DE1235589B - Verfahren zur Herstellung von Polyestern - Google Patents
Verfahren zur Herstellung von PolyesternInfo
- Publication number
- DE1235589B DE1235589B DEF34833A DEF0034833A DE1235589B DE 1235589 B DE1235589 B DE 1235589B DE F34833 A DEF34833 A DE F34833A DE F0034833 A DEF0034833 A DE F0034833A DE 1235589 B DE1235589 B DE 1235589B
- Authority
- DE
- Germany
- Prior art keywords
- phosphite
- polyesters
- weight
- parts
- triethylene glycol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920000728 polyester Polymers 0.000 title claims description 14
- 238000000034 method Methods 0.000 title claims description 12
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 claims description 12
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 8
- 229920001515 polyalkylene glycol Polymers 0.000 claims description 2
- SZIFAVKTNFCBPC-UHFFFAOYSA-N 2-chloroethanol Chemical compound OCCCl SZIFAVKTNFCBPC-UHFFFAOYSA-N 0.000 description 9
- AQSJGOWTSHOLKH-UHFFFAOYSA-N phosphite(3-) Chemical class [O-]P([O-])[O-] AQSJGOWTSHOLKH-UHFFFAOYSA-N 0.000 description 8
- 238000005809 transesterification reaction Methods 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 4
- UGXAIVCNTXGYSA-UHFFFAOYSA-N 2,2,2-trichloroethyl dihydrogen phosphite Chemical compound OP(O)OCC(Cl)(Cl)Cl UGXAIVCNTXGYSA-UHFFFAOYSA-N 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- 230000008030 elimination Effects 0.000 description 3
- 238000003379 elimination reaction Methods 0.000 description 3
- 229910052736 halogen Inorganic materials 0.000 description 3
- 150000002367 halogens Chemical class 0.000 description 3
- 239000004014 plasticizer Substances 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- 239000003381 stabilizer Substances 0.000 description 3
- 238000009835 boiling Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- -1 cyclic triesters Chemical class 0.000 description 2
- 150000002334 glycols Chemical class 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical group OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000002619 bicyclic group Chemical group 0.000 description 1
- 239000012230 colorless oil Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 125000004185 ester group Chemical group 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- 125000004437 phosphorous atom Chemical group 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 150000005691 triesters Chemical class 0.000 description 1
- RZIHJXIUVJCZNI-UHFFFAOYSA-N tris(2-bromopropyl) phosphite Chemical compound CC(Br)COP(OCC(C)Br)OCC(C)Br RZIHJXIUVJCZNI-UHFFFAOYSA-N 0.000 description 1
- ZLOPAJAMUJNFFN-UHFFFAOYSA-N tris(2-chloropropyl) phosphite Chemical compound CC(Cl)COP(OCC(C)Cl)OCC(C)Cl ZLOPAJAMUJNFFN-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M3/00—Liquid compositions essentially based on lubricating components other than mineral lubricating oils or fatty oils and their use as lubricants; Use as lubricants of single liquid substances
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/141—Esters of phosphorous acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/141—Esters of phosphorous acids
- C07F9/1411—Esters of phosphorous acids with hydroxyalkyl compounds with further substituents on alkyl
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/22—Di-epoxy compounds
- C08G59/30—Di-epoxy compounds containing atoms other than carbon, hydrogen, oxygen and nitrogen
- C08G59/304—Di-epoxy compounds containing atoms other than carbon, hydrogen, oxygen and nitrogen containing phosphorus
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G79/00—Macromolecular compounds obtained by reactions forming a linkage containing atoms other than silicon, sulfur, nitrogen, oxygen, and carbon with or without the latter elements in the main chain of the macromolecule
- C08G79/02—Macromolecular compounds obtained by reactions forming a linkage containing atoms other than silicon, sulfur, nitrogen, oxygen, and carbon with or without the latter elements in the main chain of the macromolecule a linkage containing phosphorus
- C08G79/04—Phosphorus linked to oxygen or to oxygen and carbon
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
- C08K5/51—Phosphorus bound to oxygen
- C08K5/52—Phosphorus bound to oxygen only
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
- C08K5/51—Phosphorus bound to oxygen
- C08K5/52—Phosphorus bound to oxygen only
- C08K5/524—Esters of phosphorous acids, e.g. of H3PO3
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2225/00—Organic macromolecular compounds containing phosphorus as ingredients in lubricant compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2225/00—Organic macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2225/02—Macromolecular compounds from phosphorus-containg monomers, obtained by reactions involving only carbon-to-carbon unsaturated bonds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Polyesters Or Polycarbonates (AREA)
