2012-08-28 | 2022-09-14 | Corning Incorporated | Colored and opaque glass-ceramic(s), associated colorable and ceramable glass(es), and associated process(es) |
| US9751798B2 (en) * | 2014-06-30 | 2017-09-05 | Corning Incorporated | White, opaque,β-spodumene glass-ceramic articles with inherent damage resistance and methods for making the same |
| JP2016047795A (ja) * | 2015-10-07 | 2016-04-07 | ユーロケラ | ベータ石英ガラスセラミックおよび関連する前駆体ガラス |
| CN107915412A (zh) * | 2017-12-01 | 2018-04-17 | 成都光明光电股份有限公司 | 微晶玻璃及其基板 |
| CN111971257A (zh) | 2018-03-28 | 2020-11-20 | 康宁股份有限公司 | 具有低介电损耗的硼磷酸盐玻璃陶瓷 |
| US12054422B2 (en) | 2021-06-18 | 2024-08-06 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| US12378152B2 (en) | 2021-06-18 | 2025-08-05 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| WO2022266273A1 (en) * | 2021-06-18 | 2022-12-22 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| US11597674B2 (en) | 2021-06-18 | 2023-03-07 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| WO2022266400A1 (en) * | 2021-06-18 | 2022-12-22 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| US11634354B2 (en) | 2021-06-18 | 2023-04-25 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| EP4164992B1 (en) | 2021-06-18 | 2023-08-23 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| DE102022123616A1 (de) * | 2022-09-15 | 2024-03-21 | Schott Ag | Glaskeramik mit spezifischem thermischen Ausdehnungsverhalten |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1045056B (de) * | 1956-06-04 | 1958-11-27 | Corning Glass Works | Verfahren zum Herstellen kristalliner oder glasig-kristalliner Erzeugnisse und danach hergestellte Gegenstaende |
| US3117881A (en) * | 1959-10-15 | 1964-01-14 | Owens Illinois Glass Co | Process for making devitrified products |
-
1965
- 1965-07-30 NL NL6509945A patent/NL6509945A/xx unknown
- 1965-07-30 DE DE19651496611 patent/DE1496611B1/de not_active Withdrawn
- 1965-07-31 JP JP4618265A patent/JPS4910134B1/ja active Pending
- 1965-08-02 GB GB3291265A patent/GB1124001A/en not_active Expired
- 1965-08-02 GB GB532468A patent/GB1124002A/en not_active Expired
- 1965-08-02 CH CH1082465A patent/CH491827A/de not_active IP Right Cessation
-
1967
- 1967-11-09 BE BE706265D patent/BE706265A/xx unknown
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1045056B (de) * | 1956-06-04 | 1958-11-27 | Corning Glass Works | Verfahren zum Herstellen kristalliner oder glasig-kristalliner Erzeugnisse und danach hergestellte Gegenstaende |
| US3117881A (en) * | 1959-10-15 | 1964-01-14 | Owens Illinois Glass Co | Process for making devitrified products |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2901172A1 (de) * | 1978-02-06 | 1979-08-16 | Ibm | Verfahren zum herstellen von mehrschichtigen gesinterten glaskeramiksubstraten mit aus gold, silber oder kupfer bestehenden leitungsmustern und dadurch hergestellte substrate |
Also Published As
| Publication number | Publication date |
|---|---|
| GB1124002A (en) | 1968-08-14 |
| CH491827A (de) | 1970-06-15 |
| NL6509945A (enrdf_load_stackoverflow) | 1966-02-01 |
| JPS4910134B1 (enrdf_load_stackoverflow) | 1974-03-08 |
| GB1124001A (en) | 1968-08-14 |
| BE706265A (enrdf_load_stackoverflow) | 1968-03-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EHJ | Ceased/non-payment of the annual fee |