DE1495228B2 - Verfahren zur herstellung von pulverfoermigen polymerisaten oder copolymerisaten des trioxans - Google Patents
Verfahren zur herstellung von pulverfoermigen polymerisaten oder copolymerisaten des trioxansInfo
- Publication number
- DE1495228B2 DE1495228B2 DE19621495228 DE1495228A DE1495228B2 DE 1495228 B2 DE1495228 B2 DE 1495228B2 DE 19621495228 DE19621495228 DE 19621495228 DE 1495228 A DE1495228 A DE 1495228A DE 1495228 B2 DE1495228 B2 DE 1495228B2
- Authority
- DE
- Germany
- Prior art keywords
- polymerization
- trioxane
- polymers
- cylinder
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- BGJSXRVXTHVRSN-UHFFFAOYSA-N 1,3,5-trioxane Chemical compound C1OCOCO1 BGJSXRVXTHVRSN-UHFFFAOYSA-N 0.000 title claims description 15
- 238000000034 method Methods 0.000 title claims description 14
- 238000004519 manufacturing process Methods 0.000 title claims 3
- 238000006116 polymerization reaction Methods 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 14
- 229920000642 polymer Polymers 0.000 claims description 14
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 3
- 229910015900 BF3 Inorganic materials 0.000 claims description 2
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims description 2
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 claims description 2
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- 239000000178 monomer Substances 0.000 claims 7
- 230000000379 polymerizing effect Effects 0.000 claims 4
- 239000007787 solid Substances 0.000 claims 4
- DHXVGJBLRPWPCS-UHFFFAOYSA-N Tetrahydropyran Chemical compound C1CCOCC1 DHXVGJBLRPWPCS-UHFFFAOYSA-N 0.000 claims 3
- 238000006243 chemical reaction Methods 0.000 claims 3
- 239000002685 polymerization catalyst Substances 0.000 claims 3
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims 2
- 150000004292 cyclic ethers Chemical class 0.000 claims 2
- 239000003085 diluting agent Substances 0.000 claims 2
- 239000000047 product Substances 0.000 claims 2
- 238000010008 shearing Methods 0.000 claims 2
- RBACIKXCRWGCBB-UHFFFAOYSA-N 1,2-Epoxybutane Chemical compound CCC1CO1 RBACIKXCRWGCBB-UHFFFAOYSA-N 0.000 claims 1
- ULAGGPJVDRGWTI-UHFFFAOYSA-N 1,3,5-trioxepane Chemical compound C1COCOCO1 ULAGGPJVDRGWTI-UHFFFAOYSA-N 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 241000237858 Gastropoda Species 0.000 claims 1
- 241000270295 Serpentes Species 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 239000003245 coal Substances 0.000 claims 1
- 229920001577 copolymer Polymers 0.000 claims 1
- 238000007334 copolymerization reaction Methods 0.000 claims 1
- 125000004122 cyclic group Chemical group 0.000 claims 1
- 230000000694 effects Effects 0.000 claims 1
- LEQAOMBKQFMDFZ-UHFFFAOYSA-N glyoxal Chemical compound O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 claims 1
- 229920006158 high molecular weight polymer Polymers 0.000 claims 1
- 239000003701 inert diluent Substances 0.000 claims 1
- 239000000463 material Substances 0.000 claims 1
- 125000001971 neopentyl group Chemical group [H]C([*])([H])C(C([H])([H])[H])(C([H])([H])[H])C([H])([H])[H] 0.000 claims 1
- AHHWIHXENZJRFG-UHFFFAOYSA-N oxetane Chemical compound C1COC1 AHHWIHXENZJRFG-UHFFFAOYSA-N 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims 1
- 229920001169 thermoplastic Polymers 0.000 claims 1
- 239000004416 thermosoftening plastic Substances 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- QPFMBZIOSGYJDE-UHFFFAOYSA-N 1,1,2,2-tetrachloroethane Chemical compound ClC(Cl)C(Cl)Cl QPFMBZIOSGYJDE-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- SFXNZFATUMWBHR-UHFFFAOYSA-N 2-morpholin-4-yl-2-pyridin-3-ylacetonitrile Chemical compound C=1C=CN=CC=1C(C#N)N1CCOCC1 SFXNZFATUMWBHR-UHFFFAOYSA-N 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- 241000282320 Panthera leo Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- NKDDWNXOKDWJAK-UHFFFAOYSA-N dimethoxymethane Chemical compound COCOC NKDDWNXOKDWJAK-UHFFFAOYSA-N 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 150000003018 phosphorus compounds Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2/00—Addition polymers of aldehydes or cyclic oligomers thereof or of ketones; Addition copolymers thereof with less than 50 molar percent of other substances