- Lubricants (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL282705D NL282705A (enExample) | 1961-09-01 | ||
| DEF34833A DE1235589B (de) | 1961-09-01 | 1961-09-01 | Verfahren zur Herstellung von Polyestern |
| CH959962A CH429178A (de) | 1961-09-01 | 1962-08-10 | Verfahren zur Herstellung von Hydroxylgruppen aufweisenden Polyestern der phosphorigen Säure |
| US220076A US3254142A (en) | 1961-09-01 | 1962-08-28 | Phosphorous acid esters |
| FR908148A FR1332901A (fr) | 1961-09-01 | 1962-08-30 | Procédé de préparation de polyesters hydroxylés d'acide phosphoreux |
| GB33374/62A GB978285A (en) | 1961-09-01 | 1962-08-30 | Polyesters of phosphorous acid containing free hydroxyl groups and a process for theproduction thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF34833A DE1235589B (de) | 1961-09-01 | 1961-09-01 | Verfahren zur Herstellung von Polyestern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1235589B true DE1235589B (de) | 1967-03-02 |
Family
ID=7095734
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF34833A Pending DE1235589B (de) | 1961-09-01 | 1961-09-01 | Verfahren zur Herstellung von Polyestern |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3254142A (enExample) |
| CH (1) | CH429178A (enExample) |
| DE (1) | DE1235589B (enExample) |
| GB (1) | GB978285A (enExample) |
| NL (1) | NL282705A (enExample) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3341629A (en) * | 1964-05-12 | 1967-09-12 | Weston Chemical Corp | Polyphosphites and process of making same |
| US3442982A (en) * | 1965-10-15 | 1969-05-06 | Weston Chemical Corp | Polyphosphites of 2,2-dimethyl-3-hydroxypropyl - 2 - dimethyl - 3-hydroxypropionate |
| US3376364A (en) * | 1967-06-29 | 1968-04-02 | Weston Chemical Corp | Polyphosphite stabilizers for polymeric materials |
| BE795705A (fr) * | 1972-02-22 | 1973-08-21 | Ciba Geigy | Procede de preparation de polyfluoroalcools et leur application |
| US3986990A (en) * | 1973-01-10 | 1976-10-19 | Stauffer Chemical Company | Flame retardant polyurethane foam containing polyalkylene glycol alkyl poly-phosphites |
| US3996313A (en) * | 1973-05-15 | 1976-12-07 | Borg-Warner Corporation | Halogen containing phosphorus monools |
| DE2522538A1 (de) * | 1975-05-21 | 1976-12-09 | Bayer Ag | Polymere (2-aryloxi-aethyl)-phosphite |
| US9056258B2 (en) | 2010-01-29 | 2015-06-16 | Mattel, Inc. | Toy figures |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1011866B (de) * | 1953-10-21 | 1957-07-11 | Huels Chemische Werke Ag | Verfahren zur Herstellung von neutralen und sauren Phosphorigsaeureestern hoeherer Alkohole |
| GB796446A (en) * | 1956-03-09 | 1958-06-11 | Albright & Wilson Mfg Ltd | Improvements in or relating to the production of phosphorus-containing polyester resins |
| FR1205211A (fr) * | 1957-03-08 | 1960-02-01 | Hoechst Ag | Polyesters phosphorés et leur préparation |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2353558A (en) * | 1940-02-20 | 1944-07-11 | Atlantic Refining Co | Addition agent for lubricating oil and method of making same |
| US2938877A (en) * | 1954-01-08 | 1960-05-31 | Carlisle Chemical Works | Stabilized halogen-containing resins |
| US3056824A (en) * | 1956-07-13 | 1962-10-02 | Argus Chem | Transesterification process for producing nonsymmetrical phosphite triesters and products resulting therefrom |
| US2961454A (en) * | 1960-01-27 | 1960-11-22 | Weston Chemical Corp | Ester interchange |
| US3047608A (en) * | 1960-09-15 | 1962-07-31 | Weston Chemical Corp | Phosphites |
| US3081331A (en) * | 1961-08-07 | 1963-03-12 | Weston Chemical Corp | Poly phosphorus ester condensates and their preparation |
| US3053878A (en) * | 1961-05-23 | 1962-09-11 | Weston Chemical Corp | Pentaerythritol phosphite esters |
-
0
- NL NL282705D patent/NL282705A/xx unknown
-
1961
- 1961-09-01 DE DEF34833A patent/DE1235589B/de active Pending
-
1962
- 1962-08-10 CH CH959962A patent/CH429178A/de unknown
- 1962-08-28 US US220076A patent/US3254142A/en not_active Expired - Lifetime
- 1962-08-30 GB GB33374/62A patent/GB978285A/en not_active Expired
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1011866B (de) * | 1953-10-21 | 1957-07-11 | Huels Chemische Werke Ag | Verfahren zur Herstellung von neutralen und sauren Phosphorigsaeureestern hoeherer Alkohole |
| GB796446A (en) * | 1956-03-09 | 1958-06-11 | Albright & Wilson Mfg Ltd | Improvements in or relating to the production of phosphorus-containing polyester resins |
| FR1205211A (fr) * | 1957-03-08 | 1960-02-01 | Hoechst Ag | Polyesters phosphorés et leur préparation |
Also Published As
| Publication number | Publication date |
|---|---|
| GB978285A (en) | 1964-12-23 |
| NL282705A (enExample) | |
| CH429178A (de) | 1967-01-31 |
| US3254142A (en) | 1966-05-31 |
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