- C08G2/06—Catalysts
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2/00—Addition polymers of aldehydes or cyclic oligomers thereof or of ketones; Addition copolymers thereof with less than 50 molar percent of other substances
- C08G2/10—Polymerisation of cyclic oligomers of formaldehyde
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2/00—Addition polymers of aldehydes or cyclic oligomers thereof or of ketones; Addition copolymers thereof with less than 50 molar percent of other substances
- C08G2/18—Copolymerisation of aldehydes or ketones
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyoxymethylene Polymers And Polymers With Carbon-To-Carbon Bonds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10079561A | 1961-04-05 | 1961-04-05 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE1495228A1 DE1495228A1 (de) | 1969-02-13 |
| DE1495228B2 true DE1495228B2 (de) | 1972-01-20 |
Family
ID=22281575
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19621495228 Pending DE1495228B2 (de) | 1961-04-05 | 1962-04-03 | Verfahren zur herstellung von pulverfoermigen polymerisaten oder copolymerisaten des trioxans |
Country Status (9)
| Country | Link |
|---|---|
| AT (1) | AT259228B (en, 2012) |
| BE (1) | BE616036A (en, 2012) |
| CH (1) | CH410428A (en, 2012) |
| DE (1) | DE1495228B2 (en, 2012) |
| ES (1) | ES275649A1 (en, 2012) |
| FR (1) | FR1319178A (en, 2012) |
| GB (1) | GB974819A (en, 2012) |
| NL (1) | NL276768A (en, 2012) |
| SE (1) | SE314205B (en, 2012) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0083698A1 (de) * | 1981-12-12 | 1983-07-20 | Degussa Aktiengesellschaft | Verfahren zur kontinuierlichen (Co)polymerisation von Trioxan |
| US9090770B2 (en) | 2010-04-16 | 2015-07-28 | Asahi Kasei Chemicals Corporation | Polyacetal resin composition, method for producing the same, and molded article |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3147309A1 (de) * | 1981-11-28 | 1983-06-01 | Basf Ag, 6700 Ludwigshafen | Kontinuierliches verfahren zur herstellung von oxymethylenpolymeren |
| DE4431575A1 (de) * | 1994-09-05 | 1996-03-07 | Hoechst Ag | Verfahren zur Herstellung von Polyacetalcopolymeren |
| DE10006037A1 (de) | 2000-02-10 | 2001-08-16 | Basf Ag | Verfahren zur Herstellung von Polyoxymethylenen |
| DE102004054629A1 (de) | 2004-11-11 | 2006-05-18 | Basf Ag | Basische Desaktivatoren bei der POM-Herstellung |
| US8119822B2 (en) | 2006-09-12 | 2012-02-21 | Basf Se | Ionic liquids in the preparation of POMs |
| EP2267075B1 (en) | 2008-10-28 | 2014-01-22 | Asahi Kasei Chemicals Corporation | Polyacetal resin composition and method for producing the same |
-
0
- NL NL276768D patent/NL276768A/xx unknown
- BE BE616036D patent/BE616036A/xx unknown
-
1962
- 1962-03-28 GB GB1183962A patent/GB974819A/en not_active Expired
- 1962-04-03 DE DE19621495228 patent/DE1495228B2/de active Pending
- 1962-04-04 SE SE375362A patent/SE314205B/xx unknown
- 1962-04-05 FR FR893495A patent/FR1319178A/fr not_active Expired
- 1962-04-05 AT AT281262A patent/AT259228B/de active
- 1962-04-05 CH CH417162A patent/CH410428A/fr unknown
- 1962-04-21 ES ES275649A patent/ES275649A1/es not_active Expired
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0083698A1 (de) * | 1981-12-12 | 1983-07-20 | Degussa Aktiengesellschaft | Verfahren zur kontinuierlichen (Co)polymerisation von Trioxan |
| US4412067A (en) | 1981-12-12 | 1983-10-25 | Degussa Aktiengesellschaft | Process for the continuous polymerization or copolymerization of trioxane |
| US9090770B2 (en) | 2010-04-16 | 2015-07-28 | Asahi Kasei Chemicals Corporation | Polyacetal resin composition, method for producing the same, and molded article |
Also Published As
| Publication number | Publication date |
|---|---|
| BE616036A (en, 2012) | |
| CH410428A (fr) | 1966-03-31 |
| DE1495228A1 (de) | 1969-02-13 |
| NL276768A (en, 2012) | |
| AT259228B (de) | 1968-01-10 |
| FR1319178A (fr) | 1963-02-22 |
| ES275649A1 (es) | 1962-07-01 |
| SE314205B (en, 2012) | 1969-09-01 |
| GB974819A (en) | 1964-11-11 |
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